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Heat-shock properties in yttrium-oxide films synthesized from metal–ethylenediamine tetraacetic acid complex through flame-spray apparatus

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Abstract

Recently, a new deposition technique using a metal–ethylenediamine tetraacetic acid (EDTA) complex has been developed. In this study, the heat-shock properties of metal-oxide films synthesized from a metal–EDTA complex were investigated. Y2O3 films were synthesized on stainless-steel (SUS) substrate from EDTA∙Y∙H through the combustion of H2–O2 gas. A cyclic heat-shock test was conducted on the fabricated Y2O3 films through exposure to the H2-O2 flame. The existence of Y2O3 crystals was confirmed. Surface cracks or damages were not observed in the samples after the cyclic thermal test. Although the number of cross-sectional cracks, crack lengths, and cracks per unit area was increased by the heat shock, delaminations were not observed in the Y2O3 films. The results show that the prepared Y2O3 films have high thermal-shock resistance and are suitable for use as thermal barrier coatings.

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Acknowledgements

This work was supported by JSPS KAKENHI Grant Number 26420697.

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Authors and Affiliations

  1. Department of Materials Science and Technology, Nagaoka University of Technology, 1603-1 Kamitomioka, Nagaoka, Niigata, 940-2188, Japan

    D. Y. Xin, Keiji Komatsu, Keita Abe, Takashi Costa, Yutaka Ikeda, Atsushi Nakamura, Shigeo Ohshio & Hidetoshi Saitoh

  2. Chubu Chelest, 3-3-3 Hinagashigashi, Yokkaichi, Mie, 510-0886, Japan

    Yutaka Ikeda & Atsushi Nakamura

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  1. D. Y. Xin
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  2. Keiji Komatsu
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Correspondence to Keiji Komatsu.

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Xin, D.Y., Komatsu, K., Abe, K. et al. Heat-shock properties in yttrium-oxide films synthesized from metal–ethylenediamine tetraacetic acid complex through flame-spray apparatus. Appl. Phys. A 123, 194 (2017). https://doi.org/10.1007/s00339-017-0839-z

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  • DOI: https://doi.org/10.1007/s00339-017-0839-z

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