Abstract
Drying is the crucial food processing for bioactive components from plant materials before strating extraction in addition to preservation of raw plant materials during storage period. Olive leaves were dried by various methods such as microwave drying (MD), oven drying (OD) and vacuum drying (VD) at several temperature values in the present study. Mathematical models allow to develop, design and control the processes. 14 emprical equations were used to estimate the drying behaviour and the time required for drying. Convenience of the models were evaluated according to the correlation coefficient (R2), varience (S2) and root mean square deviation (D RMS ). On the other hand, the effective diffusion coefficient and energy for activation were also calculated. Effects of the drying methods on the total phenolic (TPC), flavonoid (TFC) and oleuropein contents and free radical scavenging activity (FRSA) of the olive leaves were also investigated to take into considiration the quality of the dried product. MD has proved to be the fastest drying method having the highest effective diffusivity and the lowest activation energy with a more qualitive product.
Similar content being viewed by others
References
Arslan D, Musa Özcan M (2008) Evaluation of drying methods with respect to drying kinetics, mineral content and colour characteristics of rosemary leaves. Energy Convers Manag 49:1258–1264. https://doi.org/10.1016/j.enconman.2007.08.005
Erbay Z, Icier F (2010) Thin-Layer Drying Behaviors of Olive Leaves (Olea europaea L.) J Food Process Eng 33:287–308. https://doi.org/10.1111/j.1745-4530.2008.00275.x
Arslan D, Özcan MM (2011) Dehydration of red bell-pepper (Capsicum annuum L.): Change in drying behavior, colour and antioxidant content. Food Bioprod Process 89:504–513. https://doi.org/10.1016/j.fbp.2010.09.009
Arslan D, Musa Özcan M (2010) Study the effect of sun, oven and microwave drying on quality of onion slices. LWT Food Sci Technol 43:1121–1127. https://doi.org/10.1016/j.lwt.2010.02.019
Arslan D, Özcan MM, Mengeş HO (2010) Evaluation of drying methods with respect to drying parameters, some nutritional and colour characteristics of peppermint (Mentha x piperita L.) Energy Convers Manag 51:2769–2775. https://doi.org/10.1016/j.enconman.2010.06.013
Puente-Díaz L, Ah-Hen K, Vega-Gálvez A et al (2013) Combined Infrared-Convective Drying of Murta ( Ugni molinae Turcz) Berries: Kinetic Modeling and Quality Assessment. Dry Technol 31:329–338. https://doi.org/10.1080/07373937.2012.736113
Torki-Harchegani M, Ghanbarian D, Ghasemi Pirbalouti A, Sadeghi M (2016) Dehydration behaviour, mathematical modelling, energy efficiency and essential oil yield of peppermint leaves undergoing microwave and hot air treatments. Renew Sust Energ Rev 58:407–418. https://doi.org/10.1016/j.rser.2015.12.078
Simha P, Mathew M, Ganesapillai M (2016) Empirical modeling of drying kinetics and microwave assisted extraction of bioactive compounds from Adathoda vasica and Cymbopogon citratus. Alexandria Eng J 55:141–150. https://doi.org/10.1016/j.aej.2015.12.020
Shahdadi F, Mirzaei HO, Daraei Garmakhany A (2015) Study of phenolic compound and antioxidant activity of date fruit as a function of ripening stages and drying process. J Food Sci Technol 52:1814–1819. https://doi.org/10.1007/s13197-013-1177-6
Bahloul N, Boudhrioua N, Kouhila M, Kechaou N (2009) Effect of convective solar drying on colour, total phenols and radical scavenging activity of olive leaves ( Olea europaea L.) Int J Food Sci Technol 44:2561–2567. https://doi.org/10.1111/j.1365-2621.2009.02084.x
Boudhrioua N, Bahloul N, Ben Slimen I, Kechaou N (2009) Comparison on the total phenol contents and the color of fresh and infrared dried olive leaves. Ind Crop Prod 29:412–419. https://doi.org/10.1016/j.indcrop.2008.08.001
Erbay Z, Icier F (2009) Optimization of hot air drying of olive leaves using response surface methodology. J Food Eng 91:533–541. https://doi.org/10.1016/j.jfoodeng.2008.10.004
Bualuang O, Onwude DI, Pracha K (2017) Microwave drying of germinated corn and its effect on phytochemical properties. J Sci Food Agric. https://doi.org/10.1002/jsfa.8140
Şahin S, İlbay Z, Kırbaşlar Şİ (2017) Pulsed Ultrasound Assisted Extraction of Natural Antioxidants from Mandarin ( Citrus deliciosa Tenore) Leaves: Experimental and Modeling Study. Chem Eng Commun. https://doi.org/10.1080/00986445.2017.1328414
Malik NSA, Bradford JM (2006) Changes in oleuropein levels during differentiation and development of floral buds in “Arbequina” olives. Sci Hortic (Amsterdam) 110:274–278. https://doi.org/10.1016/j.scienta.2006.07.016
Yu J, Wang L, Walzem RL et al (2005) Antioxidant activity of citrus limonoids, flavonoids, and coumarins. J Agric Food Chem 53:2009–2014. https://doi.org/10.1021/jf0484632
Nourhène B, Mohammed K, Nabil K (2008) Experimental and mathematical investigations of convective solar drying of four varieties of olive leaves. Food Bioprod Process 86:176–184. https://doi.org/10.1016/j.fbp.2007.10.001
Mohamed LA, Kouhila M, Jamali A et al (2005) Single layer solar drying behaviour of Citrus aurantium leaves under forced convection. Energy Convers Manag 46:1473–1483. https://doi.org/10.1016/j.enconman.2004.08.001
Lahsasni S, Kouhila M, Mahrouz M et al (2004) Thin layer convective solar drying and mathematical modeling of prickly pear peel (Opuntia ficus indica). Energy 29:211–224. https://doi.org/10.1016/j.energy.2003.08.009
Simal S, Femenia A, Simal S et al (2005) Drying of Red Pepper (Capsicum Annuum): Water Desorption and Quality. Int J Food Eng. https://doi.org/10.2202/1556-3758.1022
Sarimeseli A (2011) Microwave drying characteristics of coriander (Coriandrum sativum L.) leaves. Energy Convers Manag 52:1449–1453. https://doi.org/10.1016/j.enconman.2010.10.007
Ah-Hen K, Zambra CE, Aguëro JE et al (2013) Moisture Diffusivity Coefficient and Convective Drying Modelling of Murta (Ugni molinae Turcz): Influence of Temperature and Vacuum on Drying Kinetics. Food Bioprocess Technol 6:919–930. https://doi.org/10.1007/s11947-011-0758-5
Sharma GP, Verma RC, Pathare P (2005) Mathematical modeling of infrared radiation thin layer drying of onion slices. J Food Eng 71:282–286. https://doi.org/10.1016/j.jfoodeng.2005.02.010
Aghbashlo M, Kianmehr MH, Samimi-Akhijahani H (2008) Influence of drying conditions on the effective moisture diffusivity, energy of activation and energy consumption during the thin-layer drying of berberis fruit (Berberidaceae). Energy Convers Manag 49:2865–2871. https://doi.org/10.1016/j.enconman.2008.03.009
Meziane S (2011) Drying kinetics of olive pomace in a fluidized bed dryer. Energy Convers Manag 52:1644–1649. https://doi.org/10.1016/j.enconman.2010.10.027
Kaya A, Aydın O (2009) An experimental study on drying kinetics of some herbal leaves. Energy Convers Manag 50:118–124. https://doi.org/10.1016/j.enconman.2008.08.024
Chang C-H, Lin H-Y, Chang C-Y, Liu Y-C (2006) Comparisons on the antioxidant properties of fresh, freeze-dried and hot-air-dried tomatoes. J Food Eng 77:478–485. https://doi.org/10.1016/j.jfoodeng.2005.06.061
Szumny A, Figiel A, Gutiérrez-Ortíz A, Carbonell-Barrachina ÁA (2010) Composition of rosemary essential oil (Rosmarinus officinalis) as affected by drying method. J Food Eng 97:253–260. https://doi.org/10.1016/j.jfoodeng.2009.10.019
Hamrouni-Sellami I, Rahali FZ, Rebey IB et al (2013) Total Phenolics, Flavonoids, and Antioxidant Activity of Sage (Salvia officinalis L.) Plants as Affected by Different Drying Methods. Food Bioprocess Technol 6:806–817. https://doi.org/10.1007/s11947-012-0877-7
Hirun S, Utama-ang N, Roach PD (2014) Turmeric (Curcuma longa L.) drying: an optimization approach using microwave-vacuum drying. J Food Sci Technol 51:2127–2133. https://doi.org/10.1007/s13197-012-0709-9
Ayensu A (1997) Dehydration of food crops using a solar dryer with convective heat flow. Sol Energy 59:121–126. https://doi.org/10.1016/S0038-092X(96)00130-2
Page GE (1949) Factors influencing the maximum rates of air drying of shelled corn in thin layer. Purdue University, West Lafayette
Overhults DG, White GM, Hamilton HE, Ross IJ (1973) Drying Soybeans With Heated Air. Trans ASAE 16:112–113. https://doi.org/10.13031/2013.37459
Yagcioglu A, Degirmencioglu A, Cagatay F (1999) Drying characteristic of laurel leaves under different conditions. Proc 7th Int Congr Agric Mech energy 565–569
Madamba PS, Driscoll RH, Buckle KA (1996) The thin-layer drying characteristics of garlic slices. J Food Eng 29:75–97. https://doi.org/10.1016/0260-8774(95)00062-3
Sharaf-Eldeen YI, Blaisdell JL, Hamdy MY (1980) A Model for Ear Corn Drying. Trans ASAE 23:1261–1265. https://doi.org/10.13031/2013.34757
Demir V, Gunhan T, Yagcioglu AK (2007) Mathematical modelling of convection drying of green table olives. Biosyst Eng 98:47–53. https://doi.org/10.1016/j.biosystemseng.2007.06.011
Verma L, Bucklin R, Endan J, Wratten F (1985) Effects of Drying Air Parameters on Rice Drying Models. Trans ASAE 28:0296–0301
Aghbashlo M, Kianmehr MH, Khani S et al (2016) Thin layer drying of red pepper. J Food Eng 40:109–117. https://doi.org/10.15237/gida.GD15067
Diamante LM, Munro PA (1993) Mathematical modelling of the thin layer solar drying of sweet potato slices. Sol Energy 51:271–276. https://doi.org/10.1016/0038-092X(93)90122-5
Diamante LM, Munro PA (1991) Mathematical modeling of hot air drying of sweet potato slices. Int J Food Sci Technol 26:99–109. https://doi.org/10.1111/j.1365-2621.1991.tb01145.x
Corzo O, Bracho N, Pereira A, Vásquez A (2008) Weibull distribution for modeling air drying of coroba slices. LWT Food Sci Technol 41:2023–2028. https://doi.org/10.1016/j.lwt.2008.01.002
Acknowledgements
The authors wish to thank the Research Fund of Istanbul University for financial support for this research project (Project No: 23367).
Author information
Authors and Affiliations
Corresponding author
Ethics declarations
Conflict of Interest
The authors declare that there is no conflict of interest in writing upon submission of the manuscript.
Rights and permissions
About this article
Cite this article
Elhussein, E.A.A., Şahin, S. Drying behaviour, effective diffusivity and energy of activation of olive leaves dried by microwave, vacuum and oven drying methods. Heat Mass Transfer 54, 1901–1911 (2018). https://doi.org/10.1007/s00231-018-2278-6
Received:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s00231-018-2278-6