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Characterization of a Composite of High-Impact Polystyrene, Pseudoboehmite and Graphene Oxide

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Characterization of Minerals, Metals, and Materials 2019

Abstract

The application of a composite material of pseudoboehmite, polystyrene and graphene oxide was studied. The present work is the synthesis and characterization of high-impact polystyrene (HIPS) nanocomposite, with pseudoboehmite (PSB) and graphene oxide . Pseudoboehmite particles with nanometric dimensions were obtained by sol-gel process. The composites were characterized by mechanical tests (tensile strength , flexural strength , Izod Impact, Shore D Hardness ), thermal (Flow index, temperature of thermal deflection under load -HDT, Vicat softening temperature, differential tests thermal analyses and thermogravimetric analysis) and morphologically by Scanning Electron Microscopy (SEM) . The results obtained were compared with HIPS matrix properties , without PSB and graphene oxide addition. From the thermal analyzes, composite samples showed higher decomposition temperatures compared to pure high-impact polystyrene especially in the thermogravimetric analysis results, showing a considerable increase in the temperature at which material decomposition begins (322 °C for pure high-impact polystyrene and 380 °C for the composite).

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References

  1. Chen Y, Mao J, Wu J (2018) Microwave transparent crosslinked polystyrene nanocomposites with enhanced high voltage resistance via 3D printing bulk polymerization method. Compos Sci Technol 157(22):160–167

    Article  CAS  Google Scholar 

  2. Xue Yijiao et al (2018) Effects of heterionic montmorillonites on flame resistances of polystyrene nanocomposites and the flame retardant mechanism. J Compos Mater 52(10):1295–1303

    Article  CAS  Google Scholar 

  3. Han YQ, Wu Y, Shen MX et al (2013) Preparation and properties of polystyrene nanocomposites with graphite oxide and graphene as flame retardants. J Mater Sci 48:4214–4222

    Article  CAS  Google Scholar 

  4. Moroz EM, Shefer KI, Zyuzin DA, Ivanova AS, Kulko EV, Goidin VV, Molchanov VV (2006) Local structure of pseudoboehmites. React Kinet Catal Lett 87(2):367–375

    Article  CAS  Google Scholar 

  5. Munhoz AH Jr, Miranda LF, Uehara GN (2006) Study of pseudoboehmite by sol-gel synthesis. AST-Adv Sci Technol 45:260–265

    Article  CAS  Google Scholar 

  6. Rajamani M, Maliyekkal SM (2018) Chitosan reinforced boehmite nanocomposite desiccant: a promising alternative to silica gel. Carbohyd Polym 194:245–251

    Article  CAS  Google Scholar 

  7. Miranda LF et al (2018) Obtaining hydrogels based on PVP/PVAL/Chitosan containing pseudoboehmite nanoparticles for application in drugs. In: Haider S, Haider A (eds) Hydrogels. IntechOpen. http://dx.doi.org/10.5772/intechopen.72007

    Google Scholar 

  8. Gao W (2015) The chemistry of graphene oxide. In: Gao W (ed) Graphene oxide. Springer, Cham. https://doi.org/10.1007/978-3-319-15500-5_3

    Chapter  Google Scholar 

  9. Dikin DA, Stankovich S, Zimney EJ, Piner RD, Dommett GHB, Evmenenko G, Nguyen ST, Ruoff RS (2007) Preparation and characterization of graphene oxide paper. Nature 448:457–460

    Article  CAS  Google Scholar 

Download references

Acknowledgements

The authors thank Mackenzie Presbyterian University, CAPES, FAPESP Research Foundation (2010/19157-9 and 2017/22396-4 grants) and the Mack Pesquisa for the sponsorship of this project.

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Correspondence to Antônio Hortencio Munhoz Junior .

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Munhoz Junior, A.H. et al. (2019). Characterization of a Composite of High-Impact Polystyrene, Pseudoboehmite and Graphene Oxide. In: Li, B., et al. Characterization of Minerals, Metals, and Materials 2019. The Minerals, Metals & Materials Series. Springer, Cham. https://doi.org/10.1007/978-3-030-05749-7_51

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