Taxonomy: Physicochemical and Pharmacological Properties of Alkaloids – Amine, Amide, and Sulfur Containing Alkaloids
Biological sources: Oxytropis muricata, O. trichophysa
C15H15NO2: 241.1103
Mp: 154–155°C (Me2CO) [1]
[α]D +35° (CH3OH) [1]
UV: 204 sh, 207 [1]
IR: 3350, 1650 [1]
MS m/z: 242((M + H)+, 0.3), 241(M+, 0.4), 223(2), 135(100), 134(84), 122(14), 117(11), 107(6), 105(95), 91(4), 79(11), 77(39) [1]
1 H NMR: 3.32(1H, br s, OH), 3.51(1H, ddd, J = 5, 8, 14, H-1), 3.91(1H, ddd, J = 3.5, 7, 14, H-1), 4.95(1H, dd, J = 3.5, 8, H-2), 6.59(1H, br s, NH), 7.38(8H, m, H-Ar), 7.74(2H, dd, J = 8, 2, H-2′, H-6′) [1]
13 C NMR (DMSO-d6): [1]
Table 1
C–1 |
47.8 |
C = O |
166.6 |
Ar-C |
126.1 |
 2 |
71.3 |
1′ |
144.0 |
127.4 |
|
 3 |
134.7 |
4′ |
131.2 |
128.2 |
|
 6 |
127.2 |
128.4 |
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References
D. Batsuren, S. Tsetsegmaa, N. Batbayar, D. Dungerdorzh, V.I. Akhmedzhanova, Yu.M. Mil’grom, Ya.V. Rashkes, A.A. Ibragimov, Chem. Nat. Comp. 28, 340 (1992)
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(2013). (+)-N-Benzoyl-2-phenyl-2-hydroxyethylamine. In: Azimova, S.S., Yunusov, M.S. (eds) Natural Compounds. Springer, New York, NY. https://doi.org/10.1007/978-1-4614-0560-3_83
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