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Nanocrystalline manganese dioxide synthesis by microwave-hydrothermal treatment

  • Synthesis and Properties of Inorganic Compounds
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Abstract

An efficient method is proposed for preparing manganese dioxide nanoparticles via microwave-hydrothermal (MW-HT) treatment of potassium permanganate and sodium nitrite solutions in the presence of sulfuric acid. The effect of preparation parameters on the phase composition and morphology of products is analyzed. A change in pH in the reaction mixture is shown to affect the phase composition and morphology of MnO2 nanoparticles.

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Authors and Affiliations

  1. Moscow State University, Moscow, 119991, Russia

    O. V. Boytsova, T. O. Shekunova & A. E. Baranchikov

  2. Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences, Leninskii pr. 1, Moscow, 119991, Russia

    O. V. Boytsova & T. O. Shekunova

Authors
  1. O. V. Boytsova
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  2. T. O. Shekunova
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  3. A. E. Baranchikov
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Correspondence to O. V. Boytsova.

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Original Russian Text © O.V. Boytsova, T.O. Shekunova, A.E. Baranchikov, 2015, published in Zhurnal Neorganicheskoi Khimii, 2015, Vol. 60, No. 5, pp. 612–617.

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Boytsova, O.V., Shekunova, T.O. & Baranchikov, A.E. Nanocrystalline manganese dioxide synthesis by microwave-hydrothermal treatment. Russ. J. Inorg. Chem. 60, 546–551 (2015). https://doi.org/10.1134/S0036023615050022

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  • DOI: https://doi.org/10.1134/S0036023615050022

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