Skip to main content
Log in

Microstructure Evolution and Mechanical and Corrosion Behavior of Accumulative Roll Bonded Mg-2%Zn/Al-7075 Multilayered Composite

  • Published:
Journal of Materials Engineering and Performance Aims and scope Submit manuscript

Abstract

Multilayered composite of Mg-2%Zn/Al-7075 was developed by accumulative roll bonding (ARB) of wrought Mg-2%Zn and aluminum 7075 alloy. The Mg-2%Zn/Al-7075 multilayered composite exhibited density of 2295 kg/m3 and an average grain size of 1 and 1.3 μm in Mg-2%Zn and Al-7075 layers, respectively. A thorough microstructural characterization was performed on the composites by scanning electron microscope, electron backscatter diffraction (EBSD), transmission electron microscope and phase analysis by x-ray diffraction. In addition, mechanical properties were evaluated by microhardness and tensile tests. Corrosion behavior of the multilayered composite was examined using electrochemical polarization test. EBSD analysis showed the presence of ultrafine grains with high-angle grain boundaries. The composite exhibited a significant improvement in ultimate tensile strength (~1.82 times) and elongation (~1.5 times) as compared with Mg-2%Zn alloy, after four-pass ARB process.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7
Fig. 8
Fig. 9
Fig. 10

Similar content being viewed by others

References

  1. G.L. Song and A. Atrens, Corrosion Mechanisms of Magnesium Alloys, Adv. Eng. Mater., 1999, 2648, p 10–33

    Google Scholar 

  2. R. Valiev, Nanostructuring of Metals by Severe Plastic Deformation for Advanced Properties, Nat. Mater., 2004, 3(8), p 511–516

    Article  Google Scholar 

  3. R.Z. Valiev, N. Krasilnikov, and N. Tsenev, Plastic Deformation of Alloys with Submicron-Grained Structure, Mater. Sci. Eng. A, 1991, 137, p 35–40

    Article  Google Scholar 

  4. Y. Saito, H. Utsunomiya, N. Tsuji, and T. Sakai, Novel Ultra-High Straining Process for Bulk Materials Development of the Accumulative Roll-Bonding (ARB) Process, Acta Mater., 1999, 47(2), p 579–583

    Article  Google Scholar 

  5. N. Tsuji, Y. Saito, H. Utsunomiya, and S. Tanigawa, Ultra-Fine Grained Bulk Steel Produced by Accumulative Roll-Bonding (ARB) Process, Scr. Mater., 1999, 40(7), p 795–800

    Article  Google Scholar 

  6. P. Hidalgo-Manrique, C.M. Cepeda-Jime, O.A. Ruano, and F. Carren, Effect of Warm Accumulative Roll Bonding on the Evolution of Microstructure, Texture and Creep Properties in the 7075 Aluminium Alloy, Mater. Sci. Eng. A, 2012, 556, p 287–294

    Article  Google Scholar 

  7. L.N. Tsuji and N. Kamikawa, Microstructure Homogeneity in Various Metallic Materials Heavily Deformed by Accumulative Roll-Bonding, Mater. Sci. Eng. A, 2006, 423, p 331–342

    Article  Google Scholar 

  8. S. Roy, B.R. Nataraj, S. Suwas, S. Kumar, and K. Chattopadhyay, Microstructure and Texture Evolution During Accumulative Roll Bonding of Aluminium Alloys AA2219/AA5086 Composite Laminates, J. Mater. Sci., 2012, 47, p 6402–6419

    Article  Google Scholar 

  9. Y. Xin, R. Hong, B. Feng, H. Yu, Y. Wu, and Q. Liu, Fabrication of Mg/AL Multilayer Plates Using an Accumulative Extrusion Bonding Process, Mater. Sci. Eng. A, 2015, 640, p 210–216

    Article  Google Scholar 

  10. N. Tsuji, Y. Saito, S.H. Lee, and Y. Minamino, ARB (Accumulative Roll-Bonding) and Other New Techniques to Produce Bulk Ultrafine Grained Materials, Adv. Eng. Mater., 2003, 5, p 338–344

    Article  Google Scholar 

  11. S. Lee, Y. Saito, N. Tsuji, H. Utsunomiya, and T. Sakai, Role of Shear Strain in Ultragrain Refinement by Accumulative Roll-Bonding (ARB) Process, Scr. Mater., 2002, 46, p 281–285

    Article  Google Scholar 

  12. P. Hidalgo-Manrique, A. Orozco-Caballero, C.M. Cepeda-Jimenez, O.A. Ruano, and F. Carreno, Influence of the Accumulative Roll Bonding Process Severity on the Microstructure and Superplastic Behaviour of 7075 Al Alloy, J. Mater. Sci. Technol., 2016, 32(8), p 774–782

    Article  Google Scholar 

  13. M.M. Avedesian, Hugh Baker, Magnesium and Magnesium Alloys, ASM Specialty Handbook, Metals Park, 1999

    Google Scholar 

  14. T.C. Lowe and R.Z. Valiev, Investigations and Applications of Severe Plastic Deformation, Kluwer, Dordrecht, 2000

    Book  Google Scholar 

  15. J. Roohollah, A. Sajjad, M.T. Reza, and B. Niroumand, Effect of Particle Size on Microstructure and Mechanical Properties of Composites Produced by ARB Process, Mater. Sci. Eng. A, 2011, 528, p 2143–2148

    Article  Google Scholar 

  16. E.A. Starke and J.T. Staley, Application of Modern Aluminum Alloys to Aircraft, Prog. Aerosp. Sci., 1996, 32, p 131–172

    Article  Google Scholar 

  17. Y. Saito, N. Tsuji, H. Utsunomiya, T. Sakai, and R.G. Hong, Ultra-Fine Grained Bulk Aluminum Produced by Accumulative Roll-Bonding (arb) Process, Scr. Mater., 1998, 39, p 1221–1227

    Article  Google Scholar 

  18. M.C. Chen, H.C. Hsieh, and W. Wu, The Evolution of Microstructures and Mechanical Properties During Accumulative Roll Bonding of Al/Mg Composite, J. Alloys Compd., 2006, 416, p 169–172

    Article  Google Scholar 

  19. H. Chang, M.Y. Zheng, C. Xub, G.D. Fan, H.G. Brokmeier, and K. Wu, Microstructure and Mechanical Properties of the Mg/Al Multilayer Fabricated by Accumulative Roll Bonding (ARB) at Ambient Temperature, Mater. Sci. Eng. A, 2012, 543, p 249–256

    Article  Google Scholar 

  20. H. Chang, M. Zheng, W. Gan, C. Xu, and H.G. Brokmeier, Texture Evolution of the Mg/Al Laminated Composite by Accumulative Roll Bonding at Ambient Temperature, Rare Metal Mater. Eng., 2013, 42, p 441–446

  21. D.M. Parisa and E. Beitallah, Microstructure and Mechanical Properties of Tri-Metal Al/Ti/Mg Laminated Composite Processed by Accumulative Roll Bonding, Mater. Sci. Eng. A, 2015, 628, p 135–142

    Article  Google Scholar 

  22. N. Tsuji, Y. Saito, S.H. Lee, and Y. Minamino, ARB (Accumulative Roll Bonding) and Other New Techniques to Produce Bulk Ultrafine Grained Materials, Adv. Eng. Mater., 2005, 5, p 338–344

    Article  Google Scholar 

  23. H. Jafarian, J.H. Livar, and S.H. Razavi, Microstructure Evolution and Mechanical Properties in Ultrafine Grained Al/TiC Composite Fabricated by Accumulative Roll Bonding, Compos. B, 2015, 77, p 84–92

    Article  Google Scholar 

  24. R. Zhang and V.L. Acoff, Processing Sheet Materials by Accumulative Roll Bonding and Reaction Annealing from Ti/Al/Nb Elemental Foils, Mater. Sci. Eng. A, 2007, 463, p 67–73

    Article  Google Scholar 

  25. C.Y. Liu, R. Jing, Q. Wang, B. Zhang, Y.Z. Jia, and M.Z. Ma, Fabrication of Al/Al3Mg2 Composite by Vacuum Annealing and Accumulative Roll-Bonding Process, Mater. Sci. Eng. A, 2012, 558, p 510–516

    Article  Google Scholar 

  26. R.J. Hebert and J.H. Perepezko, Deformation-Induced Synthesis and Structural Transformations of Metallic Multi Layers, Scr. Mater., 2004, 50, p 807–812

    Article  Google Scholar 

  27. K.R. Gopi, H. Shivananda Nayaka, and S. Sahu, Investigation of Microstructure and Mechanical Properties of ECAP-Processed AM Series Magnesium Alloy, J. Mater. Eng. Perform., 2016, 25(9), p P3737–P3745

    Article  Google Scholar 

  28. Y. Chino, K. Kimura, and M. Mabuchi, Twinning Behavior and Deformation Mechanisms of Extruded AZ31 Mg Alloy, Mater. Sci. Eng. A, 2008, 486, p 481–488

    Article  Google Scholar 

  29. S.O. Gashti, A. Fattah-alhosseini, Y. Mazaheri, and M.K. Keshavarz, Microstructure, Mechanical Properties and Electrochemical Behavior of AA1050 Processed by Accumulative Roll Bonding (ARB), J. Alloys Compd., 2009, 474, p 406–415

    Article  Google Scholar 

  30. K.D. Ralston and N. Birbilis, Effect of Grain Size on Corrosion, A Review, Corrosion, 2010, 66, p 075005–075013

    Article  Google Scholar 

  31. A. Zarebidaki, H. Mahmoudikohani, and M.R. Aboutalebi, Microstructure and Corrosion Behavior of Electrodeposited Nano-Crystalline Nickel Coating on AZ91 Mg Alloy, J. Alloys Compd., 2014, 615, p 825–830

    Article  Google Scholar 

  32. G.R. Argade, S.K. Panigrahi, and R.S. Mishra, Effects of Grain Size on the Corrosion Resistance of Wrought Magnesium Alloys Containing Neodymium, Corros. Sci., 2012, 58, p 145–151

    Article  Google Scholar 

  33. N. Birbilis and Y. Estrin, Corrosion of Pure Mg as a Function of Grain Size and Processing Route, Adv. Eng. Mater., 2008, 10, p 579–582

    Article  Google Scholar 

  34. P. Saha, M. Roy, M.K. Datta, B. Lee, and P.N. Kumta, Effects of Grain Refinement on the Bio Corrosion and In Vitro Bioactivity of Magnesium, Mater. Sci. Eng. C. Mater. Biol. Appl., 2015, 57, p 294–303

    Article  Google Scholar 

  35. G. Song, A. Atrens, and M. Dargusch, Influence of Microstructure on the Corrosion of Diecast AZ91D, Corros. Sci., 1998, 41, p 249–273

    Article  Google Scholar 

  36. A. Pardo, M.C. Merino, A.E. Coy, R. Arrabal, F. Viejo, and E. Matykina, Corrosion Behaviour of Magnesium/Aluminium Alloys in 3.5 wt.% NaCl, Corros. Sci., 2008, 50, p 823–834

    Article  Google Scholar 

Download references

Acknowledgments

The authors gratefully appreciate the support of Department of Materials Engineering, Indian Institute of Science Bangalore, India; Advanced Center for Material Science, Indian Institute of Technology Kanpur, India; and Exclusive Magnesium Private limited, Hyderabad, India, providing various testing facility for research work.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Gajanan Anne.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Anne, G., Ramesh, M.R., Shivananda Nayaka, H. et al. Microstructure Evolution and Mechanical and Corrosion Behavior of Accumulative Roll Bonded Mg-2%Zn/Al-7075 Multilayered Composite. J. of Materi Eng and Perform 26, 1726–1734 (2017). https://doi.org/10.1007/s11665-017-2576-z

Download citation

  • Received:

  • Revised:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11665-017-2576-z

Keywords

Navigation