Abstract
Multilayered composite of Mg-2%Zn/Al-7075 was developed by accumulative roll bonding (ARB) of wrought Mg-2%Zn and aluminum 7075 alloy. The Mg-2%Zn/Al-7075 multilayered composite exhibited density of 2295 kg/m3 and an average grain size of 1 and 1.3 μm in Mg-2%Zn and Al-7075 layers, respectively. A thorough microstructural characterization was performed on the composites by scanning electron microscope, electron backscatter diffraction (EBSD), transmission electron microscope and phase analysis by x-ray diffraction. In addition, mechanical properties were evaluated by microhardness and tensile tests. Corrosion behavior of the multilayered composite was examined using electrochemical polarization test. EBSD analysis showed the presence of ultrafine grains with high-angle grain boundaries. The composite exhibited a significant improvement in ultimate tensile strength (~1.82 times) and elongation (~1.5 times) as compared with Mg-2%Zn alloy, after four-pass ARB process.
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G.L. Song and A. Atrens, Corrosion Mechanisms of Magnesium Alloys, Adv. Eng. Mater., 1999, 2648, p 10–33
R. Valiev, Nanostructuring of Metals by Severe Plastic Deformation for Advanced Properties, Nat. Mater., 2004, 3(8), p 511–516
R.Z. Valiev, N. Krasilnikov, and N. Tsenev, Plastic Deformation of Alloys with Submicron-Grained Structure, Mater. Sci. Eng. A, 1991, 137, p 35–40
Y. Saito, H. Utsunomiya, N. Tsuji, and T. Sakai, Novel Ultra-High Straining Process for Bulk Materials Development of the Accumulative Roll-Bonding (ARB) Process, Acta Mater., 1999, 47(2), p 579–583
N. Tsuji, Y. Saito, H. Utsunomiya, and S. Tanigawa, Ultra-Fine Grained Bulk Steel Produced by Accumulative Roll-Bonding (ARB) Process, Scr. Mater., 1999, 40(7), p 795–800
P. Hidalgo-Manrique, C.M. Cepeda-Jime, O.A. Ruano, and F. Carren, Effect of Warm Accumulative Roll Bonding on the Evolution of Microstructure, Texture and Creep Properties in the 7075 Aluminium Alloy, Mater. Sci. Eng. A, 2012, 556, p 287–294
L.N. Tsuji and N. Kamikawa, Microstructure Homogeneity in Various Metallic Materials Heavily Deformed by Accumulative Roll-Bonding, Mater. Sci. Eng. A, 2006, 423, p 331–342
S. Roy, B.R. Nataraj, S. Suwas, S. Kumar, and K. Chattopadhyay, Microstructure and Texture Evolution During Accumulative Roll Bonding of Aluminium Alloys AA2219/AA5086 Composite Laminates, J. Mater. Sci., 2012, 47, p 6402–6419
Y. Xin, R. Hong, B. Feng, H. Yu, Y. Wu, and Q. Liu, Fabrication of Mg/AL Multilayer Plates Using an Accumulative Extrusion Bonding Process, Mater. Sci. Eng. A, 2015, 640, p 210–216
N. Tsuji, Y. Saito, S.H. Lee, and Y. Minamino, ARB (Accumulative Roll-Bonding) and Other New Techniques to Produce Bulk Ultrafine Grained Materials, Adv. Eng. Mater., 2003, 5, p 338–344
S. Lee, Y. Saito, N. Tsuji, H. Utsunomiya, and T. Sakai, Role of Shear Strain in Ultragrain Refinement by Accumulative Roll-Bonding (ARB) Process, Scr. Mater., 2002, 46, p 281–285
P. Hidalgo-Manrique, A. Orozco-Caballero, C.M. Cepeda-Jimenez, O.A. Ruano, and F. Carreno, Influence of the Accumulative Roll Bonding Process Severity on the Microstructure and Superplastic Behaviour of 7075 Al Alloy, J. Mater. Sci. Technol., 2016, 32(8), p 774–782
M.M. Avedesian, Hugh Baker, Magnesium and Magnesium Alloys, ASM Specialty Handbook, Metals Park, 1999
T.C. Lowe and R.Z. Valiev, Investigations and Applications of Severe Plastic Deformation, Kluwer, Dordrecht, 2000
J. Roohollah, A. Sajjad, M.T. Reza, and B. Niroumand, Effect of Particle Size on Microstructure and Mechanical Properties of Composites Produced by ARB Process, Mater. Sci. Eng. A, 2011, 528, p 2143–2148
E.A. Starke and J.T. Staley, Application of Modern Aluminum Alloys to Aircraft, Prog. Aerosp. Sci., 1996, 32, p 131–172
Y. Saito, N. Tsuji, H. Utsunomiya, T. Sakai, and R.G. Hong, Ultra-Fine Grained Bulk Aluminum Produced by Accumulative Roll-Bonding (arb) Process, Scr. Mater., 1998, 39, p 1221–1227
M.C. Chen, H.C. Hsieh, and W. Wu, The Evolution of Microstructures and Mechanical Properties During Accumulative Roll Bonding of Al/Mg Composite, J. Alloys Compd., 2006, 416, p 169–172
H. Chang, M.Y. Zheng, C. Xub, G.D. Fan, H.G. Brokmeier, and K. Wu, Microstructure and Mechanical Properties of the Mg/Al Multilayer Fabricated by Accumulative Roll Bonding (ARB) at Ambient Temperature, Mater. Sci. Eng. A, 2012, 543, p 249–256
H. Chang, M. Zheng, W. Gan, C. Xu, and H.G. Brokmeier, Texture Evolution of the Mg/Al Laminated Composite by Accumulative Roll Bonding at Ambient Temperature, Rare Metal Mater. Eng., 2013, 42, p 441–446
D.M. Parisa and E. Beitallah, Microstructure and Mechanical Properties of Tri-Metal Al/Ti/Mg Laminated Composite Processed by Accumulative Roll Bonding, Mater. Sci. Eng. A, 2015, 628, p 135–142
N. Tsuji, Y. Saito, S.H. Lee, and Y. Minamino, ARB (Accumulative Roll Bonding) and Other New Techniques to Produce Bulk Ultrafine Grained Materials, Adv. Eng. Mater., 2005, 5, p 338–344
H. Jafarian, J.H. Livar, and S.H. Razavi, Microstructure Evolution and Mechanical Properties in Ultrafine Grained Al/TiC Composite Fabricated by Accumulative Roll Bonding, Compos. B, 2015, 77, p 84–92
R. Zhang and V.L. Acoff, Processing Sheet Materials by Accumulative Roll Bonding and Reaction Annealing from Ti/Al/Nb Elemental Foils, Mater. Sci. Eng. A, 2007, 463, p 67–73
C.Y. Liu, R. Jing, Q. Wang, B. Zhang, Y.Z. Jia, and M.Z. Ma, Fabrication of Al/Al3Mg2 Composite by Vacuum Annealing and Accumulative Roll-Bonding Process, Mater. Sci. Eng. A, 2012, 558, p 510–516
R.J. Hebert and J.H. Perepezko, Deformation-Induced Synthesis and Structural Transformations of Metallic Multi Layers, Scr. Mater., 2004, 50, p 807–812
K.R. Gopi, H. Shivananda Nayaka, and S. Sahu, Investigation of Microstructure and Mechanical Properties of ECAP-Processed AM Series Magnesium Alloy, J. Mater. Eng. Perform., 2016, 25(9), p P3737–P3745
Y. Chino, K. Kimura, and M. Mabuchi, Twinning Behavior and Deformation Mechanisms of Extruded AZ31 Mg Alloy, Mater. Sci. Eng. A, 2008, 486, p 481–488
S.O. Gashti, A. Fattah-alhosseini, Y. Mazaheri, and M.K. Keshavarz, Microstructure, Mechanical Properties and Electrochemical Behavior of AA1050 Processed by Accumulative Roll Bonding (ARB), J. Alloys Compd., 2009, 474, p 406–415
K.D. Ralston and N. Birbilis, Effect of Grain Size on Corrosion, A Review, Corrosion, 2010, 66, p 075005–075013
A. Zarebidaki, H. Mahmoudikohani, and M.R. Aboutalebi, Microstructure and Corrosion Behavior of Electrodeposited Nano-Crystalline Nickel Coating on AZ91 Mg Alloy, J. Alloys Compd., 2014, 615, p 825–830
G.R. Argade, S.K. Panigrahi, and R.S. Mishra, Effects of Grain Size on the Corrosion Resistance of Wrought Magnesium Alloys Containing Neodymium, Corros. Sci., 2012, 58, p 145–151
N. Birbilis and Y. Estrin, Corrosion of Pure Mg as a Function of Grain Size and Processing Route, Adv. Eng. Mater., 2008, 10, p 579–582
P. Saha, M. Roy, M.K. Datta, B. Lee, and P.N. Kumta, Effects of Grain Refinement on the Bio Corrosion and In Vitro Bioactivity of Magnesium, Mater. Sci. Eng. C. Mater. Biol. Appl., 2015, 57, p 294–303
G. Song, A. Atrens, and M. Dargusch, Influence of Microstructure on the Corrosion of Diecast AZ91D, Corros. Sci., 1998, 41, p 249–273
A. Pardo, M.C. Merino, A.E. Coy, R. Arrabal, F. Viejo, and E. Matykina, Corrosion Behaviour of Magnesium/Aluminium Alloys in 3.5 wt.% NaCl, Corros. Sci., 2008, 50, p 823–834
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The authors gratefully appreciate the support of Department of Materials Engineering, Indian Institute of Science Bangalore, India; Advanced Center for Material Science, Indian Institute of Technology Kanpur, India; and Exclusive Magnesium Private limited, Hyderabad, India, providing various testing facility for research work.
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Anne, G., Ramesh, M.R., Shivananda Nayaka, H. et al. Microstructure Evolution and Mechanical and Corrosion Behavior of Accumulative Roll Bonded Mg-2%Zn/Al-7075 Multilayered Composite. J. of Materi Eng and Perform 26, 1726–1734 (2017). https://doi.org/10.1007/s11665-017-2576-z
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DOI: https://doi.org/10.1007/s11665-017-2576-z