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Lanthanide amides

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Organolanthoid Chemistry: Synthesis, Structure, Catalysis

Part of the book series: Topics in Current Chemistry ((TOPCURRCHEM,volume 179))

Abstract

The present review should be seen far beyond pure homage to organometallic lanthanide amide chemistry. The class which is settled between the alkyl and alkoxide counterparts has claimed its own importance within the family of organolanthanide compounds during the last ten years. Meanwhile compound design can fall back on an extensive reservoir of sterically and electronically tailored ligands. Of course, the “lanthanide dilemma” requires special emphasis on structural chemistry, although, encouraging applications should highlight this review. The thermal stability and kinetic lability of the Ln-N bond make this class of lanthanide compounds not only a valuable synthetic precursor. The article covers the literature until mid-1995 and seeks to uncover the current trends in this field.

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Abbreviations

A:

adduct ligand

ac:

acetonate

acac:

acetylacetonate

AIP:

2-phenylamino-4-phenylimino-2-pentene

bdsa:

bis(dimethylsilyl)amide

BiPy:

bipyridine

btsa:

bis(trimethylsilyl)amide

cbz:

carbazole

COT:

cyclooctatetraene

Cp:

η5-cyclopentadienyl

Cp*:

η5-pentamethylcyclopentadienyl

DAB:

1,4-diazabutadiene

H2-DAC:

4,13-diaza-18-crown-6

DME:

1,2-dimethoxyethane

dmp:

dimethylpyrrole

DMPE:

1,2-bis(dimethylphosphino)ethane

dmpz:

dimethylpyrazole

Im:

imidazole

L:

ligand

Ln:

lanthanide (Sc, Y, La, Ce-Lu)

Nc:

naphthalocyanine

OEP:

2,3,7,8,12,13,17,18-octa(ethyl)porphyrin

OEPG:

meso-octaethylporphyrinogen

p:

pyrrole

Pc:

phthalocyanine

pin:

2-phenylindole

Por:

porphyrin

Py:

pyridine

pz:

pyrazole

silox:

tri-tert-butyl siloxide

TCB:

1,2,4-trichlorobenzene

thd:

2,2,6,6-tetramethyl-3,5-heptanedionate

THF:

tetrahydrofurane

TPP:

meso-tetra(phenyl)porphyrin

tritox:

tri-tert-butyl methoxide

trop:

tropolonate

TTP:

meso-tetra(tolyl)porphyrin

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    Reiner Anwander

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Anwander, R. (1996). Lanthanide amides. In: Organolanthoid Chemistry: Synthesis, Structure, Catalysis. Topics in Current Chemistry, vol 179. Springer, Berlin, Heidelberg. https://doi.org/10.1007/BFb0015595

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