Abstract
Sulfide-based solid electrolytes were conventionally prepared by solid-state reaction methods since long time ago and the introduction of liquid phase synthesis which employing organic solvents as reaction media was just reported recently in 2012 and 2013 [1, 2]. The first two papers described the synthesis of β-Li3PS4 using tetrahydrofuran (THF) and thio-LISICON Li3.25Ge0.25P0.75S4 using hydrazine as mediated solvents. The preparation of Li3PS4 using THF underwent the suspension process whilst hydrazine dissolved all the raw materials and product of the reaction which resulted in a solution process. In this section, we will focus on the synthesis of some typical sulfide-based solid electrolytes using suspension process.
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Nguyen, H.H.P., Matsuda, A. (2021). Suspension Process. In: Kanamura, K. (eds) Next Generation Batteries. Springer, Singapore. https://doi.org/10.1007/978-981-33-6668-8_6
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DOI: https://doi.org/10.1007/978-981-33-6668-8_6
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