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Study of the Internal Structure of Isotropic Pyrolytic Graphite by Broadband Ultrasonic Spectroscopy

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Durability of Critical Infrastructure, Monitoring and Testing

Abstract

As material for structural components, isotropic pyrolytic graphite (IPG) is widely used in such objects of critical infrastructure as nuclear fission reactors. There is the possibility of using IPG as a facing material for experimental thermonuclear facilities; this is currently being explored. Also, IPG is used as a sealing and anti-friction material in the aerospace industry. It is shown that X-ray tomography is not very suitable for studying the internal structure of IPG produced by chemical vapor deposition because its density is much the same as that of heterogeneities encountered in IPG, such as carbon black inclusions and anisotropic pyrographite crystallites. Broadband ultrasonic spectroscopy has been used to detect pores and carbon deposited layers in IPG samples, 2D images of the internal structure produced.

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References

  1. Pierson, H.O.: Handbook of Carbon, Graphite, Diamond and Fullerenes. Noyes Publication, Park Ridge (1993)

    Google Scholar 

  2. Choe, J., Lim, J.W., Kim, M., Kim, J., Lee, D.G.: Durability of graphite coated carbon composite bipolar plates for vanadium redox flow batteries. Compos. Struct. 134, 106–113 (2015)

    Article  Google Scholar 

  3. Pageot, J., Rouzaud, J.N., Ahmad, M.A., Deldicque, D., Gadiou, R., Dentzer, J., et al.: Milled graphite as a pertinent analogue of French UNGG reactor graphite waste for a CO2 gasification-based treatment. Carbon 86, 174–187 (2015)

    Article  Google Scholar 

  4. Leiro, J.A., Heinonen, M.H., Laiho, T., Batirev, I.G.: Core-level XPS spectra of fullerene, highly oriented pyrolitic graphite, and glassy carbon. J. Electr. Spectrosc. Relat. Phenom. 128, 205–213 (2003)

    Article  Google Scholar 

  5. Maslova, O.A., Ammar, M.-R., Guimbretiere, G., Rouzaud, J.-N., Simon, P.: Determination of crystallite size in polished graphitized carbon by Raman spectroscopy. Phys. Rev. B 86, 134205 (2012)

    Article  Google Scholar 

  6. Salver-Disma, F., Tarascon, J.-M., Clinard, C., Rouzaud, J.-N.: Transmission electron microscopy studies on carbon materials prepared by mechanical milling. Carbon 37, 1941–1959 (1999)

    Article  Google Scholar 

  7. Wirth, R.: Focused ion beam (FIB) combined with SEM and TEM: advanced analytical tools for studies of chemical composition, microstructure and crystal structure in geomaterials on a nanometer scale, Chem. Geol. 261 (2009) 217. Chem. Geol. 261, 217229 (2009)

    Article  Google Scholar 

  8. Le Guillou, M., Rouzaud, J.N., Deldicque, D., Toulhoat, N., Pipon, Y., Moncoffre, N.: Structural and nanostructural behavior of deuterium implanted Highly Ordered Pyrolytic Graphite investigated by combined High Resolution Transmission Electron Microscopy Scanning Electron Microscopy and Raman microspectrometry. Carbon 94, 277–284 (2015)

    Article  Google Scholar 

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Acknowledgments

This work was carried out with financial support from the Ministry of Education and Science of the Russian Federation in the framework of the Increase Competitiveness Program of NUST ‘MISiS’ (no. K1-2015-025).

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Correspondence to Anton S. Bychkov .

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Bychkov, A.S. et al. (2017). Study of the Internal Structure of Isotropic Pyrolytic Graphite by Broadband Ultrasonic Spectroscopy. In: Kravcov, A., Cherepetskaya, E., Pospichal, V. (eds) Durability of Critical Infrastructure, Monitoring and Testing. Lecture Notes in Mechanical Engineering. Springer, Singapore. https://doi.org/10.1007/978-981-10-3247-9_1

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  • DOI: https://doi.org/10.1007/978-981-10-3247-9_1

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