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On-Site Sample Work-Up Procedures to Isolate Chemical Warfare Related Compounds using Solid Phase Extraction and Solid Phase Microextraction Technology

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Analytical Chemistry Associated with the Destruction of Chemical Weapons

Part of the book series: NATO ASI Series ((ASDT,volume 13))

Abstract

The rapid preparation and accurate analysis in the field of suspect samples is most important for on-site investigations relevant to the planned Chemical Weapons Convention (CWC) inspections. Sample preparation becomes the limiting factor and one of the most critical aspects of the challenge inspection. The primary aim of the analysis is to detect the presence of undeclared chemicals subject to control by the Convention.

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References

  1. Alcaraz, A., Hulsey, S.S., Haas, J.S., Riley, M.O., and Andresen, B.D., (September 1994) “The Development of Solid Phase Extraction Methods for CW On-Site Sample Preparation In Support of the Cooperative On-Site Analysis Exercise (COSAX) Project”, Report UCRL-ID-119316.

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  2. K.D. Buchholz and J. Pawlisyn, (1994) “Solid Phase MicroExtraction”, Anal. Chem., 66, pp l60–167.

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  3. Alcaraz, A., Hulsey, S.S., and Andresen, B.D., (1995) “A Rapid Screening Procedure for the Analysis of Proliferation Compounds in Complex Matrices Using Solid Phase MicroExtraction (SPME) and SPME with In-Situ Derivatization”, 43rd ASMS Conference on Mass Spectrometry and Allied Topics, Atlanta GA, p. 192.

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© 1997 Springer Science+Business Media Dordrecht

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Alcaraz, A., Hulsey, S.S., Whipple, R.E., Andresen, B.D. (1997). On-Site Sample Work-Up Procedures to Isolate Chemical Warfare Related Compounds using Solid Phase Extraction and Solid Phase Microextraction Technology. In: Heyl, M., McGuire, R. (eds) Analytical Chemistry Associated with the Destruction of Chemical Weapons. NATO ASI Series, vol 13. Springer, Dordrecht. https://doi.org/10.1007/978-94-011-5600-4_6

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  • DOI: https://doi.org/10.1007/978-94-011-5600-4_6

  • Publisher Name: Springer, Dordrecht

  • Print ISBN: 978-94-010-6362-3

  • Online ISBN: 978-94-011-5600-4

  • eBook Packages: Springer Book Archive

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