Skip to main content

Analysis of the Microstructure; Analysis of Lattice Imperfections: Light and Electron Microscopical and X-Ray Diffraction Methods

  • Chapter
  • First Online:
Fundamentals of Materials Science
  • 9193 Accesses

Abstract

Materials are substances that have now, or are expected to find in a not too distant future, practical use (see Chap. 1). The microstructure of a material (beautifully described by the untranslatable German word “Gefüge”) is a notion that comprises all aspects of the atomic arrangement in a material that should be known in order to understand its properties. Mostly we are concerned with crystalline materials. The conception microstructure then narrows to the description of the so-called crystal imperfection (cf. Chap. 5).

This is a preview of subscription content, log in via an institution to check access.

Access this chapter

Institutional subscriptions

Preview

Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.

References

General

  • Amelinckx S, Van Dyck D, Van Landuyt J, Van Tendeloo G (1997) Handbook of microscopy, vol. 1–3. VCH Verlagsgesellschaft, Weinheim, Germany

    Google Scholar 

  • de Graef M (2003) Introduction to convential transmission electron microscopy. Cambridge University Press, Cambridge

    Book  Google Scholar 

  • Mittemeijer EJ, Scardi P (eds) (2004) Diffraction analysis of the microstructure of materials. Springer Series in Materials Science, vol. 68. Springer, Berlin, Heidelberg, New York

    Google Scholar 

  • Warren BE (1969) X-ray diffraction. Addison-Wesley, Reading, MA

    Google Scholar 

  • Williams DB, Carter CB (1996) Transmission electron microscopy, vols. I–IV. Plenum Press, New York

    Google Scholar 

Specific

  • van Berkum JGM, Delhez R, de Keijser ThH, Mittemeijer EJ (1996) Diffraction-line broadening due to strain fields in materials. Acta Crystallographica A52:730–747

    Google Scholar 

  • Delhez R, de Keijser ThH, Mittemeijer EJ (1982) Determination of crystallite size and lattice distortions through X-ray diffraction line profile analysis. Recipes, methods and comments. Fresenius Zeitschrift für Analytische Chemie 312:1–16

    Article  CAS  Google Scholar 

  • Drent P (2005) Properties and selection of objective lenses for light microscopical applications. Microscopy Anal 19:5–7

    Google Scholar 

  • Hauk V (ed) (1997) Structural and residual stress analysis by nondestructive methods; evaluation-application-assessment. Elsevier, Amsterdam

    Google Scholar 

  • Horn E, Zantl R (2006) Phase-contrast light microscopy of living cells cultured in small volumes. Microscopy Anal 20:15–17

    Google Scholar 

  • Kumar A, Welzel U, Mittemeijer EJ (2006) Depth dependence of elastic grain interaction and mechanical stress: analysis by X-ray diffraction measurements at fixed penetration/information depths. J Appl Phys 100:114904

    Article  Google Scholar 

  • Mittemeijer EJ, Welzel U (2008) The “state of the art” of the diffraction analysis of crystallite size and lattice strain. Zeitschrift für Kristallographie 223:552–560

    Article  CAS  Google Scholar 

  • Noyan IC, Cohen JB (1978) Residual stress; measurement by diffraction and interpretation. Springer, New York

    Google Scholar 

  • Sato A, Mori N, Takakura M, Notoya S (2007) Examination of analytical conditions for trace elements based on the detection limit of EPMA (WDS). JEOL News 42E:46–52

    Google Scholar 

  • Urban KW (2007) The new paradigm of transmission electron microscopy. MRS Bull 32:946–952

    Article  CAS  Google Scholar 

  • Welzel U, Ligot J, Lamparter P, Vermeulen AC, Mittemeijer EJ (2005) Stress analysis of polycrystalline thin films and surface regions by X-ray diffraction (Review). J Appl Crystallography 38:1–29

    Article  Google Scholar 

  • Williamson GK, Smallman RE (1956) Dislocation densities in some annealed and cold-worked metals from measurements on the X-ray Debye-Scherrer spectrum. Philos Mag 1:34–46

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Eric J. Mittemeijer .

Rights and permissions

Reprints and permissions

Copyright information

© 2010 Springer-Verlag Berlin Heidelberg

About this chapter

Cite this chapter

Mittemeijer, E.J. (2010). Analysis of the Microstructure; Analysis of Lattice Imperfections: Light and Electron Microscopical and X-Ray Diffraction Methods. In: Fundamentals of Materials Science. Springer, Berlin, Heidelberg. https://doi.org/10.1007/978-3-642-10500-5_6

Download citation

Publish with us

Policies and ethics