Abstract
Propagation based X-ray phase contrast imaging (PCI) offers unique opportunities for ultrafast, high-resolution measurements to examine dynamic materials response at extreme conditions. Within the past decade, efforts on the IMPULSE system at the Advanced Photon Source included the development of a novel Multi-frame X-ray PCI (MPCI) system that was used to obtain the first shock-movies to examine material deformation with micron spatial resolution on nanosecond timescale. The MPCI system has been systematically developed over the years to improve optical efficiencies, spatial resolution, obtain more images per experiment, and to develop a dual-imaging, dual-zoom feature useful for many applications. With the MPCI system, X-ray PCI has been successfully used to study a wide range of phenomena including jet-formation in metals, crack nucleation and propagation, response of additively manufactured materials, and detonator dynamics to name a few. In this paper, a brief overview of the MPCI system development is provided along with its application to study shock propagation in materials.
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References
Asay, J.R., Fowles, G.R., Duvall, D.E., Miles, M.H., Tinder, R.F.: Effects of point defects on elastic precursor decay in LiF. J. Appl. Phys. 43, 2132 (1972)
Dolan, D.H., Johnson, J.N., Gupta, Y.M.: Nanonsecond freezing of water under multiple shock wave compression: continuum modeling and wave profile measurements. J. Chem. Phys. 123, 064702 (2005)
Jensen, B.J., Gray, G.T., Hixson, R.S.: Direct measurement of the α-ε transition stress and kinetics for shocked iron. J. Appl. Phys. 105, 013502 (2009)
Jensen, B.J., Cherne, F.J.: Dynamic compression of cerium in the low-pressure γ-α region of the phase diagram. J. Appl. Phys. 112, 013515 (2012)
Jensen, B.J., Gupta, Y.M.: Time-resolved x-ray diffraction experiments to examine the elastic-plastic transition in shocked magnesium-doped LiF. J. Appl. Phys. 104, 013510 (2008)
Jensen, B.J., Gupta, Y.M.: X-ray diffraction measurements in shock compressed magnesium doped LiF crystals. J. Appl. Phys. 100(5), 053512 (2006)
Kalantar, D.H., Belak, J.F., Collins, G.W., Colvin, J.D., Davies, H.M., et al.: Direct observation of the $\alpha-\epsilon$ transition in shock-compressed iron via nanosecond X-ray diffraction. Phys. Rev. Lett. 95, 075502 (2005)
Jensen, B.J., Lou, S.N., Hooks, D.E., Fezzaa, K., Ramos, K.J., Yeager, J.D., Kwiatkowski, K., Shimada, T., Dattelbaum, D.M.: Ultrafast, high resolution, phase contrast imaging of impact response with synchrotron radiation. AIP Adv. 2(1), 012170–012176 (2012)
Luo, S.N., Jensen, B.J., Hooks, D.E., Fezzaa, K., Ramos, K.J., Yeager, J.D., Kwiatkowski, K., Shimada, T.: Gas gun shock experiments with single-pulse x-ray phase contrast imaging and diffraction at the advanced photon source. Rev. Sci. Instrum. 83(7), 073903 (2012)
Jensen, B.J., Owens, C.T., Ramos, K.J., Yeager, J.D., Saavedra, R.A., Iverson, A.J., Luo, S.N., Fezzaa, K.: Hooks DE impact system for ultrafast synchrotron experiments. Rev. Sci. Instrum. 84(1), 013904–013905 (2013)
Gupta, Y.M., Turneaure, S.J., Perkins, K., Zimmerman, K., Arganbright, N., Shen, G., Chow, P.: Real-time, high-resolution x-ray diffraction measurements on shocked crystals at a synchrotron facility. Rev. Sci. Instrum. 83(12), 123905 (2012)
Montgomery, D.S., Nobile, A., Walsh, P.J.: Characterization of National Ignitition Facility cryogenic beryllium capsules using x-ray phase contrast imaging. Rev. Sci. Instrum. 75, 3986–3988 (2004)
Yeager, J.D., Luo, S.N., Jensen, B.J., Fezzaa, K., Montgomery, D.S., Hooks, D.E.: High-speed synchrotron X-ray phase contrast imaging for analysis of low-Z composite microstructure. Compos. A: Appl. Sci. Manuf. 43(6), 885–892 (2013). https://doi.org/10.1016/j.compositesa.2012.01.013
Ramos, K.J., Jensen, B.J., Yeager, J.D., Bolme, C.A., Iverson, A.J., Carlson, C.A., Fezzaa, K.: Investigation of dynamic material cracking with in situ synchrotron-based measurements. In: Song, B., Casem, D., Kimberley, J. (eds.) Dynamic Behavior of Materials, vol. 1, pp. 413–420. Springer International Publishing, Dordrecht (2014). ISBN 978–3–319-00770-0
Jensen, B.J., Cherne, F.J., Ramos, K.J., Iverson, A.J., Carlson, C.A., Yeager, J.D., Fezzaa, K., Dimonte, G., Hooks, D.E.: Multiphase material strength determined through shock generated Richtmyer-Meshkov instabilities. J. Appl. Phys. 118, 195903 (2015)
Brown, E.N., Ramos, K.J., Dattelbaum, D.M., Jensen, B.J., Gray III, G.T., Matterson, B.M., Trujillo, C.P., Martinez, D.T., Pierce, T.H., Iverson, A.J., Carlson, C.A., Fezzaa, K., Furmanski, J.: In situ and postmortem measures of damage in polymers at high strain-rate. Conference Proceedings of the Society for Experimental Mechanics Series. 65(1), 53–59 (2015)
Brown, E.N., Furmanski, J., Ramos, K.J., Dattelbaum, D.M., Jensen, B.J., Iverson, A.J., Carlson, C.A., Fezzaa, K., Trujillo, C.P., Martinez, D.T., Gray III, G.T., Patterson, B.M.: High-density polyethylene damage at extreme tensile conditions. J. Phys. Conf. Ser. 500, 112011 (2014)
Hawreliak, J., Lind, J., Maddox, B., Barham, M., Messner, M., Barton, N., Jensen, B.J., Kumar, M.: Dynamic behavior of engineered lattice materials. Nature Scientific Reports. 6, 28094 (2016)
Branch, B., Ionita, A., Clements, B., Montgomery, D., Jensen, B.J., Patterson, B., Mueller, A., Dattelbaum, D.M.: Controlling shockwave dynamics using architecture in periodic porous materials. J. Appl. Phys. 121, 135102 (2017)
Willey, T.M., Champley, K., Hodgin, R., Lauderbach, L., Bagge-Hansen, M., May, C., Sanchez, N.J., Jensen, B.J., Iverson, A.J., Van Buuren, T.: X-ray Imaging and 3D Reconstruction of In-Flight Exploding Foil Initiator Flyers. J. Appl. Phys. 119, 235901 (2016)
Sanchez, N.J., Neal, W.E., Jensen, B.J., Iverson, A.J., Carlson, C.A.: Dynamic Exploding Foil Initiator Imaging at the Advanced Photon Source. AIP Conf. Proc. 1979(160023), (2018)
Neal, W.E., Sanchez, N., Jensen, B.J., Gibson, J., Martinez, M., et al.: The effect of surface heterogeneity in exploding metal foils. AIP Conf. Proc. 1979(180007), (2018)
Mandal, A., Jensen, B.J., Aslam, T.D., Iverson, A.J.: Dynamic Compaction of Nickel Powder Examined by X-ray phase contrast imaging. AIP Conf. Proc. 1979(110010), (2018)
Ramos, K.J., Jensen, B.J., Hooks, D.E., Fezzaa, K., Yeager, J.D., Iverson, A.J., Carlson, C.A., Cherne, F.J.: In situ investigation of the dynamic response of energetic materials using IMPULSE at the advanced photon source. J. Phys. Conf. Ser. 500, 142028 (2014)
Jensen, B.J., Hooks, D.E., Fezzaa, K., Ramos, K.J., Yeager, J.D., Iverson, A.J., Carlson, C.A., Cherne, F.J., Kwiatkowski, K.: Dynamic experiments using IMPULSE at the advanced photon source. J. Phys. Conf. Ser. 500, 042001 (2014)
Jensen, B.J., Montgomery, D.S., Iverson, A.J., Carlson, C.A., Clements, B., Short, M., Fredenburg, D.A.: X-ray phase contrast imaging of granular systems. LA-UR-17-27104 Los Alamos Laboratory Report (2017)
Branch, B., Jensen, B.J.: Dynamic X-ray diffraction to study the shock-induced a-e phase transition in iron. AIP Conf. Proc. 1979(040001), (2018)
Jensen, B.J., Holtkamp, D.B., Rigg, P.A., Dolan, D.H.: Accuracy limits and window corrections for Photon Doppler velocimetry. J. Appl. Phys. 101, 013523 (2007)
LASL SHOCK HUGONIOT DATA (University of California Press, Berkley and Los Angeles, CA, 1980)
Carter WJ, Marsh SP. Hugoniot Equation of State of Polymers. LA-12006-MS Los Alamos National Laboratory (1995)
Millett, J.C.F., Bourne, N.K.: Shock and release of polycarbonate under one-dimensional strain. J. Mater. Sci. 41, 1683–1690 (2006)
Acknowledgements
This work was performed by Los Alamos National Laboratory (LANL) at Los Alamos and at the Dynamic Compression Sector (DCS) at the Advanced Photon Source (APS). All x-ray phase contrast images shown here were obtained using LANL’s multi-frame x-ray phase contrast imaging system (MPCI) developed on the IMPULSE capability at APS. Chuck Owens, Joe Rivera, and John Wright (LANL) are thanked for sample assembly, experiment preparation and execution. Nick Sinclair and Adam Schuman (DCS/WSU) are thanked for their technical support at the Sector 35 beamline setting up the X-ray beam. The authors gratefully acknowledge the financial support provided by Science Campaigns, Joint Munitions Program (JMP), and National Security Technologies (NSTec) Shock Wave Physics Related Diagnostic (SWRD) program. LANL is operated by Los Alamos National Security, LLC for the U.S. Department of Energy (DOE) under Contract No. DE-AC52-06NA25396. DCS is supported by the Department of Energy (DOE), National Nuclear Security Administration, under Award Number DE-NA0002442 and operated by Washington State University (WSU). This research used resources of APS, a U.S. Department of Energy (DOE) Office of Science User Facility operated for the DOE Office of Science by Argonne National Laboratory under Contract No. DE-AC02-06CH11357.
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Jensen, B.J. et al. (2019). Examining Material Response Using X-Ray Phase Contrast Imaging. In: Kimberley, J., Lamberson, L., Mates, S. (eds) Dynamic Behavior of Materials, Volume 1. Conference Proceedings of the Society for Experimental Mechanics Series. Springer, Cham. https://doi.org/10.1007/978-3-319-95089-1_14
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