Abstract
Some of the earliest X-ray Photoemission Spectroscopy (XPS) studies with high-energy X-rays took place in the 1970s as a way of demonstrating the feasibility of using synchrotron radiation from a multi-GeV storage ring to study materials. These developments took place at the SPEAR storage ring at the Stanford Linear Accelerator Center and showed that synchrotron radiation could be tamed but that the technologies of the time would not allow hard X-ray photoemission to become a tool for routine experiments. However, soft X-rays did fulfill that promise and dominated the XPS research for the next several decades with important contributions to the study of surfaces and interfaces . With the advent of second and particularly third generation synchrotron sources, XPS with high-energy X-rays has become a practical tool for the study of bulk properties and buried interfaces. The development of these techniques will be discussed as will the need for both hard and soft X-rays to provide complimentary details on bulk and surface properties of materials.
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Acknowledgements
The authors acknowledge the support of the Stanford Synchrotron Radiation Lightsource, SLAC National Accelerator Laboratory, which is supported by the U.S. Department of Energy, Office of Science, Office of Basic Energy Sciences under Contract No. DE-AC02-76SF00515. The authors are grateful to Tien-Lin Lee of the Diamond Lightsource for providing the description and results from BL I09 at the Diamond Lightsource.
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Pianetta, P., Lindau, I. (2016). HAXPES at the Dawn of the Synchrotron Radiation Age. In: Woicik, J. (eds) Hard X-ray Photoelectron Spectroscopy (HAXPES). Springer Series in Surface Sciences, vol 59. Springer, Cham. https://doi.org/10.1007/978-3-319-24043-5_3
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