Skip to main content
SpringerLink
Log in

Experimental Design and Optimization

  • Chapter
  • First Online:
Chemometrics in Electroanalysis

Part of the book series: Monographs in Electrochemistry ((MOEC))

Abstract

Some typical strategies of experimental design are reviewed and their applications to electroanalytical studies are illustrated with examples from the literature. The experimental designs considered are mainly based on the concepts of response surface and factorial design and are essentially applied for screening, optimization and calibration purposes.

This is a preview of subscription content, log in via an institution to check access.

Access this chapter

Log in via an institution
Chapter
USD 29.95
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
eBook
USD 119.00
Price excludes VAT (USA)
  • Available as EPUB and PDF
  • Read on any device
  • Instant download
  • Own it forever
Softcover Book
USD 159.99
Price excludes VAT (USA)
  • Compact, lightweight edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info
Hardcover Book
USD 159.99
Price excludes VAT (USA)
  • Durable hardcover edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info

Tax calculation will be finalised at checkout

Purchases are for personal use only

Institutional subscriptions

References

  1. Esbensen KH, Guyot D, Westad F (2000) Multivariate data analysis in practice: an introduction to multivariate data analysis and experimental design, 4th edn. Camo, Oslo

    Google Scholar 

  2. Brown SD, Tauler R, Walczak B (eds) (2009) Comprehensive chemometrics: chemical and biochemical data analysis. Elsevier, Amsterdam

    Google Scholar 

  3. Montgomery DC (2005) Design and analysis of experiments, 6th edn. Wiley, Hoboken, NJ

    Google Scholar 

  4. Hanrahan G, Lu K (2006) Crit Rev Anal Chem 36:141

    Article  CAS  Google Scholar 

  5. Leardi R (2009) Anal Chim Acta 652:161

    Article  CAS  Google Scholar 

  6. Candioti LV, De Zan MM, Cámara MS, Goicoechea HC (2014) Talanta 124:123

    Article  Google Scholar 

  7. Tarley CRT, Silveira G, dos Santos WNL, Matos GD, da Silva EGP, Bezerra MA, Miró M, Ferreira SLC (2009) Microchem J 92:58

    Article  CAS  Google Scholar 

  8. Box GEP, Wilson KB (1951) J R Stat Soc B13:1

    Google Scholar 

  9. Box GEP, Draper NR (1987) Empirical model-building and response surfaces, vol 424. Wiley, New York

    Google Scholar 

  10. Plackett RL, Burman JP (1946) Biometrika 33:305

    Article  Google Scholar 

  11. Vanaja K, Shobha Rani RH (2007) Clin Res Regul Aff 24:1

    Article  Google Scholar 

  12. Nguyen NK, Miller AJ (1992) Comput Stat Data Anal 14:489

    Article  Google Scholar 

  13. de Aguiar PF, Bourguignon B, Khots MS, Massart DL, Phan-Than-Luu R (1995) Chemom Intell Lab Syst 30:199

    Article  CAS  Google Scholar 

  14. Ferreira SL, Dos Santos WN, Quintella CM, Neto BB, Bosque-Sendra JM (2004) Talanta 63:1061

    Article  CAS  Google Scholar 

  15. dos Santos-Depoi F, Bentlin FR, Ferrao MF, Pozebon D (2012) Anal Methods 4:2809

    Article  Google Scholar 

  16. Duarte MMMB, Neto GO, Kubota LT, Filho JLL, Pimentel MF, Lima F, Lins V (1997) Anal Chim Acta 350:353

    Article  CAS  Google Scholar 

  17. Akhmetshin A, Baranovsky V, Akhmetshina A (1998) Fresenius’ J Anal Chem 361:282

    Article  CAS  Google Scholar 

  18. Dabrowska S, Migdalski J, Lewenstam A (2017) Electroanalysis 29:140

    Article  CAS  Google Scholar 

  19. Furlanetto S, Gratteri P, Pinzauti S, Leardi R, Dreassi E, Santoni G (1995) J Pharmaceut Biomed Anal 13:431

    Article  CAS  Google Scholar 

  20. Pinzauti S, Gratteri P, Furlanetto S, Mura P, Dreassi E, Phan-Tan-Luu R (1996) J Pharm Biomed Anal 14:881

    Article  CAS  Google Scholar 

  21. Domínguez O, Sanllorente S, Arcos MJ (1999) Electroanalysis 11:1273

    Article  Google Scholar 

  22. Alonso-Lomillo MA, Domínguez-Renedo O, Arcos-Martínez MJ (2002) Helv Chim Acta 85:2430

    Article  Google Scholar 

  23. Teófilo RF, Reis EL, Reis C, Silva GAD, Kubota LT (2004) J Braz Chem Soc 15:865

    Article  Google Scholar 

  24. Muñoz E, Palmero S (2004) Food Control 15:635

    Article  Google Scholar 

  25. Muñoz E, Palmero S (2004) Electroanalysis 16:1528

    Article  Google Scholar 

  26. Tarley CRT, Kubota LT (2005) Anal Chim Acta 548:11

    Article  CAS  Google Scholar 

  27. Giberteau-Cabanillas A, Rodríguez-Cáceres MI, Martínez-Cañas MA, Ortiz-Burguillos JM, Galeano-Diaz T (2007) Talanta 72:932

    Article  Google Scholar 

  28. Domínguez-Renedo O, Calvo M, Arcos-Martínez MJ (2008) Sensors 8:4201

    Article  Google Scholar 

  29. Pinto L, Lemos SG (2013) Microchem J 110:417

    Article  CAS  Google Scholar 

  30. Bia G, Borgnino L, Ortiz PI, Pfaffen V (2014) Sens Actuat B-Chem 203:396

    Article  CAS  Google Scholar 

  31. Lima T, Silva HTD, Labuto G, Simões FR, Codognoto L (2016) Electroanalysis 28:817

    Article  CAS  Google Scholar 

  32. Cuéllar M, Pfaffen V, Ortiz PI (2016) J Electroanal Chem 765:37

    Article  Google Scholar 

  33. Patris S, Vandeput M, Kenfack GM, Mertens D, Dejaegher B, Kauffmann JM (2016) Biosens Bioelec 77:457

    Article  CAS  Google Scholar 

  34. Zhao G, Wang H, Liu G, Wang Z (2016) Sens Actuat B-Chem 235:67

    Article  CAS  Google Scholar 

  35. Terzi F, Zanfrognini B, Dossi N, Ruggeri S, Maccaferri G (2016) Electrochim Acta 188:327

    Article  CAS  Google Scholar 

  36. del Torno-de Román L, Alonso-Lomillo MA, Domínguez-Renedo O, Arcos-Martínez MJ (2016) Sens Actuat B-Chem 227:48

    Article  Google Scholar 

  37. Krepper G, Pierini GD, Pistonesi MF, Di Nezio MS (2017) Sens Actuat B-Chem 241:560

    Article  CAS  Google Scholar 

  38. Zhang H, Lunsford SK, Marawi I, Rubinson JF, Mark HB (1997) J Electroanal Chem 424:101

    Article  CAS  Google Scholar 

  39. Hoffmann AA, Dias SL, Benvenutti EV, Lima EC, Pavan FA, Rodrigues JR, Scotti R, Ribeiro ES, Gushikem Y (2007) J Braz Chem Soc 18:1462

    Article  CAS  Google Scholar 

  40. Uliana CV, Tognolli JO, Yamanaka H (2011) Electroanalysis 23:2607

    Article  CAS  Google Scholar 

  41. Shahrokhian S, Kamalzadeh Z, Hamzehloei A (2013) Bioelectrochemistry 90:36

    Article  CAS  Google Scholar 

  42. Zhang Y, Qi M, Liu G (2015) Electroanalysis 27:1110

    Article  CAS  Google Scholar 

  43. Nosuhi M, Nezamzadeh-Ejhieh A (2017) Electrochim Acta 223:47

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Faculty of Chemistry, University of Barcelona, Barcelona, Spain

    José Manuel Díaz-Cruz, Miquel Esteban & Cristina Ariño

Authors
  1. José Manuel Díaz-Cruz
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. Miquel Esteban
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. Cristina Ariño
    View author publications

    You can also search for this author in PubMed Google Scholar

Rights and permissions

Reprints and permissions

Copyright information

© 2019 Springer Nature Switzerland AG

About this chapter

Check for updates. Verify currency and authenticity via CrossMark

Cite this chapter

Díaz-Cruz, J.M., Esteban, M., Ariño, C. (2019). Experimental Design and Optimization. In: Chemometrics in Electroanalysis. Monographs in Electrochemistry. Springer, Cham. https://doi.org/10.1007/978-3-030-21384-8_4

Download citation

Publish with us

Policies and ethics

Search

Navigation