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Change in the magnetic properties of nanoferrihydrite with an increase in the volume of nanoparticles during low-temperature annealing

  • Magnetism
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Abstract

The results of the investigation into the effect of low-temperature annealing of a powder of nanoparticles of bacterial ferrihydrite on its magnetic properties have been presented. It has been found that an increase in the time (up to 240 h) and temperature (in the range from 150 to 200°C) of annealing leads to a monotonic increase in the superparamagnetic blocking temperature, the coercive force, and the threshold field of the opening of the magnetic hysteresis loop (at liquid-helium temperatures), as well as to an increase in the magnetic resonance line width at low temperatures and in the magnetic susceptibility at room temperature. At the same time, according to the results of the analysis of the Mössbauer spectra, the annealing of ferrihydrite does not lead to the formation of new iron oxide phases. Most of these features are well consistent with the fact that the low-temperature annealing of ferrihydrite causes an increase in the size of nanoparticles, which is confirmed by the results of transmission electron microscopy studies.

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References

  1. S. Mørup, D. E. Madsen, C. Fradsen, C. R. H. Bahl, and M. F. Hansen, J. Phys.: Condens. Matter. 19, 213202 (2007).

    ADS  Google Scholar 

  2. Yu. L. Raikher and V. I. Stepanov, J. Exp. Theor. Phys. 107 (3), 435 (2008).

    Article  ADS  Google Scholar 

  3. Q. A. Pankhurst, N. T. K. Thanh, S. K. Jones, and J. Dobson, J. Phys. D: Appl. Phys. 42, 224001 (2009).

    Article  ADS  Google Scholar 

  4. K. Dobretsov, S. Stolyar, and A. Lopatin, Acta Otorhinolaryngol. Ital. 35 (2), 97 (2015).

    Google Scholar 

  5. S. A. Makhlouf, F. T. Parker, and A. E. Berkowitz, Phys. Rev. B: Condens. Matter 55 (22), R14717 (1997).

    Article  ADS  Google Scholar 

  6. M. S. Seehra, V. S. Babu, A. Manivannan, and J. W. Lynn, Phys. Rev. B: Condens. Matter 61 (5), 3513 (2000).

    Article  ADS  Google Scholar 

  7. M. S. Seehra and A. Punnoose, Phys. Rev. B: Condens. Matter 64 (13), 132410 (2001).

    Article  ADS  Google Scholar 

  8. A. Punnoose, T. Phanthavady, M. S. Seehra, N. Shah, and G. P. Huffman, Phys. Rev. B: Condens. Matter 69 (8), 054425 (2004).

    Article  ADS  Google Scholar 

  9. E. L. Duarte, R. Itri, E. Lima, M. S Baptista, T. S. Berquó, and G. F. Goya, Nanotechnology 17, 5549 (2006).

    Article  ADS  Google Scholar 

  10. T. S. Berquó, J. J. Erbs, A. Lindquist, R. L. Penn, and S. K. Banerjee, J. Phys.: Condens. Matter 21, 176005 (2009).

    ADS  Google Scholar 

  11. N. J. O. Silva, V. S. Amaral, A. Urtizberea, R. Bustamante, A. Millán, F. Palacio, E. Kampert, U. Zeitler, S. de Brion, Ó. Iglesias, and A. Labarta, Phys. Rev. B: Condens. Matter 84 (10), 104427 (2011).

    Article  ADS  Google Scholar 

  12. J. G. E. Harris, J. E. Grimaldi, D. D. Awschalom, A. Chiolero, and D. Loss, Phys. Rev. B: Condens. Matter 60 (5), 3453 (1999).

    Article  ADS  Google Scholar 

  13. C. Gilles, P. Bonville, H. Rakoto, J. M. Broto, K. K. W. Wong, and S. Mann, J. Magn. Magn. Mater. 241, 430 (2002).

    Article  ADS  Google Scholar 

  14. N. J. O. Silva, V. S. Amaral, and L. D. Carlos, Phys. Rev. B: Condens. Matter 71 (18), 184408 (2005).

    Article  ADS  Google Scholar 

  15. N. J. O. Silva, A. Millán, F. Palacio, E. Kampert, U. Zeitler, H. Rakoto, and V. S. Amaral, Phys. Rev. B: Condens. Matter 79 (10), 104405 (2009).

    Article  ADS  Google Scholar 

  16. R. P. Guertin, N. Harrison, Z. X. Zhou, S. McCall, and F. Drymiotis. J. Magn. Magn. Mater. 308, 97 (2007).

  17. D. A. Balaev, A. A. Krasikov, A. A. Dubrovskiy, S. V. Semenov, S. I. Popkov, S. V. Stolyar, R. S. Iskhakov, V. P. Ladygina, and P. H. Yaroslavtsev, Phys. Solid State 58 (2), 287 (2016).

    Article  ADS  Google Scholar 

  18. D. A. Balaev, A. A. Dubrovskii, A. A. Krasikov, S. V. Stolyar, R. S. Iskhakov, V. P. Ladygina, and E. D. Khilazheva, JETP Lett. 98 (3), 139 (2013).

  19. D. A. Balaev, A. A. Krasikov, A. A. Dubrovskii, S. V. Semenov, O. A. Bayukov, S. V. Stolyar, R. S. Iskhakov, V. P. Ladygina, and L. A. Ishchenko, J. Exp. Theor. Phys. 119 (3), 479 (2014).

  20. D. A. Balaev, A. A. Krasikov, A. A. Dubrovskii, O. A. Bayukov, S. V. Stolyar, R. S. Iskhakov, V. P. Ladygina, and P. H. Yaroslavtsev, Tech Phys. Lett. 41 (7), 705 (2015).

    Article  ADS  Google Scholar 

  21. S. V. Stolyar, O. A. Bayukov, Yu. L. Gurevich, V. P. Ladygina, R. S. Iskhakov, and P. P. Pustoshilov, Inorg. Mater. 43 (6), 638 (2007).

    Article  Google Scholar 

  22. S. V. Stolyar, O. A. Bayukov, Yu. L. Gurevich, E. A.Denisova, R. S. Iskhakov, V. P. Ladygina, A. P. Puzyr’, P. P. Pustoshilov, and M. A. Bikhetina, Inorg. Mater. 42 (7), 763 (2006).

    Article  Google Scholar 

  23. Yu. L. Raikher, V. I. Stepanov, S. V. Stolyar, V. P. Ladygina, D. A. Balaev, L. A. Ishchenko, and M. Balasoiu, Phys. Solid State 52 (2), 298 (2010).

    Article  ADS  Google Scholar 

  24. A. D. Balaev, Yu. V. Boyarshinov, M. M. Karpenko, and B. P. Khrustalev, Prib. Tekh. Eksp., No. 3, 167 (1985).

    Google Scholar 

  25. M. Balasoiu, S. V. Stolyar, R. S. Iskhakov, L. A. Ischenko, Y. L. Raikher, A. I. Kuklin, O. L. Orelovich, Yu. S. Kovalev, and T. S. Kurkin, Rom. J. Phys. 55 (7–8), 782 (2010).

    Google Scholar 

  26. S. V. Stolyar, O. A. Bayukov, V. P. Ladygina, R. S. Iskhakov, L. A. Ishchenko, V. Yu. Yakovchuk, K. G. Dobretsov, A. I. Pozdnyakov, and O. E. Piksina, Phys. Solid State 53 (1), 100 (2011).

    Article  ADS  Google Scholar 

  27. D. Tobia, E. Winkler, R. D. Zysler, M. Granada, H. E. Troiani, and D. Fiorani, J. Appl. Phys. 106, 103920 (2009).

  28. J. C. Denardin, A. L. Brandl, M. Knobel, P. Panissod, A. B. Pakhomov, H. Liu, and X. X. Zhang, Phys. Rev. B: Condens. Matter 65 (6), 064422 (2002).

    Article  ADS  Google Scholar 

  29. E. C. Stoner and E. P. Wohlfarth, Philos. Trans. R. Soc. London, Ser. A 240, 599 (1948).

    Article  ADS  Google Scholar 

  30. S. V. Komogortsev, R. S. Iskhakov, A. D. Balaev, A. V.Okotrub, A. G. Kudashov, N. A. Momot, and S. I. Smirnov, Phys. Solid State 51 (11), 2286 (2009).

    Article  ADS  Google Scholar 

  31. L. Néel, C. R. Hebd. Seances Acad. Sci. 252, 4075 (1961).

  32. J. T. Richardson, D. I. Yiagas, B. Turk, K. Forster, and M. V. Twigg, J. Appl. Phys. 70, 6977 (1991).

    Article  ADS  Google Scholar 

Download references

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Authors and Affiliations

  1. Kirensky Institute of Physics, Siberian Branch of the Russian Academy of Sciences, Akademgorodok 50/38, Krasnoyarsk, 660036, Russia

    D. A. Balaev, A. A. Krasikov, S. V. Stolyar, R. S. Iskhakov, O. A. Bayukov, A. M. Vorotynov, M. N. Volochaev & A. A. Dubrovskiy

  2. Siberian Federal University, Svobodny pr. 79, Krasnoyarsk, 660041, Russia

    D. A. Balaev, A. A. Krasikov, S. V. Stolyar & R. N. Yaroslavtsev

  3. International Scientific Centre for Organism Extreme States Research, Presidium of the Krasnoyarsk Scientific Centre of the Siberian Branch of the Russian Academy of Sciences, Akademgorodok 50, Krasnoyarsk, 660036, Russia

    V. P. Ladygina

  4. International Laboratory of High Magnetic Fields and Low Temperatures, ul. Gajowicka 95, Wroclaw, 53-421, Poland

    A. A. Dubrovskiy

Authors
  1. D. A. Balaev
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  2. A. A. Krasikov
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  3. S. V. Stolyar
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  4. R. S. Iskhakov
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  5. V. P. Ladygina
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  6. R. N. Yaroslavtsev
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  7. O. A. Bayukov
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  8. A. M. Vorotynov
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  9. M. N. Volochaev
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  10. A. A. Dubrovskiy
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Correspondence to D. A. Balaev.

Additional information

Original Russian Text © D.A. Balaev, A.A. Krasikov, S.V. Stolyar, R.S. Iskhakov, V.P. Ladygina, R.N. Yaroslavtsev, O.A. Bayukov, A.M. Vorotynov, M.N. Volochaev, A.A. Dubrovskiy, 2016, published in Fizika Tverdogo Tela, 2016, Vol. 58, No. 9, pp. 1724–1732.

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Balaev, D.A., Krasikov, A.A., Stolyar, S.V. et al. Change in the magnetic properties of nanoferrihydrite with an increase in the volume of nanoparticles during low-temperature annealing. Phys. Solid State 58, 1782–1791 (2016). https://doi.org/10.1134/S1063783416090092

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  • DOI: https://doi.org/10.1134/S1063783416090092

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