Skip to main content
Log in

Molecular and crystal structure of (1R,5S)-8-oxo-1,5,6,8-tetrahydro-2H-1,5-methanopyrido[1,2-a][1,5]diazocine-3(4H)-carboxamide and (1R,5S)-8-OXO-1,5,6,8-tetrahydro-2H-1,5-methanopyrido[1,2-a][1,5]diazocine-3(4H)-thiocarboxamide

  • Brief Communications
  • Published:
Journal of Structural Chemistry Aims and scope Submit manuscript

Abstract

The molecular and crystal structure of (1R,5S)-8-oxo-1,5,6,8-tetrahydro-2H-1,5-methanopyrido[1,2-a][1,5]diazocine-3(4H)-carboxamide and (1R,5S)-8-oxo-1,5,6,8-tetrahydro-2H-1,5-methanopyrido[1,2-a][1,5]diazocine-3(4H)-thiocarboxamide are determined.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

References

  1. I. P. Tsypysheva, A. V. Kovalskaya, N. S. Makara, A. N. Lobov, I. A. Petrenko, E. G. Galkin, T. A. Sapozhnikova, F. S. Zarudii, and M. S. Yunusov, Chem. Nat. Compd., 48, 629 (2012).

    Article  CAS  Google Scholar 

  2. APEX2 and SAINT, Bruker AXS Inc., Madison, Wisconsin, USA (2009).

  3. G. M. Sheldrick, Acta Crystallogr., A64, 112 (2008).

    Article  Google Scholar 

  4. I. P. Tsypysheva, A. N. Lobov, A. V. Kovalskaya, V. I. Vinogradova, K. Yu. Suponitsky, S. L. Khursan, and M. S. Yunusov, Tetrahedron: Asymmetry, 24, 1318 (2013).

    Article  CAS  Google Scholar 

  5. I. P. Tsypysheva, A. V. Kovalskaya, A. N. Lobov, M. Kh. Salimgareeva, U. Sh. Fatkullina, P. R. Petrova, S. F. Gabdrakhmanova, N. S. Makara, K. Yu. Suponitskii, Yu. V. Vakhitova, F. S. Zarudii, and M. S. Yunusov, Chem. Nat. Compd., 49, 707 (2013).

    Article  CAS  Google Scholar 

  6. I. V. Kulakov, O. A. Nurkenov, D. M. Turdybekov, A. A. Ainabaev, and Z. M. Zhambekov, Russ. J. Org. Chem., 46, 543 (2010).

    Article  CAS  Google Scholar 

  7. I. V. Kulakov, O. A. Nurkenov, A. E. Arinova, D. M. Turdybekov, S. A. Talipov, and B. T. Ibragimov, Chem. Nat. Compd., 47, 777 (2011).

    Article  CAS  Google Scholar 

  8. P. Mascagni, M. Christodoulou, W. Gibbons, K. Asres, J. D. Phillipdon, N. Niccolai, and S. Mangani, J. Chem. Soc., Perkin Trans. II, 1159 (1987).

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to I. P. Tsypysheva.

Additional information

Original Russian Text © 2015 K. Yu. Suponitskii, I. P. Tsypysheva, A. V. Koval’skaya.

__________

Translated from Zhurnal Strukturnoi Khimii, Vol. 56, No. 1, pp. 195–197, January–February, 2015.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Suponitskii, K.Y., Tsypysheva, I.P. & Koval’skaya, A.V. Molecular and crystal structure of (1R,5S)-8-oxo-1,5,6,8-tetrahydro-2H-1,5-methanopyrido[1,2-a][1,5]diazocine-3(4H)-carboxamide and (1R,5S)-8-OXO-1,5,6,8-tetrahydro-2H-1,5-methanopyrido[1,2-a][1,5]diazocine-3(4H)-thiocarboxamide. J Struct Chem 56, 188–190 (2015). https://doi.org/10.1134/S0022476615010278

Download citation

  • Received:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1134/S0022476615010278

Keywords

Navigation