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UV spectroscopic quantitative determination of methanofullerene derivatives with a different degree of substitution

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Abstract

A spectroscopic method for the analysis of compounds belonging to methanofullerenes with different functionalization and a number of substituents is developed. In order to determine the composition of mixtures of these compounds the standard spectrophotometric procedure along with derivative spectroscopy are applied. Acceptable reproducubility and sensitivity of the methods used are demonstrated on model mixtures of fullerene derivatives. The reaction mass obtained in the interaction of fullerene with diallyl ester of malonic acid is analyzed.

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Authors and Affiliations

  1. Faculty of Chemistry, Bashkir State University, Ufa, Russia

    Yu. N. Biglova, V. V. Mikheev & A. G. Mustafin

  2. Institute of Organic Chemistry, Ufa Scientific Center, Russian Academy of Sciences, Ufa, Russia

    V. A. Kraikin, S. A. Torosyan, S. V. Kolesov & M. S. Miftakhov

Authors
  1. Yu. N. Biglova
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  2. V. A. Kraikin
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  3. V. V. Mikheev
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  4. S. A. Torosyan
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  5. S. V. Kolesov
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  6. A. G. Mustafin
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  7. M. S. Miftakhov
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Corresponding author

Correspondence to Yu. N. Biglova.

Additional information

Original Russian Text Copyright © 2013 by Yu. N. Biglova, V. A. Kraikin V. V. Mikheev, S. A. Torosyan, S. V. Kolesov, A. G. Mustafin, M. S. Miftakhov

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Translated from Zhurnal Strukturnoi Khimii, Vol. 54, No. 4, pp. 674–678, July–August, 2013.

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Biglova, Y.N., Kraikin, V.A., Mikheev, V.V. et al. UV spectroscopic quantitative determination of methanofullerene derivatives with a different degree of substitution. J Struct Chem 54, 719–723 (2013). https://doi.org/10.1134/S0022476613040094

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  • DOI: https://doi.org/10.1134/S0022476613040094

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