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An investigation of the growth of β-BaB2O4 crystals in the BaB2O4-NaF system and new fluoroborate Ba2Na3[B3O6]2F

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Abstract

The phase formation in the BaB2O4-NaF cut has been investigated by the methods of solid-phase synthesis, visual polythermal analysis, and spontaneous crystallization on a platinum loop. A range of primary crystallization of the new compound Ba2Na3[B3O6]2F (hexagonal system, P63/m, a = 7.346(1) Å, c = 12.636(2) Å) is revealed in this cut, which is used to grow single crystals of low-temperature barium borate modification β-BaB2O4.

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References

  1. R. S. Feigelson, R. J. Raymakers, and R. K. Route, J. Cryst. Growth 97, 352 (1986).

    Article  Google Scholar 

  2. P. P. Fedorov, A. E. Kokh, and N. G. Kononova, Usp. Khim. 71(8), 741 (2002).

    Google Scholar 

  3. K. Itoh, F. Marumo, and Y. Kuwano, J. Cryst. Growth 106(4), 728 (1990).

    Article  ADS  Google Scholar 

  4. A. E. Kokh, N. G. Kononova, P. P. Fedorov, et al., Neorg. Mater. 41(1), 64 (2005).

    Google Scholar 

  5. M. Roth and D. Perlov, J. Cryst. Growth 169, 734 (1996).

    Article  ADS  Google Scholar 

  6. W. Chen, A. Jiang, and G. Wang, J. Cryst. Growth 256, 383 (2003).

    Article  ADS  Google Scholar 

  7. A. E. Kokh, V. N. Popov, T. B. Bekker, et al., J. Cryst. Growth 275(1–2), e669 (2005).

    Article  ADS  Google Scholar 

  8. N. G. Kononova and A. E. Kokh, RF Patent No. 2 195 520, Byull. Izobret., No. 36 (2002).

  9. N. G. Kononova, A. E. Kokh, and P. P. Fedorov, RF Patent No. 2 229 702, Byull. Izobret., No. 15 (2005).

  10. É. G. Rakov and V. V. Teslenko, Pyrohydrolysis of Inorganic Fluorides (Énergoatomizdat, Moscow, 1987) [in Russian].

    Google Scholar 

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Authors and Affiliations

  1. Institute of Geology and Mineralogy, Siberian Branch, Russian Academy of Sciences, pr. Akademika Koptyuga 3, Novosibirsk, 630090, Russia

    A. E. Kokh, N. G. Kononova, T. B. Bekker & E. A. Nigmatulina

  2. Prokhorov General Physics Institute, Russian Academy of Sciences, ul. Vavilova 38, Moscow, 119991, Russia

    P. P. Fedorov

  3. Shubnikov Institute of Crystallography, Russian Academy of Sciences, Leninskiĭ pr. 59, Moscow, 119333, Russia

    A. G. Ivanova

Authors
  1. A. E. Kokh
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  2. N. G. Kononova
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  3. T. B. Bekker
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  4. P. P. Fedorov
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  5. E. A. Nigmatulina
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  6. A. G. Ivanova
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Corresponding author

Correspondence to T. B. Bekker.

Additional information

Original Russian Text © A.E. Kokh, N.G. Kononova, T.B. Bekker, P.P. Fedorov, E.A. Nigmatulina, A.G. Ivanova, 2009, published in Kristallografiya, 2009, Vol. 54, No. 1, pp. 153–158.

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Kokh, A.E., Kononova, N.G., Bekker, T.B. et al. An investigation of the growth of β-BaB2O4 crystals in the BaB2O4-NaF system and new fluoroborate Ba2Na3[B3O6]2F. Crystallogr. Rep. 54, 146–151 (2009). https://doi.org/10.1134/S1063774509010258

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  • DOI: https://doi.org/10.1134/S1063774509010258

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