Abstract
Analysis of fishmeal concentrations in feedstuff is critical to quality control and ingredient statement of commercial feed. Near-infrared reflectance spectroscopy (NIRS) determination for fishmeal was established through the spectral data processed by mean center, normalization, Savitzky–Golay first, partial least square 1 and cross validation. The coefficient of determination (R 2) of NIRS calibration model, the standard error estimated by cross validation (SECV) were 0.9554 and 0.9541, respectively. At the same time, the coefficient of determination of validation was 0.9867. Moreover, it has been proven to be directly correlated between the fishmeal spectra and the loading of the second principal components, and the coefficient of determination of the spectra of the calibration model. These results support our theory that the NIRS method constructed in our study could be used to quantify fishmeal in compound feeds.
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Balabin RM, Safieva RZ (2011) Anal Chim Acta 689:190–197
Balabin RM, Safieva RZ, Lomakina EI (2010) Anal Chim Acta 671:27–35
Barker RF, Harberd NP, Jarvis MG, Flavell RB (1988) J Mol Biol 201:1–17
Bellamy LJ, Nordon A, Littlejohn D (2008) Analyst 133:58–64
Benedetto A, Abete MC, Squadrone S (2011) Food Chem 126:1436–1442
Bhalla V, Grimm PC, Chertow GM, Pao AC (2009) Kidney Int 75:774–779
Bruun SW, Sondergaard I, Jacobsen S (2007) J Agric Food Chem 55:7234–7243
Cámara-Martos F, Zurera-Cosano G, Moreno-Rojas R, García-Gimeno R (2012) Pérez-Rodr íguez F. Food Anal Method 5:19–28
Chen L, Xue X, Ye Z, Zhou J, Chen F, Zhao J (2011) Food Chem 128:1110–1114
Dalmasso A, Fontanella E, Piatti P, Civera T, Rosati S, Bottero MT (2004) Mol Cell Probes 18:81–87
Daszykowski M, Wrobel MS, Czarnik-Matusewicz H, Walczak B (2008) Analyst 133:1523–1531
European Council Decision (2000) Official Journal L 306, 07/12/2000, 32–33
Fernandez-Cabanas VM, Garrido-Varo A, Perez-Marin D, Dardenne P (2006) Appl Spectrosc 60:17–23
Fumière O, Veys P, Boix A, Holst C, Baeten V, Berben G (2009) Biotechnol Agron Soc Environ 13:59–70
Ingravalle F, Abete MC, Crescio MI, Ru G (2007) J Food Prot 70:986–990
Karalazos V, Treasurer J, Cutts CJ, Alderson R, Galloway TF, Albrektsen S, Arnason J, MacDonald N, Pike I, Bell JG (2007) J Agric Food Chem 55:5788–5795
Krcmar P, Rencova E (2003) J Agric Food Chem 51:7655–7658
Lachenmeier DW, Humpfer E, Fang F, Schutz B, Dvortsak P, Sproll C, Spraul M (2009) J Agric Food Chem 57:7194–7199
Mark J, Karner M, Andre M, Rueland J, Huck CW (2010) Anal Chem 82:4209–4215
Martín I, García T, Rojas M, Pegels N, Pavón MÁ, Hernández PE, González I, Martín R (2010) J AOAC Int 93:1768–1777
Mirschel G, Heymann K, Scherzer T (2010) Anal Chem 82:8088–8094
Morita H, Hasunuma T, Vassileva M, Tsenkova R, Kondo A (2011) Anal Chem 83:4023–4029
Nam HM, Srinivasan V, Gillespie BE, Murinda SE, Oliver SP (2005) Int J Food Microbiol 102:161–171
Pavino D, Squadrone S, Cocchi M, Martra G, Marchis D, Abete MC (2010) Food Chem 121:826–831
Pérez-Juan M, Afseth NK, González J, Díaz I, Gispert M, Furnols MF, Oliver MA, Realini CE (2010) Food Res Int 43:1416–1422
Perez-Marin DC, Garrido-Varo A, Guerrero-Ginel JE, Gomez-Cabrera A (2004) Anim Feed Sci Tech 116:333–349
Perez-Marin DC, Garrido-Varo A, Guerrero JE (2006) Appl Spectrosc 60:1432–1437
Péron G, Mittaine JF, Gallic BL (2010) Mar Policy 34:815–820
Pierna JA, Lecler B, Conzen JP, Niemoeller A, Baeten V, Dardenne P (2011) Anal Chim Acta 705:30–34
Pratoomyot J, Bendiksen EÅ, Bell JG, Tocher DR (2010) Aquaculture 305:124–132
Schoringhumer K, Cichna-Markl M (2007) J Agric Food Chem 55:10540–10547
Smyth HE, Cozzolino D, Cynkar WU, Dambergs RG, Sefton M, Gishen M (2008) Anal Bioanal Chem 390:1911–1916
Storme-Paris I, Rebiere H, Matoga M, Civade C, Bonnet PA, Tissier MH, Chaminade P (2010) Anal Chim Acta 658:163–174
Tanabe S, Miyauchi E, Muneshige A, Mio K, Sato C, Sato M (2007) Biosci Biotechnol Biochem 71:1663–1667
Verstraete F (2011) Toxicol Appl Pharm doi:10.1016/j.taap.2010.09.015.
Xiaobo Z, Jiewen Z, Povey MJ, Holmes M, Hanpin M (2010) Anal Chim Acta 667:14–32
Yancy HF, Washington JD, Callahan L, Mason JA, Deaver CM, Farrell DE, Ha T, Sespico E, Falmlen D, Myers MJ (2009) J Food Prot 72:2368–2374
Yuan W, Xiang B, Yu L, Xu J (2011) Food Anal Method 4:550–558
Zhang ZM, Chen S, Liang YZ (2010) Anal Chim Acta 668:149–154
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This study was supported by the National Twelve-Five plan project “Key technology research and demonstration of high level of safety and efficiency of feed industry.” The authors acknowledge Dr. Qin Chen for her useful suggestions and English editing.
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X. Lv and H. Li contributed equally to this work.
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Lv, X., Li, H., Wang, J. et al. Quantification of Fishmeal in Compound Feed Using NIR Spectroscopy. Food Anal. Methods 6, 906–914 (2013). https://doi.org/10.1007/s12161-012-9501-8
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DOI: https://doi.org/10.1007/s12161-012-9501-8