Skip to main content
Log in

Structure and Morphology of Inclusions in 4° Offcut 4H-SiC Epitaxial Layers

  • Published:
Journal of Electronic Materials Aims and scope Submit manuscript

Abstract

The structure of inclusions and their influence on surface morphology, local strain, and basal plane dislocations were investigated in silicon carbide (SiC) epitaxial layers grown on 4° offcut substrates. On high-resolution x-ray topography images, strain fields were observed surrounding the inclusions. Ultraviolet photoluminescence images revealed the presence of strain-induced dislocations around the inclusions. Micro-Raman and microphotoluminescence spectroscopy showed that the inclusions exhibited a complex structure that consisted of 3C polytype regions and misoriented 4H polytype regions. The resulting lattice deformation typically propagates in the step-flow growth direction and causes distorted surface morphology.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. P.G. Neudeck, J. Electron. Mater. 24, 283 (1995).

    Article  CAS  Google Scholar 

  2. S. Ha, P. Mieszkowski, M. Skowronski, and L.B. Roland, J.␣Cryst. Growth 244, 257 (2002).

    Article  CAS  Google Scholar 

  3. J.J. Sumakeris, J.R. Jenny, and A.R. Powell, Mater. Res. Soc. Bull. 30, 280 (2005).

    Article  CAS  Google Scholar 

  4. Basceri, I. Khlebnikov, Y. Khlebnikov, P. Muzykov, M. Sharma, G. Stratiy, M. Silan, and C. Balkas, Mater. Sci. Forum 39, 527 (2006).

    Google Scholar 

  5. J.P. Bergman, H. Lendenmann, P.A. Nilsson, U. Lindefelt, and P. Skytt, Mater. Sci. Forum 353, 299 (2001).

    Article  Google Scholar 

  6. H. Lendenmann, F. Dahlquist, N. Johansson, R. Soderholm, P.A. Nilsson, J.P. Bergman, and P. Skytt, Mater. Sci. Forum 353–356, 727 (2001).

    Article  Google Scholar 

  7. M. Skowronski and S. Ha, J. Appl. Phys. 99, 011101 (2006).

    Article  Google Scholar 

  8. R.E. Stahlbush, M.E. Twigg, K.G. Irvine, J.J. Sumakeris, T.P. Chow, P.A. Losee, L. Zhu, Y. Tang, and W. Wang, Mater. Sci. Forum 457–460, 533 (2004).

    Article  Google Scholar 

  9. S.I. Maximenko and T.S. Sudarshan, J. Appl. Phys. 97, 074501 (2005).

    Article  Google Scholar 

  10. H. Jacobson, J.P. Bergman, C. Hallin, E. Janzén, T. Tuomi, and H. Lendenmann, J. Appl. Phys. 95, 1485 (2004).

    Article  CAS  Google Scholar 

  11. W. Chen and M.A. Capano, J. Appl. Phys. 98, 114907 (2005).

    Article  Google Scholar 

  12. R.L. Myers-Ward, B.L. Van Mil, R.E. Stahlbush, S.L. Katz, J.M. McCrate, S.A. Kitt, C.R. Eddy Jr., and D.K. Gaskill, Mater. Sci. Forum 615–617, 105 (2009).

    Article  Google Scholar 

  13. J.A. Powell, D.J. Larkin, P.B. Abel, L. Zhou, and P. Pirouz, Inst. Phys. Conf. Ser. 142, 77 (1996).

    CAS  Google Scholar 

  14. W. Si, M. Dudley, H.S. Kong, J. Sumakeris, and C. Carter Jr., J. Electron. Mater. 26, 151 (1997).

    Article  CAS  Google Scholar 

  15. T. Okada, T. Kimoto, K. Yamai, H. Matsunami, and F. Inoko, Mater. Sci. Forum 457–460, 521 (2004).

    Article  Google Scholar 

  16. H. Tsuchida, M. Ito, I. Kamata, and M. Nagano, Phys. Status Solidi B 246, 1553 (2009).

    Article  CAS  Google Scholar 

  17. T. Tomota, S. Matsuo, T. Okada, T. Kimoto, T. Mitani, and S. Nakashima, Mater. Sci. Forum 527–529, 339 (2006).

    Article  Google Scholar 

  18. H. Tsuchida, I. Kamata, and M. Nagano, J. Cryst. Growth 306, 254 (2007).

    Article  CAS  Google Scholar 

  19. R.E. Stahlbush, K.K. Liu, Q. Zhang, and J.J. Sumakeris, Mater. Sci. Forum 556, 295 (2007).

    Article  Google Scholar 

  20. N.A. Mahadik, S.B. Qadri, and M.V. Rao, Thin Solid Films 516, 233 (2007).

    Article  CAS  Google Scholar 

  21. O.J. Glembocki, J.D. Caldwell, J.A. Mittereder, J.P. Calame, S.C. Binari, and R.E. Stahlbush, Mater. Sci. Forum 600, 1111 (2009).

    Article  Google Scholar 

  22. R.A. Berechman, M. Skowronski, and Q. Zhang, J. Appl. Phys. 105, 074513 (2009).

    Article  Google Scholar 

  23. S. Maximenko, J.A. Freitas, Y.N. Picard, P.B. Klein, R.L. Myers-Ward, K.K. Lew, P.G. Muzykov, D.K. Gaskill, C.R. Eddy Jr., and T.S. Sudarshan, Mater. Sci. Forum 645–648, 211 (2010).

    Article  Google Scholar 

  24. B.K. Tanner, X-Ray Diffraction Topography (Oxford: Pergamon, 1966).

    Google Scholar 

  25. S. Nakashima and H. Harima, Phys. Status Solidi A 162, 39 (1997).

    Article  CAS  Google Scholar 

  26. A. Galeckas, J. Linnros, and P. Pirouz, Appl. Phys. Lett. 81, 883 (2002).

    Article  CAS  Google Scholar 

  27. A.J. Giles, J.D. Caldwell, R.E. Stahlbush, B.A. Hull, N.A. Mahadik, O.J. Glembocki, K.D. Hobart, and K.K. Lew, J.␣Electron. Mater. 39, 777 (2010).

    Article  CAS  Google Scholar 

Download references

Acknowledgements

N.A.M. and D.A.A. would like to acknowledge the support of the National Research Council’s postdoctoral program at the US Naval Research Laboratory. J.L.T. would like to acknowledge the support of the American Association for Engineering Education’s NRL Postdoctoral Fellowship program. Work at NRL is supported by the Office of Naval Research.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Nadeemullah A. Mahadik.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Mahadik, N.A., Stahlbush, R.E., Qadri, S.B. et al. Structure and Morphology of Inclusions in 4° Offcut 4H-SiC Epitaxial Layers. J. Electron. Mater. 40, 413–418 (2011). https://doi.org/10.1007/s11664-011-1570-8

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11664-011-1570-8

Keywords

Navigation