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Mini-Tensile Experiments of Clock-Rolled Zirconium Plate

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Abstract

We present our efforts to measure the tensile strength of clock-rolled pure zirconium in the through-thickness (TT) direction of the plate. Although the plate is too thin to produce standard ASTM tensile samples in the TT orientation, such measurements are relevant to benchmarking our constitutive models of hardening and texture evolution. We have designed a fixture and sample to perform tensile tests on our 9 mm thick plate. The sample is a double-ligament mini-tensile sample: 8 × 8 × 1 mm overall; each ligament has a gage section of 1 × 1 × 3 mm. In contrast, our standard “macro” tensile sample is a flat dogbone with a gage section of 3 × 1.5 × 25 mm. We validate our design by comparing the results of mechanical tests performed on samples of both geometries. Although the hardening response is nearly identical, the flow stress of the miniature samples is offset by +25 MPa at the onset of plastic yield. We present our efforts to resolve the origin of this offset.

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References

  1. Tomé CN, Maudlin PJ, Lebensohn RA, Kaschner GC (2001) Mechanical response of zirconium—I. Derivation of a polycrystal constitutive law and finite element analysis. Acta Mater 49:3085–3096. doi:10.1016/S1359-6454(01)00190-2

    Article  Google Scholar 

  2. Kaschner GC, Bingert JF, Liu C, Lovato ML, Maudlin PJ, Stout MG, Tome CN (2001) Mechanical response of zirconium—II. Experimental and finite element analysis of bent beams. Acta Mater 49:3097–3108. doi:10.1016/S1359-6454(01)00191-4

    Article  Google Scholar 

  3. Tomé CN, Agnew SR, Blumenthal WR, Bourke MAM, Brown DW, Kaschner GC, Rangaswamy P (2002) The relation between texture, twinning and mechanical properties in hexagonal aggregates. Mater Sci Forum 408–412:263–268

    Article  Google Scholar 

  4. Tomé CN, Kaschner GC (2005) Modeling texture, twinning, and hardening evolution during deformation of hexagonal materials. Mater Sci Forum 495–497:1001–1006. doi:10.4028/0-87849-975-x.1001

    Article  Google Scholar 

  5. Kaschner GC, Tomé CN, Beyerlein IJ, Vogel SC, Brown DW, McCabe RJ (2006) Role of twinning in the hardening response of zirconium during temperature reloads. Acta Mater 54:2887–2896. doi:10.1016/j.actamat.2006.02.036

    Article  Google Scholar 

  6. McCabe RJ, Cerreta EK, Misra A, Kaschner GC, Tome CN (2006) Effects of texture, temperature, and strain on the deformation modes of zirconium. Philos Mag 86:3595–3611. doi:10.1080/14786430600684500

    Article  Google Scholar 

  7. Kaschner GC, Tomé CN, McCabe RJ, Misra A, Vogel SC, Brown DW (2007) Exploring the dislocation/twin interactions in zirconium. Mater Sci Eng A 463:122–127. doi:10.1016/j.msea.2006.09.115

    Article  Google Scholar 

  8. Proust G, Tomé CN, Kaschner GC (2007) Modeling texture, twinning, and hardening evolution during deformation of hexagonal materials. Acta Mater 55:2137–2148. doi:10.1016/j.actamat.2006.11.017

    Article  Google Scholar 

  9. Beyerlein IJ, Kaschner GC, Tomé CN (2007) Plastic Anisotropy of Pure Zirconium from 76 k to 450 k. Proceedings Plasticity, June 2–7, 2007, pp

  10. Proust G, Kaschner GC, Beyerlein IJ, Clausen B, Brown DW, McCabe RJ, Tomé CN (2009) Detwinning of pure zirconium: In situ neutron diffraction experiments. J Exp Mech (in press)

  11. Conrad H (1981) Effect of interstitial solutes on the strength and ductility of titanium. Prog Mater Sci 26:123–403. doi:10.1016/0079-6425(81)90001-3

    Article  Google Scholar 

  12. Christian JW, Mahajan S (1995) Deformation twinning. Prog Mater Sci 39:1–157. doi:10.1016/0079-6425(94)00007-7

    Article  Google Scholar 

  13. Biget MP, Saada G (1995) Effect of interstitital impurities on twinning of titanium and zirconium. J Phys III 5:1833–1840. doi:10.1051/jp3:1995219

    Article  Google Scholar 

  14. Kaschner GC, Gray GT III (2000) The influence of crystallographic texture and interstitial impurities on the mechanical behavior of zirconium. Metall Mater Trans A 31:1997–2003. doi:10.1007/s11661-000-0227-7

    Article  Google Scholar 

  15. Mayer M (1997) SIMNRA User’s Guide, Technical Report IPP 9/113. Max-Plank Institut fur Plasmaphysik, Garching

    Google Scholar 

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Kaschner, G.C., Lovato, M.L., Stout, M.G. et al. Mini-Tensile Experiments of Clock-Rolled Zirconium Plate. Exp Mech 50, 65–70 (2010). https://doi.org/10.1007/s11340-009-9224-y

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  • DOI: https://doi.org/10.1007/s11340-009-9224-y

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