Abstract
Gas evacuation from a partially saturated composite prepregs—a woven fabric reinforcement with a laminated liquid resin film—was characterized using the pulse-decay method. Dimensionless analysis was used to show how the initial pressure, boundary conditions (vacuum pressure at \(x=0\) and with or without a reservoir volume at \(x=L\)), and Klinkenberg parameter effect the predicted decay of gas pressure. By comparing the experimental data to a set of dimensionless master curves, the intrinsic permeability, Klinkenberg parameter, and porosity were determined. Resin saturation was inferred by monitoring the area of resin saturating the initially dry side of the fabric. By mapping the gas flow parameters to the observed area fraction of resin, a complete and repeatable characterization method is demonstrated.
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Acheson, J.A., Simacek, P., Advani, S.G.: The implications of fiber compaction and saturation on fully coupled VARTM simulation. Compos. Part A: Appl. Sci. Manuf. 35(2), 159–169 (2004)
Ahn, K.J., Seferis, J.C., Price, J.O., Berg, A.J.: Permeation measurements through prepreg laminates. Sampe J. 27(6), 19–26 (1991)
Arafath, A.R.A., Fernlund, G., Poursartip, A.: Gas transport in prepregs: model and permeability experiments. In: International Conference on Composite Materials 17. Edinburgh (2009)
Bear, J.: Dynamics of Fluids in Porous Media. Courier Corporation, Chelmsford, MA (1972)
Bourbie, T., Coussy, O., Zinszner, B.: Acoustics of Porous Media. Gulf Publishing Company, Houston (1987)
Brace, W.F., Walsh, J.B., Frangos, W.T.: Permeability of granite under high pressure. J. Geophys. Res. 73(6), 2225–2236 (1968)
Brooks, R. H., Corey, A. T.: Hydraulic properties of porous media. In: Hydrology Papers 3. Colorado State University (1964)
Carman, P.C.: Fluid flow through granular beds. Chem. Eng. Res. Des. 15, S32–S48 (1937)
Cender, T.A., Simacek, P., Advani, S.G.: Resin film impregnation in fabric prepregs with dual length scale permeability. Compos. Part A: Appl. Sci. Manuf. 53, 118–128 (2013)
Cender, T.A., Simacek, P., Advani, S.G.: A method to determine open pore volume with pulse decay. Appl. Phys. Lett. 105(13), 134101 (2014)
Centea, T., Hubert, P.: Measuring the impregnation of an out-of-autoclave prepreg by micro-CT. Compos. Sci. Technol. 71(5), 593–599 (2011)
Centea, T., Hubert, P.: Out-of-autoclave prepreg consolidation under deficient pressure conditions. J. Compos. Mater. (2013). doi:10.1177/0021998313494101
Centea, T., Grunenfelder, L.K., Nutt, S.R.: A review of out-of-autoclave prepregs-material properties, process phenomena, and manufacturing considerations. Compos. Part A: Appl. Sci. Manuf. 70, 132–154 (2015)
Civan, F.: Effective correlation of apparent gas permeability in tight porous media. Transp. Porous Media 82, 375–384 (2010)
Darabi, H., Ettehad, A., Javadpour, F., Sepehrnoori, K.: Gas flow in ultra-tight shale strata. J. Fluid Mech. 710, 641–658 (2012)
Darcy, H.: Les fontaines publiques de la ville de Dijon. Victor Dalmont, Paris (1856)
Feser, J., Prasad, A., Advani, S.G.: Experimental characterization of in-plane permeability of gas diffusion layers. J. Power Sources 162(2), 1226–1231 (2006)
Florence, F.A., Rushing, J., Newsham, K.E., Blasingame, T.A.: Improved permeability prediction relations for low permeability sands. In Rocky mountain oil & gas technology symposium. Society of Petroleum Engineers (2007)
Grunenfelder, L.K., Centea, T., Hubert, P., Nutt, S.R.: Effect of room-temperature out-time on tow impregnation in an out-of-autoclave prepreg. Compos. Part A: Appl. Sci. Manuf. 45, 119–126 (2013)
Grunenfelder, L.K., Nutt, S.R.: Void formation in composite prepregs-effect of dissolved moisture. Compos. Sci. Technol. 70(16), 2304–2309 (2010)
Helmus, R., Centea, T., Hubert, P., Hinterholzl, R.: Out-of-autoclave prepreg consolidation: Coupled air evacuation and prepreg impregnation modeling. J. Compos. Mater. 50, 1403–1413 (2015)
Hou, Y., Comas-Cardona, S., Binetruy, C., Drapier, S.: Gas transport in fibrous media: application to in-plane permeability measurement using transient flow. J. Compos. Mater. 47(18), 2237–2247 (2012)
Hsiao, K.: Gas Transport and Water Vapourization in Out-of-Autoclave Prepreg Laminates. Master’s thesis, University of British Columbia, Vancouver (2012)
Jannot, Y., Lasseux, D.: A new quasi-steady method to measure gas permeability of weakly permeable porous media. Rev. Sci. Instrum. 83(1), 015113 (2012)
Jones, S.C.: A rapid accurate unsteady-state Klinkenberg permeameter. SPE 3535, 383–397 (1972)
Klinkenberg, L.J.: The permeability of porous media to liquids and gases. American Petroleum Institute (1941)
Knudsen, M.: Die Gesetze der Molekularströmung und der inneren Reibungsströmung der Gase durch Röhren. Ann. Phys. 333(1), 75–130 (1909)
Kozeny, J.: Über kapillare Leitung des Wassers im Boden, vol. 136. Sitzungsber Akad Wiss, Wien (1927)
Kratz, J., Hubert, P.: Anisotropic air permeability in out-of-autoclave prepregs: Effect on honeycomb panel evacuation prior to cure. Compos. Part A: Appl. Sci. Manuf. 49, 179–191 (2013)
Leclaire, P., Umnova, O., Horoshenkov, K.V., Maillet, L.: Porosity measurement by comparison of air volumes. Rev. Sci. Instrum. 74(3), 1366–1370 (2003)
Levy, A., Kratz, J., Hubert, P.: Air evacuation during vacuum bag only prepreg processing of honeycomb sandwich structures: In-plane air extraction prior to cure. Compos. Part A: Appl. Sci. Manuf. 68, 365–376 (2015)
Li, J., Zhan, H., Huang, G.: Applicability of the linearized governing equation of gas flow in porous media. Trans. Porous Media 87(3), 815–834 (2011)
Liang, Y., Price, J.D.: Nonlinear pressure diffusion in a porous medium: approximate solutions with applications to permeability measurements using transient pulse decay method. J. Geophys. Res. 106, 529–535 (2001)
Muskat, M.: The flow of compressible fluids through porous media and some problems in heat conduction. J. Appl. Phys. 5, 71–94 (1934)
Parseval, Y.D.E., Pillai, K.M., Advani, S.G.: A simple model for the variation of permeability due to partial saturation in dual scale porous media. Trans. Porous Media 27, 243–264 (1997)
Pettersson, P.: Fluid Flow in Wood Fiber Networks. Ph.D. Thesis, Lulea University of Technology, Lulea (2006)
Roy, S., Raju, R., Chuang, H.F., Cruden, B., Meyyappan, M.: Modeling gas flow through microchannels and nanopores. J. Appl. Phys. 93(8), 4870 (2003)
Salissou, Y., Panneton, R.: Pressure/mass method to measure open porosity of porous solids. J. Appl. Phys. 101(12), 124913 (2007)
Standard, A.S.T.M.: D6226-10: Standard Test Method for Open Cell Content of Rigid Cellular Plastics. ASTM International, West Conshohocken, PA (2010)
Steckelmacher, W.: Knudsen flow 75 years on: the current state of the art for flow of rarefied gases in tubes and systems. Rep. Prog. Phys. 49, 1083–1107 (1986)
Tavares, S.S., Michaud, V.: Through thickness air permeability of prepregs during cure. Compos. Part A: Appl. Sci. Manuf. 40(10), 1587–1596 (2009)
Tavares, S.S., Michaud, V.: Assessment of semi-impregnated fabrics in honeycomb sandwich structures. Compos. Part A: Appl. Sci. Manuf. 41(1), 8–15 (2010)
Thomas, S., Bongiovanni, C., Nutt, S.R.: In situ estimation of through-thickness resin flow using ultrasound. Compos. Sci. Technol. 68, 3093–3098 (2008)
Vazques, J.L.: The Porous Media Equation: Mathematical Theory. Oxford University Press, Oxford (2006)
Wu, Y.S., Pruess, K., Persoff, P.: Gas flow in porous media with Klinkenberg effects. Trans. Porous Media 32, 117–137 (1998)
Zhang, D., Heider, D., Gillespie Jr., J.W.: Role of Prepreg Interlayer Permeability on Void Reduction During Oven Vacuum Bag Processing of Thick Section Thermoplastic Composites. Society for Advanced Materials and Processes Engineering, Baltimore (2015)
Ziarani, A.S., Aguilera, R.: Knudsens permeability correction for tight porous media. Trans. Porous Media 91, 239–260 (2012)
Acknowledgments
We would like to thank Mehmet Ömer and Emily Readdy for their help with the experimental validation. Research was sponsored by the Office of Naval Research under Grant No. N00014-10-1-0971. Any opinions, findings, and conclusions or recommendations expressed in this material are those of the author(s) and do not necessarily reflect the views of the Office of Naval Research. Research was also supported by the Delaware Space Grant College and Fellowship Program (NASA Grant NNX15AI19H).
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Cender, T.A., Simacek, P., Davis, S. et al. Gas Evacuation from Partially Saturated Woven Fiber Laminates. Transp Porous Med 115, 541–562 (2016). https://doi.org/10.1007/s11242-016-0784-x
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DOI: https://doi.org/10.1007/s11242-016-0784-x