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Recrystallization, texture evolution, and magnetostriction behavior of rolled (Fe81Ga19)98B2 sheets during low-to-high temperature heat treatments

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Abstract

In order to study the texture evolution and magnetostriction behavior in the rolled Fe–Ga–B sheets during the heat treatments from low to high temperatures, (Fe81Ga19)98B2 sheets were prepared and investigated. The phase structure, recrystallization, grain size, texture evolution, and magnetostriction behavior during the annealing from 525 to 1200 °C for 1–5 h were investigated using X-ray diffraction, electron backscattering diffraction, and standard strain-gauge measurements. Results indicated that the primary recrystallization temperature for 1-h annealing was found as 525–575 °C in (Fe81Ga19)98B2 sheets. Annealing the sample below 575 °C for 1 h, the release of rolling stress and increase of 〈100〉 η-fiber texture during the primary recrystallization jointly resulted in a rapid improvement in magnetostriction. After annealed between 575 and 1100 °C for 1 h, the grains of the sheets underwent a normal growth, and the three (α-, γ- and η-fiber) types of textures kept an approximate balance, leading to a plateau of magnetostriction around 75 ppm. When the abnormal grain growth proceeded above 1100 °C for 1 h, the proportion of η-fiber texture markedly increased, and the magnetostriction was subsequently increased to 97 ppm. For longer annealing durations, the strong ideal cube texture (η-fiber) was firstly formed and then changed to undesired texture (γ-fiber), producing a corresponding magnetostriction peak of 136 ppm at 2 h for the annealing at 1200 °C. The clear correlation among heat treatments, recrystallization, texture, and magnetostriction provides an essential understanding for Fe–Ga–B alloy sheets.

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References

  1. Clark AE, Restorff JB, Wun-Fogle M, Lograsso TA, Schlagel DL (2000) Magnetostrictive properties of body-centered cubic Fe–Ga and Fe–Ga–Al alloys. IEEE Trans Magn 36:3238–3240

    Article  Google Scholar 

  2. Cullen JR, Clark AE, Wun-Fogle M, Restorff JB, Lograsso TA (2001) Magnetoelasticity of Fe–Ga and Fe–Al alloys. J Magn Magn Mater 226–230:948–949

    Article  Google Scholar 

  3. Srisukhumbowornchai N, Guruswamy S (2001) Large magnetostriction in directionally solidified FeGa and FeGaAl alloys. J Appl Phys 90:5680–5688

    Article  Google Scholar 

  4. Liu JH, Wang ZB, Jiang CB, Xu HB (2010) Magnetostriction under high prestress in Fe81Ga19 crystal. J Appl Phys 108:033913–033914

    Article  Google Scholar 

  5. Guruswamy S, Srisukhumbowornchai N, Clark AE, Restorff JB, Wun-Fogle M (2000) Strong, ductile, and low-field-magnetostrictive alloys based on Fe–Ga. Scripta Mater 43:239–244

    Article  Google Scholar 

  6. Clark AE, Wun-Fogle M, Restorff JB, Lograsso TA, Cullen JR (2001) Effect of quenching on the magnetostriction on Fe1−x Ga x (0.13 < x < 0.21). IEEE Trans Magn 37:2678–2680

    Article  Google Scholar 

  7. Kellogg RA, Russell AM, Lograsso TA, Flatau AB, Clark AE, Wun-Fogle M (2003) Mechanical properties of magnetostrictive iron–gallium alloys. Proc SPIE 5053:534–543

    Article  Google Scholar 

  8. Olabi AG, Grunwald A (2008) Design and application of magnetostrictive materials. Mater Des 29:469–483

    Article  Google Scholar 

  9. Downey PR, Flatau AB (2005) Magnetoelastic bending of Galfenol for sensor applications. J Appl Phys 97:10R505-3

    Article  Google Scholar 

  10. Clark AE, Hathaway KB, Wun-Fogle M, Restorff JB, Lograsso TA, Keppens VM, Petculescu G, Taylor RA (2003) Extraordinary magnetoelasticity and lattice softening in bcc Fe–Ga alloys. J Appl Phys 93:8621–8623

    Article  Google Scholar 

  11. Srisukhumbowornchai N, Guruswamy S (2004) Crystallographic textures in rolled and annealed Fe–Ga and Fe–Al alloys. Metall Mater Trans A 35:2963–2970

    Article  Google Scholar 

  12. Na SM, Flatau AB (2005) Magnetostriction and surface-energy-induced selective grain growth in rolled Galfenol doped with sulfur. Proc SPIE 5761:192–199

    Article  Google Scholar 

  13. Summers EM, Meloy R, Na S-M (2009) Magnetostriction and texture relationships in annealed galfenol alloys. J Appl Phys 105:07A922-923

    Article  Google Scholar 

  14. Li JH, Gao XX, Xie JX, Yuan C, Zhu J, Yu RB (2012) Recrystallization behavior and magnetostriction under pre-compressive stress of Fe–Ga–B sheets. Intermetallics 26:66–71

    Article  Google Scholar 

  15. Na SM, Flatau AB (2012) Single grain growth and large magnetostriction in secondarily recrystallized Fe–Ga thin sheet with sharp Goss (011)[100] orientation. Scripta Mater 66:307–310

    Article  Google Scholar 

  16. Na SM, Flatau AB (2007) Secondary recrystallization, crystallographic texture and magnetostriction in rolled Fe–Ga based alloys. J Appl Phys 101:09N518-3

    Article  Google Scholar 

  17. Li J, Gao X, Zhu J, He C, Qiao J, Zhang M (2009) Texture evolution and magnetostriction in rolled (Fe81Ga19)99Nb1 alloy. J Alloy Compd 476:529–533

    Article  Google Scholar 

  18. Li JH, Gao XX, Zhu J, Bao XQ, Xia T, Zhang MC (2010) Ductility, texture and large magnetostriction of Fe–Ga-based sheets. Scripta Mater 63:246–249

    Article  Google Scholar 

  19. Na SM, Flatau AB (2012) Surface-energy-induced selective growth of (001) grains in magnetostrictive ternary Fe–Ga-based alloys. Smart Mater Struct 21:055024-10

    Google Scholar 

  20. Cheng LM, Nolting AE, Voyzelle B, Galvani C (2007) Deformation behavior of polycrystalline Galfenol at elevated temperatures. Proc SPIE 6526:N5262

    Google Scholar 

  21. Na SM, Flatau AB (2008) Deformation behavior and magnetostriction of polycrystalline Fe–Ga–X (X = B, C, Mn, Mo, Nb, NbC) alloys. J Appl Phys 103:07D304-3

    Article  Google Scholar 

  22. Li J, Gao X, Zhu J, Li J, Zhang M (2009) Ductility enhancement and magnetostriction of polycrystalline Fe–Ga based alloys. J Alloy Compd 484:203–206

    Article  Google Scholar 

  23. Huang M, Lograsso TA, Clark AE, Restorff JB, Wun-Fogle M (2008) Effect of interstitial additions on magnetostriction in Fe–Ga alloys. J Appl Phys 103:07B314-3

    Google Scholar 

  24. Bormio-Nunes C, dos Santos CT, Dias MB, Doerr M, Granovsky S, Loewenhaupt M (2012) Magnetostriction of the polycrystalline Fe80Al20 alloy doped with boron. J Alloy Compd 539:226–232

    Article  Google Scholar 

  25. Bormio-Nunes C, dos Santos CT, Leandro IF, Turtelli RS, Grossinger R, Atif M (2011) Improved magnetostriction of Fe72Ga28 boron doped alloys. J Appl Phys 109:07A934-3

    Google Scholar 

  26. Gong Y, Jiang CB, Xu HB (2006) Effects of boron addition on phase structure and magnetostriction of Fe–Ga alloys. Acta Metall Sin 42:830–834

    Google Scholar 

  27. Lograsso TA, Summers EM (2006) Detection and quantification of D03 chemical order in Fe–Ga alloys using high resolution X-ray diffraction. Mater Sci Eng A 416:240–245

    Article  Google Scholar 

  28. Lograsso TA, Ross AR, Schlagel DL, Clark AE, Wun-Fogle M (2003) Structural transformations in quenched Fe–Ga alloys. J Alloy Compd 350:95–101

    Article  Google Scholar 

  29. Yu LG, Chen XJ, Khor KA, Sundararajan G (2005) FeB/Fe2B phase transformation during SPS pack-boriding: boride layer growth kinetics. Acta Mater 53:2361–2368

    Article  Google Scholar 

  30. Dybkov VI, Lengauer W, Gas P (2006) Formation of boride layers at the Fe-25 % Cr alloy–boron interface. J Mater Sci 41:4948–4960. doi:10.1007/s10853-006-0032-9

    Article  Google Scholar 

  31. Bormio-Nunes C, Dias MB, Ghivelder L (2013) High magnetostriction of the polycrystalline alloy (Fe0.8Al0.2)97B3. J Alloy Compd 574:467–471

    Article  Google Scholar 

  32. Liang YF, Ge JW, Fang XS, Ye F, Lin JP (2013) Hot deformation behavior and softening mechanism of Fe-6.5 wt% Si alloy. Mater Sci Eng A 570:8–12

    Article  Google Scholar 

  33. Sauvage X, Wilde G, Divinski SV, Horita Z, Valiev RZ (2012) Grain boundaries in ultrafine grained materials processed by severe plastic deformation and related phenomena. Mater Sci Eng A 540:1–12

    Article  Google Scholar 

  34. Zhang Y, Tao NR, Lu K (2008) Mechanical properties and rolling behaviors of nano-grained copper with embedded nano-twin bundles. Acta Mater 56:2429–2440

    Article  Google Scholar 

  35. Chan Hee P, Jong Woo W, Jin-Woo P, Semiatin SL, Chong Soo L (2012) Mechanisms and kinetics of static spheroidization of hot-worked Ti-6Al-2Sn-4Zr-2Mo-0.1Si with a lamellar microstructure. Metall Mater Trans A 43:977–985

    Article  Google Scholar 

  36. Asuda T, Morikawa T, Nakayama Y, Suzuki S (1997) Grain-boundary migration of quartz during annealing experiments at high temperatures and pressures, with implications for metamorphic geology. J Metamorph Geol 15:311–322

    Article  Google Scholar 

  37. Yoshitomi Y, Iwayama K, Nagashima T, Harase J, Takahashi N (1993) Coincidence grain-boundary and role of inhibitor for secondary recrystallization in Fe-3 % Si alloy. Acta Metall Mater 41:1577–1585

    Article  Google Scholar 

  38. Suok-Min N, Jin-Hyeong Y, Flatau AB (2009) Abnormal (110) grain growth and magnetostriction in recrystallized Galfenol with dispersed niobium carbide. IEEE Trans Magn 45:4132–4135

    Article  Google Scholar 

  39. Chun H, Na S-M, Yoo J-H, Wuttig M, Flatau AB (2011) Tension and strain annealing for abnormal grain growth in magnetostrictive Galfenol rolled sheet. J Appl Phys 109:07A941–943

    Article  Google Scholar 

  40. Raabe D, Lücke K (1992) Annealing textures of bcc metals. Scripta Metall Mater 27:1533–1538

    Article  Google Scholar 

  41. Raabe D, Lücke K (1994) Rolling and annealing textures of bcc metals. Mater Sci Forum 157:597–610

    Article  Google Scholar 

Download references

Acknowledgements

This work was supported by the National Basic Research Program of China (973 Program: 2012CB619404) and the National Natural Science Foundation of China (Grant Nos. 51101006, 51221163, and 50925101).

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Correspondence to Chengbao Jiang.

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Sun, A., Liu, J. & Jiang, C. Recrystallization, texture evolution, and magnetostriction behavior of rolled (Fe81Ga19)98B2 sheets during low-to-high temperature heat treatments. J Mater Sci 49, 4565–4575 (2014). https://doi.org/10.1007/s10853-014-8156-9

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