Skip to main content
Log in

Determination of styrene-butadiene rubber composition by attenuated total internal reflection infrared spectroscopy

  • Published:
Journal of Applied Spectroscopy Aims and scope

A rapid method for determining the composition of styrene-butadiene rubber using attenuated total internal reflection infrared spectroscopy was proposed. PMR and 13C NMR spectroscopy and infrared transmission spectroscopy were used as absolute techniques for determining the compositions of calibration samples. It was shown that the method was applicable to a wide range of styrene-butadiene rubbers, did not require additional sample preparation, and was easily reproducible.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. F. E. Kuperman, New Rubbers for Tires [in Russian], NIIShP, Moscow (2011), pp. 176–179.

    Google Scholar 

  2. F. E. Kuperman, F. S. Kantor, L. V. Masagutova, and S. V. Novikov, Kauch. Rezina, No. 9, 15–18 (1983).

  3. F. E. Kuperman, Proizvod. Ispol’z. Elastomerov, No. 10–11, 5–19 (1997).

  4. C. E. Miller, B. E. Eichinger, T. W. Gurley, and J. G. Hermiller, Anal. Chem., 62, 1778–1785 (1990).

    Article  Google Scholar 

  5. J. F. Masson, L. Pelletier, and P. Collins, J. Appl. Polym. Sci., 79, No. 5, 1034–1041 (2001).

    Article  Google Scholar 

  6. J. Guilment and L. Bokobza, Vib. Spectrosc., 26, 133–149 (2001).

    Article  Google Scholar 

  7. S. B. Munteanu and C. Vasile, J. Optoelectron. Mater., 7, No. 6, 3135–3148 (2005).

    Google Scholar 

  8. A. S. Orlov, V. I. Mashukov, A. R. Rakintin, and E. S. Novikova, Zh. Prikl. Spektrosk., 79, No. 3, 499–504 (2012).

    Google Scholar 

  9. M. Yao, H. Zhang, X. Zhang, and S. Zhao, Chin. J. Polym. Sci., 29, No. 4, 431–438 (2011).

    Article  Google Scholar 

  10. A. J. Brandolini and D. D. Hills, NMR Spectra of Polymers and Polymer Additives, Marcel Dekker Inc., New York (2000), pp. 660–670.

    Google Scholar 

  11. J. Dechant, R. Danz, W. Kimmer, and R. Schmolke, Ultrarotspektroskopische Untersuchungen an Polymeren, Akademie-Verlag, Berlin (1972).

    Google Scholar 

  12. L. A. Kazitsyna and N. B. Kupletskaya, Application of UV, IR, and NMR Spectroscopy in Organic Chemistry [in Russian], Vysshaya Shkola, Moscow (1971), pp. 214–234.

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to A. S. Orlov.

Additional information

Translated from Zhurnal Prikladnoi Spektroskopii, Vol. 80, No. 1, pp. 51–57, January–February, 2013.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Orlov, A.S., Kiselev, S.A., Kiseleva, E.A. et al. Determination of styrene-butadiene rubber composition by attenuated total internal reflection infrared spectroscopy. J Appl Spectrosc 80, 47–53 (2013). https://doi.org/10.1007/s10812-013-9719-2

Download citation

  • Received:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s10812-013-9719-2

Keywords

Navigation