Abstract
As a result of the miniaturization of machined shapes, the conventional micro-milling technology has been widely used in many industrial areas. However, the machining of some types of materials proved to be very difficult. One of the hard-to-machine materials is also pure molybdenum, which, thanks to its high melting temperature, is used, besides others, in the energy industry and for physical applications. To ensure proper functionality of the manufactured parts, it is essential that they are machined without defects and with the required surface quality. The aim of this study was to find an optimal tool with a diameter of 0.8 mm and to set the machine parameters for machining of pure molybdenum with the highest quality of the surface layer possible without any defects. For this purpose, 26-round design of experiment (DoE) was carried out, in which the parameters, like cutting speed, feed, and coating (yes/no) were systematically changed. The machined samples were evaluated for topography using a 3D profilometer; their morphology and burrs were studied using an electron microscope, and the microscopic implications on the microstructure of the subsurface layer were studied on the produced lamellae using transmission electron microscope (TEM). In addition, the tool wear curve was examined and evaluated. In this study, an optimal setup of machining parameters for pure molybdenum machining (cutting speed = 80 m/min, feed = 0.002 mm/tooth, non-coated tool) was found with which high-quality and defect-free surfaces can be machined.
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References
Li H, Lai X, Li C, Feng J, Ni J (2007) Modelling and experimental analysis of the effects of tool wear, minimum chip thickness and micro tool geometry on the surface roughness in micro-end-milling. J Micromech Microeng 18(2):025006. https://doi.org/10.1088/0960-1317/18/2/025006
Chae J, Park SS, Freiheit T (2006) Investigation of micro-cutting operations. Int J Mach Tools Manuf 46(3):313–332. https://doi.org/10.1016/j.ijmachtools.2005.05.015
Shields J (2013) Applications of molybdenum metal and its alloys. Int Molybdenum Ass. ISBN 978-1-907470-30-1
Mouralova K, Kovar J, Klakurkova L, Blazik P, Kalivoda M, Kousal P (2018) Analysis of surface and subsurface layers after WEDM for Ti-6Al-4V with heat treatment. Measurement 116:556–564. https://doi.org/10.1016/j.measurement.2017.11.053
Mouralova K, Kovar J, Klakurkova L, Bednar J, Benes L, Zahradnicek R (2018) Analysis of surface morphology and topography of pure aluminium machined using WEDM. Measurement 114:169–176. https://doi.org/10.1016/j.measurement.2017.09.040
Mouralova K, Kovar J, Zahradnicek R, Holub M (2017) Analysis of machinability of pure-cobalt disc for magnetron deposition using WEDM. In International Conference Mechatronics, 141–148. https://doi.org/10.1007/978-3-319-65960-2_19.
Mouralova K, Zahradnicek R, Hrdy R (2017) Using WEDM machine a pure molybdenum welding electrode. MM Sci J 2017:2109–2113
Mouralova K, Benes L, Zahradnicek R (2017) Defects in the surface layer of pure molybdenum after WEDM. Manuf Technol:786–790
Sortino M, Totis G, Prosperi F (2013) Dry turning of sintered molybdenum. J Mater Process Technol 213(7):1179–1190. https://doi.org/10.1016/j.jmatprotec.2013.01.017
Bonaiti G, Parenti P, Annoni M, Kapoor S (2017) Micro-milling machinability of DED additive titanium Ti-6Al-4V. Procedia Manuf 10:497–509. https://doi.org/10.1016/j.promfg.2017.07.104
Ahmadi M, Karpat Y, Acar O, Kalay YE (2018) Microstructure effects on process outputs in micro scale milling of heat treated Ti6Al4V titanium alloys. J Mater Process Technol 252:333–347. https://doi.org/10.1016/j.jmatprotec.2017.09.042
Swain N, Venkatesh V, Kumar P, Srinivas G, Ravishankar S, Barshilia HC (2017) An experimental investigation on the machining characteristics of Nimonic 75 using uncoated and TiAlN coated tungsten carbide micro-end mills. CIRP J Manuf Sci Technol 16:34–42. https://doi.org/10.1016/j.cirpj.2016.07.005
Ucun İ, Aslantaş K, Gökçe B, Bedir F (2014) Effect of tool coating materials on surface roughness in micromachining of Inconel 718 super alloy. Proc Inst Mech Eng B J Eng Manuf 228(12):1550–1562. https://doi.org/10.1177/0954405414522217
Ucun I, Aslantas K, Bedir F (2013) An experimental investigation of the effect of coating material on tool wear in micro milling of Inconel 718 super alloy. Wear 300(1):8–19. https://doi.org/10.1016/j.wear.2013.01.103
Kuram E, Ozcelik B (2017) Optimization of machining parameters during micro-milling of Ti6Al4V titanium alloy and Inconel 718 materials using Taguchi method. Proc Inst Mech Eng B J Eng Manuf 231(2):228–242. https://doi.org/10.1177/0954405415572662
Ucun I, Aslantas K, Bedir F (2015) The performance of DLC-coated and uncoated ultra-fine carbide tools in micromilling of Inconel 718. Precis Eng 41:135–144. https://doi.org/10.1016/j.precisioneng.2015.01.002
Lekkala R, Bajpai V, Singh RK, Joshi SS (2011) Characterization and modeling of burr formation in micro-end milling. Precis Eng 35(4):625–637. https://doi.org/10.1016/j.precisioneng.2011.04.007
Schueler GM, Engmann J, Marx T, Haberland R, Aurich JC (2010) Burr formation and surface characteristics in micro-end milling of titanium alloys. In: Burrs-analysis, control and removal. Springer, Berlin, pp 129–138. https://doi.org/10.1007/978-3-642-00568-8_14
Lee K, Dornfeld DA (2004) A study of surface roughness in the micro-end-milling process
Liu X, DeVor RE, Kapoor SG, Ehmann KF (2004) The mechanics of machining at the microscale: assessment of the current state of the science. J Manuf Sci Eng 126(4):666–678. https://doi.org/10.1115/1.1813469
Tansel I, Rodriguez O, Trujillo M, Paz E, Li W (1998) Micro-end-milling-I. Wear and breakage. Int J Mach Tools Manuf 38(12):1419–1436. https://doi.org/10.1016/S0890-6955(98)00015-7
Tansel I, Trujillo M, Nedbouyan A, Velez C, Bao WY, Arkan TT, Tansel B (1998) Micro-end-milling—III. Wear estimation and tool breakage detection using acoustic emission signals. Int J Mach Tools Manuf 38(12):1449–1466. https://doi.org/10.1016/S0890-6955(98)00017-0
Bao WY, Tansel IN (2000) Modeling micro-end-milling operations. Part III: influence of tool wear. Int J Mach Tools Manuf 40(15):2193–2211. https://doi.org/10.1016/S0890-6955(00)00056-0
Weinert K, Petzoldt V (2008) Machining NiTi micro-parts by micro-milling. Mater Sci Eng A 481:672–675. https://doi.org/10.1016/j.msea.2006.10.220
Rahman M, Kumar AS, Prakash JRS (2001) Micro milling of pure copper. J Mater Process Technol 116(1):39–43. https://doi.org/10.1016/S0924-0136(01)00848-2
Montgomery DC (2013) Design and analysis of experiments, Eighth edition, ISBN 978-1118146927-X.
Hasson R (1968) Metallography of molybdenum in color. Microscope 16:329–334
Jiang XJ, Whitehouse DJ (2012) Technological shifts in surface metrology. CIRP Ann Manuf Technol 61(2):815–836. https://doi.org/10.1016/j.cirp.2012.05.009.
Geometrical Product Specifications (GPS) - Surface texture (1996) Profile method; surfaces having stratified functional properties - part 2: height characterization using the linear material ratio curve. ISO 13565-2. International Organization for Standardization, Geneva
Geometrical Product Specifications (GPS) -Surface texture (1997) Profile method -terms, definitions and surface texture parameters. ISO 4287. International Organization for Standardization, Geneva
Li G, Li N, Wen C, Ding S (2017) Investigation and modeling of flank wear process of different PCD tools in cutting titanium alloy Ti6Al4V. Int J Adv Manuf Technol 95:1–15. https://doi.org/10.1007/s00170-017-1222-0
Cheng K, Huo D (2013) Micro-cutting: fundamentals and applications. ISBN:9780470972878
Hashimura M, Hassamontr J, Dornfeld DA (1999) Effect of in-plane exit angle and rake angles on burr height and thickness in face milling operation. J Manuf Sci Eng 121(1):13–19. https://doi.org/10.1115/1.2830566
Fitzpatrick ME, Fry AT, Holdway P, Kandil FA, Shackleton J, Suominen L (2005) Determination of residual stresses by X-ray diffraction, ISSN: 1368-6550
Acknowledgements
This work was carried out with the support of CEITEC Nano Research Infrastructure (ID LM2015041, MEYS CR, 2016–2019), CEITEC Brno University of Technology.
This work is an output of research and scientific activities of NETME Centre, supported through project NETME CENTRE PLUS (LO1202) by financial means from the Ministry of Education, Youth and Sports under the National Sustainability Programme I.
The article was supported by project no. FEKT-S-17-3934, Utilization of novel findings in micro and nanotechnologies for complex electronic circuits and sensor applications.
This research work was supported by the BUT, Faculty of Mechanical Engineering, Brno, Specific research 2016, with the grant “Research of modern production technologies for specific applications”, FSI-S-16-3717, and technical support of Intemac Solutions, Ltd., Kurim.
This work was supported through the internal grant provided by the Jan Evangelista Purkyně University in Ústí nad Labem, called SGS (Student Grant Competition), No. 0004/2015, and partly by the Ministry of Education, Youth, and Sport of the Czech Republic, the program NPU1, project No. LO1207.
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Mouralova, K., Benes, L., Prokes, T. et al. Micro-milling machinability of pure molybdenum. Int J Adv Manuf Technol 102, 4153–4165 (2019). https://doi.org/10.1007/s00170-019-03524-5
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DOI: https://doi.org/10.1007/s00170-019-03524-5