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Thermo-oxidative aging of elastomers: a temperature control unit for operation with the NMR-MOUSE

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Abstract

Temperature-controlled measurements of the transverse relaxation time were conducted with the NMR-MOUSE (nuclear magnetic resonance mobile universal surface explorer) at 50°C to investigate the heterogeneity of rubber sheets induced by thermo-oxidative aging. With temperature stabilization the relative error ofT 2 decreased by a factor of 4 on the short time scale. Without temperature stabilization it may reach 30% in the long-time range because of temperature changes in the laboratory. Two different types of mobile temperature control units operating with the NMR-MOUSE are described. These temperature control units are small and portable like the NMR-MOUSE.

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Authors and Affiliations

  1. Military Institute, Kaliningrad State University, Kaliningrad, Russian Federation

    S. Anferova & V. Anferov

  2. Institute for Technical Chemistry and Macromolecular Chemistry, Aachen University of Technology, Aachen, Germany

    M. Adams, R. Fechete, G. Schroeder & B. Blümich

  3. AixNMR Zentrum für Magnetische Resonanz e.V., Roetgen, Germany

    B. Blümich

  4. Macromolecular Chemistry, Rheinisch-Westfälische Technische Hochschule Aachen, 52056, Aachen, Germany

    B. Blümich

Authors
  1. S. Anferova
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  2. V. Anferov
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  3. M. Adams
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  4. R. Fechete
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  5. G. Schroeder
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  6. B. Blümich
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Anferova, S., Anferov, V., Adams, M. et al. Thermo-oxidative aging of elastomers: a temperature control unit for operation with the NMR-MOUSE. Appl. Magn. Reson. 27, 361–370 (2004). https://doi.org/10.1007/BF03166737

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  • DOI: https://doi.org/10.1007/BF03166737

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