Abstract
15N and14N NMR data are reported for a number of fused ring N-heterocycles.14N line widths,15N-1H couplings and nitrogen shielding additivity rales are used for15N signal assignments. The results obtained lead to some progress in the generalization of the effects of nitrogen-nitrogen interactions on nitrogen shieldings.
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Albert, A., Brown, D. J., and Cheeseman, G. (1951)J. Chem. Soc. 979.
Albert, A., and Pedersen, C. (1956)J. Chem. Soc. 4683.
Allen, C. F. H., Beilfuss, H. R., Barnes, D. M., Reynolds, G. A., Finker, J. F., and Van Allan, J. A. (1959)J. Org. Chem. 24, 796.
Goodman, M. M., Atwood, J. L., Carlin, R., Hunter, W., and Paudler, W. W. (1976)J. Org. Chem. 41, 2860.
Kaczmarek, L., Nantka-Namirski, P., Stefaniak, L., Webb, G. A., Davoust, D., and Basselier, J. J. (1985)Magn. Reson. Chem. 23, 853.
Mazur, J. A., and Koczergin, P. M. (1970)Chim Giotierocycl. Soedin, 508.
Miyadera, T., and Iwai, I. (1964)Chem. Pharm. Bull. 12, 1338.
Paudler, W. W., and Helmiek, L. S. (1966)J. Hetero. Chem. 3, 269.
Paudler, W. W., Van Dahm, R. A., and Park, Y. N. (1972)J. Hetero. Chem. 9, 81.
Shaw, J. T., O'Connor, M. E., and Allen, R. C. (1979)J. Hetero. Chem. 11, 627.
Stefaniak, L., Roberts, J. D., Witanowski, M., and Webb, G. A. (1984a)Org. Magn. Reson. 22, 201.
Stefaniak, L., Roberts, J. D., Witanowski, M., Hamdi, B. T., and Webb, G. A. (1984b)Org. Magn. Reson. 22, 209.
Stefaniak, L., Roberts, J. D., Witanowski, M., and Webb, G. A. (1984c)Org. Magn. Reson. 22, 215.
Stefaniak, L., Witanowski, M., Hamdi, B. T., and Webb, G. A. (1983)Bull. Pol. Ac. Sci. Chem. 31, 93.
Stefaniak, L., Witanowski, M., Webb, G. A., and Smith, W. B. (1987)Bull. Pol. Ac. Sci. Chem. 35, 301.
Temple, C., McKee, R. L., and Montgomery, J. A. (1965)J. Org. Chem. 30, 829.
Witanowski, M., Stefaniak, L., and Webb, G. A. (1986)Annual Reports on NMR Spectroscopy, Webb, G. A., Ed. (Academic Press, London), vol. 18, pp. 1–761.
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Stefaniak, L., Witanowski, M., Mahmoud, U. et al. Nitrogen NMR studies on some fused ring N-heterocycles. Journal of Crystallographic and Spectroscopic Research 19, 159–166 (1989). https://doi.org/10.1007/BF01160852
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DOI: https://doi.org/10.1007/BF01160852