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Evaluation of SafTestTM methods for monitoring frying oil quality

  • Published:
Journal of the American Oil Chemists' Society

Abstract

The feasibility of applying methods developed by Safety Associates, Inc., to monitor oil degradation products, including malondialdehydes (AldeSafeTM), FFA (FASafeTM), and peroxides (PeroxySafeTM), in fresh and heat-abused deep-fat frying oil was evaluated. Based on performance qualification studies, the AldeSafe method was the most suitable SafTestTM assay for monitoring the quality of frying oil because of its high accuracy, precision, linearity, and reproducibility, and low detection/quantitation limits. A strong correlation (r=0.924) between the AldeSafe method and its counterpart, AOCS Official Method Cd 19-90, also supported the suitability of the SafTest method for monitoring oil quality. Moreover, the FASafe method had a moderately strong relationship with AOCS Official Method Ca 5a-40 (r=0.761). Our studies suggest that this test can be applied for monitoring frying oil; however, certain method performance limitations must be considered for routine analysis purposes. In contrast, the PeroxySafe method probably should not be used to monitor heat-abused oil without further development because of high variability, low accuracy, and low correlation (r=0.062) with the AOCS Official Method Cd 8-53 assay.

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References

  1. Paul, S., and G.S. Mittal, Regulating the Use of Degraded Oil/Fat in Deep-Fat/Oil Food Frying, Crit. Rev. Food Sci. Nutr. 37:635–643 (1997).

    Article  CAS  Google Scholar 

  2. White, P.J., Methods for Measuring Changes in Deep-Fat Frying Oils, Food Technol. 45:75–80 (1991).

    CAS  Google Scholar 

  3. Clark, W.L., and G. Serbia, Safety Aspects of Frying Fats and Oils, 45:84–89 (1991).

    Google Scholar 

  4. Dina, D., and S.I. Saguy, Frying of Nutritious Foods: Obstacles and Feasibility, Food Sci. Technol. Res. 7:265–279, 2001.

    Google Scholar 

  5. Stier, R.F., M.K. Gupta, K. Warner, and P.J. White, Toxicology of Frying Fats, in Frying Technology and Practices, AOCS Press, Champaign, 2004, pp. 178–199.

    Google Scholar 

  6. Gerhard, B., Health Aspects of Thermooxidized Oils and Fats, Eur. J. Lipid Sci. Technol. 102:587–593 (2000).

    Article  Google Scholar 

  7. Guillen-Sans, R., and M. Guzman-Chozas, The Thiobarbituric Acid (TBA) Reaction in Foods: A Review, Crit. Rev. Food Sci. Nutr. 38:315–330 (1998).

    Article  CAS  Google Scholar 

  8. Nawar, W., Lipids, in Food Chemistry, edited by O. Fennema, Marcel Dekker, New York, 1996, pp. 225–320.

    Google Scholar 

  9. AOCS, Official Methods and Recommended Practices of the American Oil Chemists’ Society, 5th edn., AOCS Press, Champagin, 1998, Method Cd 8-53.

    Google Scholar 

  10. AOCS,, Method Cd 19-90.

    Google Scholar 

  11. AOCS,, Method Ca 5a-40.

    Google Scholar 

  12. Fernandez, J., J. Perez-Alvarez, and J. Fernandez-Lopez, Thiobarbituric Acid Test for Monitoring Lipid Oxidation in Meat, Food Chem. 59:345–353 (1997).

    Article  CAS  Google Scholar 

  13. Rosell, J., Measurement of Rancidity, in Rancidity in Foods, edited by J. Allen and R. Hamilton, Blackie Academic, London, 1994, pp. 22–32.

    Google Scholar 

  14. The SafTest TM System: Rapid Standardized Testing for the Food Industry, Safety Associates Inc., Tempe, AZ, 2000.

  15. Younathan, M.T., B.G. Tarladgis, and B.M. Watts, Distillation Method for the Quantitative Determination of Malondialdehyde in Rancid Foods, J. Am. Oil Chem. Soc. 37:44–48 (1960).

    Google Scholar 

  16. Validation of Compendial Methods, in United States Pharmacopoeia and National Formulary, United States Pharmacopoeial Convention, Rockville, MD, 1995, pp. 1982–1984.

Download references

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Correspondence to Vicki Schlegel.

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Yee Foo, S., Cuppett, S. & Schlegel, V. Evaluation of SafTestTM methods for monitoring frying oil quality. J Amer Oil Chem Soc 83, 15–20 (2006). https://doi.org/10.1007/s11746-006-1169-z

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  • DOI: https://doi.org/10.1007/s11746-006-1169-z

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