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Bestimmung von Permethrin in Holz – Ergebnisse von Vergleichsanalysen

Determination of Permethrin in timber – results of comparative analyses

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Zusammenfassung

Vergleichsanalysen zur Bestimmung von Permethrin aus Holz ergaben, dass sich sowohl Extraktion mit Methanol im Ultraschallverfahren als auch Soxhlet-Extraktion mit Ethylacetat gut eignen, um Permethrin aus behandeltem Holz zu lösen. Verschiedene andere Extraktionsverfahren führen zu Minderbefunden. Zur quantitativen Bestimmung von Permethrin können sowohl Hochdruckflüssigchromatographie als auch Gaschromatographie eingesetzt werden.

Abstract

Parallel experiments to analyse permethrin in treated timber demonstrated that extraction with methanol by sonication as well as Soxhlet extraction with ethyl acetate are suitable methods to dissolve permethrin from treated wood. Several other extraction methods yield low recoveries. Quantification of permethrin can be realised by either high performance liquid chromatography or gas chromatography.

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Authors and Affiliations

  1. Bundesanstalt für Materialforschung u. -prüfung, Unter den Eichen 87, 12205, Berlin, Germany

    U. Schoknecht

  2. Holzforschung Austria, Franz-Grill-Straße 7, 1031, Wien, Austria

    C. Fürhapper

  3. Fraunhofer Wilhelm-Klauditz-Institut, Bienroder Weg 54 E, 38108, Braunschweig, Germany

    J. Gunschera

  4. Rütgers Organics GmbH, Sandhofer Straße 96, 68305, Mannheim, Germany

    H. Härtner

  5. Staatliche Materialprüfanstalt Darmstadt, TU Darmstadt, Grafenstraße 2, 64283, Darmstadt, Germany

    R. Hill

  6. Bundesforschungsanstalt für Forst- u. Holzwirtschaft, Leuschnerstraße 91, 21031, Hamburg, Germany

    E. Melcher

  7. Sachverständigenbüro Marx, Türkenloisstraße 5, 77851, Bühl-Vimbuch, Germany

    G. Schwarz

  8. Lanxess Deutschland GmbH, Rheinuferstraße 7–9, 47829, Uerdingen, Germany

    P. Spetmann

  9. Remmers Baustofftechnik GmbH, Bernhard-Remmers-Straße 13, 49624, Löningen, Germany

    U. Wilken

  10. Dr. Wolman GmbH, Dr.-Wolman-Straße 31–33, 76547, Sinzheim, Germany

    J. Wittenzellner

  11. Materialprüfanstalt für das Bauwesen, TU Braunschweig, Beethovenstraße 52, 38106, Braunschweig, Germany

    M. Wobst

Authors
  1. U. Schoknecht
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  2. C. Fürhapper
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  3. J. Gunschera
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  4. H. Härtner
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  5. R. Hill
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  6. E. Melcher
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  7. G. Schwarz
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  8. P. Spetmann
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  9. U. Wilken
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  10. J. Wittenzellner
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  11. M. Wobst
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Corresponding author

Correspondence to U. Schoknecht.

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Schoknecht, U., Fürhapper, C., Gunschera, J. et al. Bestimmung von Permethrin in Holz – Ergebnisse von Vergleichsanalysen . Holz Roh Werkst 66, 57–61 (2008). https://doi.org/10.1007/s00107-007-0208-2

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  • DOI: https://doi.org/10.1007/s00107-007-0208-2

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