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Sorption of Amphenicols on Magnetic Hypercrosslinked Polystyrene

  • PHYSICAL CHEMISTRY OF NANOCLUSTERS AND NANOMATERIALS
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Abstract

A study is performed of the sorption of chloramphenicol, florfenicol, and thiamphenicol on magnetic hypercrosslinked polystyrene (HCPS/Fe3O4). Magnetic HCPS is obtained via the sorption of Fe3O4 nanoparticles on commercially available HCPS Diapak P-3. The specific surface areas and parameters of the porous structure of the magnetic HCPS are determined by means of low-temperature nitrogen adsorption. It is found that introducing Fe3O4 nanoparticles into the HCPS matrix slightly lowers the specific surface area of the sorbent (from 1132 to 1080 m2/d) and the volume of pores, but these characteristics are strong enough to use the resulting composite as a sorbent. It is established that the HCPS-based magnetic sorbent exhibits superparamagnetic properties. The saturation magnetization is 1.7 emu/g, enough to extract the sorbent from the solution under the action of the magnetic field of a permanent magnet. It is shown that magnetic HCPS can be used for the group sorption concentration of amphenicols via magnetic solid-phase extraction.

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Funding

This work was financed by the Russian Science Foundation, grant no. 18-73-10001 (https://rscf.ru/en/project/18-73-10001/).

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Authors and Affiliations

  1. Department of Chemistry, Lomonosov Moscow State University, 119991, Moscow, Russia

    V. V. Tolmacheva, V. Yu. Savinova, N. O. Goncharov, S. G. Dmitrienko, V. V. Apyari, P. A. Chernavsky & G. V. Pankina

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  1. V. V. Tolmacheva
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  2. V. Yu. Savinova
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  3. N. O. Goncharov
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  4. S. G. Dmitrienko
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  5. V. V. Apyari
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  6. P. A. Chernavsky
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  7. G. V. Pankina
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Correspondence to V. V. Tolmacheva.

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Tolmacheva, V.V., Savinova, V.Y., Goncharov, N.O. et al. Sorption of Amphenicols on Magnetic Hypercrosslinked Polystyrene. Russ. J. Phys. Chem. 96, 1268–1272 (2022). https://doi.org/10.1134/S0036024422060267

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  • DOI: https://doi.org/10.1134/S0036024422060267

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