Skip to main content
Log in

Specialized Methods of Thermal Treatment of Riverine and Marine Suspensions Preparatorily to Their Analysis for Trace Concentrations of Chemical Elements

  • Short Communications
  • Published:
Geochemistry International Aims and scope Submit manuscript

Abstract

The paper considerations of the possibility of the low-temperature (1000°C) and high-temperature (>1500°C) thermal decomposition of solid samples of suspensions and the selective fractional evaporation–condensation of elements in specialized electrothermal crucible and rod atomizers for the purposes of direct atomic-absorption analysis. The approach is applied to analyze samples of riverine and marine suspensions for Ag, Cd, and Tl.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

References

  • V. V. Gordeev and V. N. Oreshkin, “Silver, cadmium, and lead in the waters, tributaries, and an estuary of the Amazon River,” Geokhimiya (2), 244–256 (1990).

    Google Scholar 

  • V. V. Gordeev, Geochemistry of the River–Sea System (IPMatushkina, Moscow, 2012) [in Russian].

    Google Scholar 

  • K. Govindaraju, “Compilation of working values and sample description for 272 geostandards,” Geostand. Newslet. 13 (Special Ed.), 1–113 (1989).

    Article  Google Scholar 

  • Yu. A. Karpov and A. P. Savostin, Methods of Sampling and Sample Preparation (BINOM, Laboratoriya Znanii, Moscow, 2003) [in Russian].

    Google Scholar 

  • I. V. Kubrakova T. F. Kudinova, A. A. Formanovsky, H. M. Kuzmin, G. I. Tsisin, and Yu. A. Zolotov, “Determination of chromium (III) and chromium (VI) in river water by electrothermal atomic absorption spectrometry after sorption preconcentration in microwave field,” Analyst 119 (11), 24–27 (1994).

    Article  Google Scholar 

  • K. Yu. Nagulin, I. V. Tsivil’skii, R. I. Nazmiev, and A. Kh. Gil’mutdinov, “Numerical simulation of thermal and gas-geodynamic processes in the two-stage atomizer for analytical spectrometry,” Optich. Zh. 79 (12), 46–55 (2012).

    Google Scholar 

  • V. N. Oreshkin and G. I. Tsizin, “Atomic absorption determination of elements in natural samples using a vaporization crucible with two condensation zones,” J. Analyt. Chem. 67 (10), 830–833 (2012).

    Article  Google Scholar 

  • V. N. Oreshkin and G. I. Tsizin, “Electrothermal atomic absorption determination of elements in natural waters and particulates after extraction of concentrates on the membrane filters,” Zavod. Lab. Diagnost. Material. 79 (3), 16–18 (2013).

    Google Scholar 

  • V. N. Oreshkin and G. I. Tsizin, “Sorption–atomic absorption determination of metal ultratraces in marine and river particulate matter,” Geochem. Int. 41 (3), 345–349 (2003).

    Google Scholar 

  • V. N. Oreshkin and Uu. G. Tatsy, “Direct atomic absorption determination of mercury traces in solid geochemical samples,” in Mercury in the Biosphere: Ecological–Geochemical Aspects (GEOKHI RAS, Moscow, 2010), pp. 372–376.

    Google Scholar 

  • V. N. Oreshkin, G. I. Tsizin, and G. L. Vnukovskaya, “Sorption–atomic absorption determinations of metal traces (Ag, Bi, In, Cd, Pb, and Tl) in marine and river waters using two-chamber powder atomizer,” Zh. Analit. Chem. 49 (7), 755–759 (1994).

    Google Scholar 

  • V. N. Oreshkin, G. I. Tsizin, and Yu. A. Zolotov, “Sorption–atomic absorption determination of trace elements in natural waters with dynamic preconcentration in electrothermal atomizers,” J. Analit. Chem. 57 (9), 778–783 (2002).

    Article  Google Scholar 

  • V. N. Oreshkin, Yu. I. Belyaev, and G. L. Vnukovskaya, “Atomizer of powders of geochemical samples and environmental objects for direct atomic absorption analysis,” Zavod. Lab. 56 (12), 50–53 (1990).

    Google Scholar 

  • V. N. Oreshkin, Yu. I. Belyaev, Yu. G. Tatsy, and G. L. Vnukovskaya, “Electrothermal atomizer for nonflame atomic absorption analysis,” Byul. Izobret. 48, 291 (1986).

    Google Scholar 

  • A. A. Pupyshev, Atomic Absorption Spectral Analysis (Tekhnosfera, Moscow, 2009) [in Russian].

    Google Scholar 

  • V. S. Savenko, Chemical Composition of Suspended Sediments of Rivers and Seas (GEOS, Moscow, 2006) [in Russian]

    Google Scholar 

  • Yu. A. Zakharov, O. B. Kokorina, Yu. V. Lysogorskii, and A. E. Staroverov, “Computer simulation of two-step atomization in graphite furnaces for analytical atomic spectrometry,” J. Analyt. Chem. 67 (8), 714–721 (2012).

    Article  Google Scholar 

  • Kh. I. Zil’bershtein, M. P. Semov, O. N. Nikitina, and Z. G. Fratikin, Spectral Analysis of Pure Substances (Khimiya, Leningrad, 1971) [in Russian].

    Google Scholar 

  • Yu. A. Zolotov, G. I. Tsizin, S. G. Dmitrienko, and E. I. Morosanova, Sorption Concentration of Trace Components from Solutions (Nauka, Moscow, 2007) [in Russian].

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to V. N. Oreshkin.

Additional information

Original Russian Text © V.N. Oreshkin, G.I. Tsizin, Yu.G. Tatsii, 2018, published in Geokhimiya, 2018, No. 3, pp. 290–295.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Oreshkin, V.N., Tsizin, G.I. & Tatsii, Y.G. Specialized Methods of Thermal Treatment of Riverine and Marine Suspensions Preparatorily to Their Analysis for Trace Concentrations of Chemical Elements. Geochem. Int. 56, 276–281 (2018). https://doi.org/10.1134/S0016702918030060

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1134/S0016702918030060

Keywords

Navigation