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Spectroscopic analysis and nuclear magnetic resonance for silver nanoparticles synthesized with trans-resveratrol and cis-resveratrol

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Abstract

The synthesis of silver nanoparticles with polyphenolic molecules (AgResvNPs) is important due to potential applications as nanocarriers of resveratrol. Silver nanoparticles were synthesized with trans-3,5,4′-trihydroxystilbene (resveratrol) and irradiated under UV light. Further AgResvNPs were characterized by transmission electron microscopy (TEM), energy-dispersive X-ray spectroscopy (EDS), selected area electron diffraction (SAED), UV–Vis spectroscopy, Fourier transform infrared spectroscopy (FTIR), Raman spectroscopy with surface-enhanced Raman scattering (SERS), nuclear magnetic resonance (NMR), zeta potential, and dynamic light scattering (DLS) and study of aggregation kinetic and colloidal stability for this system in water and s-DMEM and evaluate the antioxidant capacity with total phenols count assay. Ultraviolet light irradiation promotes the synthesis of AgResvNPs and modifies the conformational structure of resveratrol. NMR confirmed these changes structurally in the molecule. Applications in SERS are an important application of this system.

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Acknowledgements

BERV would like to thank Conacyt for Doctoral Fellowship number 722868.

Funding

TEM analysis was supported by LUME, Laboratorio Universitario de Microscopía Electrónica del Instituto de Investigaciones en Materiales, Universidad Nacional Autónoma de México.

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Authors and Affiliations

  1. Departamento de Investigación en Polímeros Y Materiales, Universidad de Sonora, Rosales and Transversal, 83000, Hermosillo, Sonora, Mexico

    Blanca E. Rodríguez Vázquez, Hisila Santacruz-Ortega, Yedith Soberanes & Rosa Elena Navarro

  2. Departamento de Física, Universidad de Sonora, Rosales and Transversal, 83000, Hermosillo, Sonora, Mexico

    Cesar Rodríguez-Beas, Ramón Alfonso Iñiguez-Palomares & Ericka Rodríguez-León

  3. Instituto de Investigaciones en Materiales, Universidad Nacional Autónoma de México, 04510, Ciudad de Mexico, Mexico

    Rubén Mendoza-Cruz & Lourdes Soledad Bazán-Díaz

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  1. Blanca E. Rodríguez Vázquez
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  2. Cesar Rodríguez-Beas
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Correspondence to Ericka Rodríguez-León or Rosa Elena Navarro.

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Vázquez, B.E.R., Rodríguez-Beas, C., Iñiguez-Palomares, R.A. et al. Spectroscopic analysis and nuclear magnetic resonance for silver nanoparticles synthesized with trans-resveratrol and cis-resveratrol. Colloid Polym Sci 300, 465–475 (2022). https://doi.org/10.1007/s00396-022-04957-3

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  • DOI: https://doi.org/10.1007/s00396-022-04957-3

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