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Reaction of nickel β-aminovinyl-ketonates with stationary liquid phases

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Bulletin of the Academy of Sciences of the USSR, Division of chemical science Aims and scope

Conclusions

  1. 1.

    In the gas-liquid chromatography of microquantities of nickel β-aminovinyl-ketonates, the interphase adsorption does not introduce an appreciable contribution to the retention data.

  2. 2.

    The influence of the enthalpy and entropy factors on the dissolution of fluoroalkyl-containing nickel β-aminovinyl-ketonates in stationary liquid phases was analyzed, and it was shown that entropy of solution plays a dominant role in the determination of the order of retention of these chelates on the siloxane phases, depending on the number of difluoromethylene groups in the chain.

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Authors and Affiliations

  1. Institute of Chemistry of the Ural Scientific Center, Academy of Sciences of the USSR, Sverdlovsk

    L. N. Bazhenova, V. E. Kirichenko, K. I. Pashkevich, I. P. Sereda & V. P. Mikhailenko

Authors
  1. L. N. Bazhenova
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  2. V. E. Kirichenko
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  3. K. I. Pashkevich
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  4. I. P. Sereda
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  5. V. P. Mikhailenko
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Additional information

Translated from Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, No. 4, pp. 741–745, April, 1987.

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Bazhenova, L.N., Kirichenko, V.E., Pashkevich, K.I. et al. Reaction of nickel β-aminovinyl-ketonates with stationary liquid phases. Russ Chem Bull 36, 670–673 (1987). https://doi.org/10.1007/BF00962294

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  • DOI: https://doi.org/10.1007/BF00962294

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