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Parfumine

Reference work entry

CAS Registry Number: 28230-70-8 Open image in new window

Taxonomy: Physicochemical and Pharmacological Properties of Alkaloids – Isoquinoline Alkaloids

Biological sources: Fumaria parviflora, F. vaillantii

C20H19NO5: 353.1263

Mp: 111–112°C (dec.)

[α]D +18° (CHCl3) [1]

Solubility: spar. sol. Me2CO, Et2O; very sol. EtOH, CHCl3 [1]

UV: 235, 260, 290, 358 [1]

IR: 3420, 3100, 1710, 1610, 1505, 1030, 920 [1]

MSm/z: 353(M+), 338, 324, 308 [1]

1H NMR: 2.27(3H, s, NCH3), 2.60–3.60(6H, m), 3.71(3H, s, OCH3), 6.03(2H, s, CH2O2), 6.18, 6.48(each 1H, s, p–H–Ar), 6.77, 6.99(each 1H, d, J = 8, o–H–Ar) [1]

X-ray: [2]

HPLC: [3]

References

  1. 1.
    I.A. Israilov, M.S. Yunusov, S.Yu. Yunusov, DAN SSSR 189, 1262 (1969)Google Scholar
  2. 2.
    S.M. Nasirov, L.G. Kuz’mina, Yu.T. Struchkov, I.A. Israilov, M.S. Yunusov, S.Yu. Yunusov, Chem. Nat. Comp. 16, 55 (1980)Google Scholar
  3. 3.
    I. Valka, V. Simanek, J. Chromatogr. 445, 258 (1988)Google Scholar

Copyright information

© Springer Science+Business Media New York 2013

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