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Folimine

Reference work entry

CAS Registry Number: 3148-24-1 Open image in new window

Taxonomy: Physicochemical and Pharmacological Properties of Alkaloids – Quinoline Alkaloids

Biological sources: Haplophyllum bungei, H. dauricum, H. foliosum, H. obtusifolium, H. perforatum

C12H13NO3: 219.0895

Mp: 139–140°C (C6H6-pet. ether.), 172°C (hydrochloride), 194°C (picrate) [1]

Solubility: sol. CHCl3, MeOH, EtOH [1]

UV: 214, 234, 253, 267 sh, 282 sh, 328 (4.40. 4.49, 4.44, 3.88, 3.80, 3.48) [2, 3]

IR: 1649, 1590, 1580, 1490, 1470, 1398, 1240 [3]

MSm/z: 219(M+, 100), 218(13), 204(93), 189(41), 174(54) [1]

1H NMR: 3.80(9H, s, NCH3, 2 × OCH3), 5.94(1H, s, H-3), 6.97(2H, m, H-7, H-6), 7.45(1H, dd, J = 9, 2.5, H-5) [1]

References

  1. 1.
    D.M. Razakova, I.A. Bessonova, S.Yu. Yunusov, Chem. Nat. Comp. 8, 139 (1972)Google Scholar
  2. 2.
    V.I. Pastukhova, G.P. Sidyakin, S.Yu. Yunusov, Chem. Nat. Comp. 1, 20 (1965)Google Scholar
  3. 3.
    R. Shakirov, M.V. Telezhenetskaya, I.A. Bessonova, S.F. Aripova, I.A. Israilov, M.N. Sultankhodzhaev, V.I. Vinogradova, V.I. Akhmedzhanova, T.S. Tulyaganov, B.T. Salimov, V.A. Tel’nov, Chem. Nat. Comp. 32, 932 (1996)Google Scholar

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© Springer Science+Business Media New York 2013

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