Folidine

Reference work entry

CAS Registry Number: 102719-91-5 Open image in new window

Taxonomy: Physicochemical and Pharmacological Properties of Alkaloids – Quinoline Alkaloids

Biological sources: Haplophyllum foliosum

C16H19NO4: 289.1314

Mp: 148–149°C (Me2CO-pet. ether.) [1]

Solubility: very sol. Et2O, CHCl3, Me2CO, EtOH; insol. H2O [1]

UV: 233, 249, 273, 286, 325 (3.42, 3.32, 2.89. 2.84, 2.60) [1]

IR: 1730, 1640, 1590, 1580, 1491, 1470, 1390 [1]

MSm/z: 289(M+, 89), 218(62), 205(59), 204(100), 71(26) [1]

1H NMR: 1.14(6H, d, J = 7.5, 2 × CH3), 2.80(1H, q, J = 7.5, CH), 4.78(2H, s, CH2O), 3.90, 3.94(each 3H, s, OCH3, NCH3), 6.08(1H, s, H-3), 6.85–7.45(2H, m, H-6, H-7), 7.72(1H, dd, J = 7.5, 3, H-5) [1]

References

  1. 1.
    V.I. Akhmedzhanova, I.A. Bessonova, S.Yu. Yunusov, Chem. Nat. Comp. 21, 782 (1985)Google Scholar

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© Springer Science+Business Media New York 2013

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