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Evodine

Reference work entry

CAS Registry Number: 6989-38-4 Open image in new window

Taxonomy: Physicochemical and Pharmacological Properties of Alkaloids – Quinoline Alkaloids

Biological sources: Haplophyllum ferganicum, H. obtusifolium, H. perforatum, H. ramosissimum

C18H19NO5: 329.1263

Mp: 152–153°C (Me2CO), 127°C (Ac) [1]

[α]D −60° (EtOH) [1]

Solubility: sol. CHCl3; spar. sol. Me2CO, Et2O; insol. H2O [1]

UV: 250, 323, 335 (4.56, 3.82, 3.80) [2]

IR: 3320, 3145, 1630, 1628, 1590, 1520, 1498 [2]

MSm/z: 329(M+, 78), 258(16), 245(50), 244(25), 227(100), 216(25), 71(7) [1]

1H NMR: 1.79(3H, s, CH3), 3.47(1H, OH), 3.94–4.54(3H, m, CH2–CH), 4.09, 4.34(each 3H, s, 2 × OCH3), 4.93, 5.09(each 1H, s, =CH2), 6.96, 7.52(each 1H, d, J = 3, H-3, H-2), 7.13, 7.90(each 1H, d, J = 9.4, H-6, H-5) [1]

References

  1. 1.
    V.I. Akhmedzhanova, I.A. Bessonova, S.Yu. Yunusov, Chem. Nat. Comp. 13, 254 (1977)Google Scholar
  2. 2.
    R. Shakirov, M.V. Telezhenetskaya, I.A. Bessonova, S.F. Aripova, I.A. Israilov, M.N. Sultankhodzhaev, V.I. Vinogradova, V.I. Akhmedzhanova, T.S. Tulyaganov, B.T. Salimov, V.A. Tel’nov, Chem. Nat. Comp. 32, 932 (1996)Google Scholar

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© Springer Science+Business Media New York 2013

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