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Edulinine

Reference work entry

CAS Registry Number: 27495-36-9 Open image in new window

Taxonomy: Physicochemical and Pharmacological Properties of Alkaloids – Quinoline Alkaloids

Biological sources: Haplophyllum foliosum

C16H21NO4: 291.1471

Mp: 141–142°C (Me2CO), 92°C (acetonide) [1]

UV: 230, 245 sh, 267 sh, 275, 285, 316 sh, 326, 337 (4.44, 4.02, 3.74, 3.86, 3.82, 3.72, 3.82, 3.69) [1]

IR: 3425, 3215, 1630, 1590, 1470, 1378, 1115, 765 [1, 2]

MSm/z: 276(1), 273(3), 258(2), 232(100), 203(58), 188(67), 160(8), 59(19) [1]

MS (acetonide) m/z: 331(M+, 5), 316(100), 274(23), 273(90), 258(16), 256(19), 232(6), 59(32) [1]

1H NMR: 1.26(6H, s, 2 × CH3), 2.67, 3.07, 3.56(each 1H, q, J = 13, 10, 2, CH2–CH–O), 3.68, 3.89(each 3H, OCH3, NCH3), 7.33(3H, m, H–Ar), 7.75(1H, d, J = 7.6, H-5) [1]

References

  1. 1.
    V.I. Akhmedzhanova, I.A. Bessonova, S.Yu. Yunusov, Chem. Nat. Comp. 16, 574 (1980)Google Scholar
  2. 2.
    R. Shakirov, M.V. Telezhenetskaya, I.A. Bessonova, S.F. Aripova, I.A. Israilov, M.N. Sultankhodzhaev, V.I. Vinogradova, V.I. Akhmedzhanova, T.S. Tulyaganov, B.T. Salimov, V.A. Tel’nov, Chem. Nat. Comp. 32, 932 (1996)Google Scholar

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© Springer Science+Business Media New York 2013

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