CAS Registry Number: 484-29-7
Taxonomy: Physicochemical and Pharmacological Properties of Alkaloids – Quinoline Alkaloids
Biological sources: Dictamnus angustifolius, D. caucasicus, Haplophyllum bucharicum, H. bungei, H. dauricum, H. obtusifolium, H. perforatum, H. ramosissimum, H. robustum, Ruta graveolens
C12H9NO2: 199.0633
Mp: 132–133°C (Me2CO), 170°C (hydrochloride), 163°C (picrate), 188°C (isodictamine) [1]
UV: 212 sh, 233, 242 sh, 299 sh, 307, 334, 358 (4.42, 4.59, 4.50, 3.34, 3.94, 3.59, 3.57) [2]
IR: 3145, 3120, 1623, 1580, 1510, 1470, 1450, 1370, 1266 [2]
MS m/z: 199(M+, 100), 184(70), 156(33), 140(4), 128(26), 101(11), 76(7) [2]
1 H NMR: 4.30(3H, s, OCH3), 6.90, 7.48(each 1H, d, J = 2.5, H-3, H-2), 7.20–8.00(3H, m, H–Ar), 8.10(1H, dd, J = 8.2, 2, H-5) [2]
13 C NMR: [3]
Table 1
C-2 |
143.6 |
C-4 |
122.4 |
C-7 |
129.6 |
 2a |
− |
 4a |
− |
 8 |
127.9 |
 3 |
104.7 |
 5 |
122.4 |
 8a |
− |
 3a |
− |
 6 |
123.7 |
4-OCH3 |
59.0 |
HPLC: [4]
Pharm./Biol.: 0.05–0.055 mg/kg – death of the animal with symptoms of asphyxia; 0.001...
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References
D. Kurbanov, G.P. Sidyakin, S.Yu. Yunusov, Chem. Nat. Comp. 3, 56 (1967)
R. Shakirov, M.V. Telezhenetskaya, I.A. Bessonova, S.F. Aripova, I.A. Israilov, M.N. Sultankhodzhaev, V.I. Vinogradova, V.I. Akhmedzhanova, T.S. Tulyaganov, B.T. Salimov, V.A. Tel’nov, Chem. Nat. Comp. 32, 386 (1996)
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F.S. Sadritdinov, A.G. Kurmukov, The Pharmacology of the Plant Alkaloids and Their Use in Medicine [in Russian] (UzSSR, Tashkent, 1980), p. 269
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(2013). Dictamnine. In: Azimova, S.S., Yunusov, M.S. (eds) Natural Compounds. Springer, New York, NY. https://doi.org/10.1007/978-1-4614-0560-3_1120
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