Taxonomy: Physicochemical and Pharmacological Properties of Sesquiterpene Esters – The Monocyclic Sesquiterpene Esters – Humulanes – Monoesters
Biological sources: Ferula haussknechtii Wolff. ex Rech. [1]
C23H30O4: 370.2144
Mp: gum [1]
IR (NaCl): 3400, 3080, 2975, 2938, 2870, 1710, 1610, 1600, 1515, 1460, 1450, 1428, 1283, 1220, 1105, 1030, 880, 830, 785, 762, 725 [1]
EI-MS: 370 [M]+ (4), 202 (13.9), 187 (11.6), 168 (18), 159 (15.8), 151 (100) [1]
1 H NMR (500 MHz, CDCl3, TMS): 1.07 (3H, s, H-13), 1.16 (3H, s, H-12), 1.48 (3H, d, J = 1.1, H-14), 1.58 (1H, m, H-9b), 1.92 (1H, m, H-8b), 2.17 (1H, m, H-9a), 2.22 (1H, m, H-2a), 2.24 (1H, m, H-8a), 2.33 (1H, m, H-2b), 2.38 (2H, m, H-3), 4.68 (1H, br d, J = 6.9, H-7), 4.90 (1H, d, J = 2.1, H-15b), 4.96 (1H, d, J = 2.1, H-15a), 5.32 (1H, br t, J = 8.5, H-1), 5.59 (1H, d, J = 16.1, H-6), 6.04 (1H, d, J = 16.1, H-5); OVan: 3.95 (3H, s, OCH3), 6.96 (1H, d, J = 8.3, H-5′), 7.62 (1H, d, J = 1.8, H-2′), 7.66 (1H, dd, J = 1.8; 8.3, H-6′) [1]
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References
M. Miski, T.J. Mabry, O. Saya, Phytochemistry 26(6), 1733 (1987)
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(2013). 7β-Vanilloyloxy-humula-1(10)Z,5E,4(15)-triene (Fervanol Vanillate). In: Azimova, S.S., Saidkhodzhaev, A.I. (eds) Natural Compounds. Springer, New York, NY. https://doi.org/10.1007/978-1-4614-0539-9_781
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