Taxonomy: Physicochemical and Pharmacological Properties of Sesquiterpene Esters – The Bicyclic Sesquiterpene Esters – Eremophilanes – Furanoeremophilanes – Monoesters
C20H30O4: 334.2144
Mp: ca. 40°C [1]
UV (EtOH) 218 (ε 9100) [1]
IR (CCl4): 3570, 3500, 1725, 1640, 1565, 1245 [2]
MS: 334 [M]+ (C20H30O4), 159 (base peak) [2]
1 H NMR (CDCl3): 0.88 (3H, t, J = 5.5, H-15), 1.14 (3H, d, J = 7, H-14), 2.34 (1H, m, H-2′) [1]
1 H NMR (CDCl3): 0.83 (3H, d, J = 7.5, H-15), 1.25 (3H, s, H-14), 1.90 (3H, d, J = 1.5, H-11), 2.65 and 3.20 (each 1H, d, J = 17.5, H-9), ca. 3.3 (1H, br s, OH), 6.19 (1H, s, H-6), 7.07 (1H, m, H-12); OMeBu: 0.88 (3H, t, J = 5.5, H-4′), 1.14 (3H, d, J = 7, H-5′), 2.34 (1H, m, H-2′) [2]
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References
M. Tada, Y. Moriyama, Y. Tanahashi, T. Takahashi, M. Fukuyama, K. Sato, Tetrahedron Lett. 12, 4007 (1971)
M. Tada, Y. Moriyama, Y. Tanahashi, T. Takahashi, Bull. Chem. Soc. Jpn. 47, 1999 (1974)
F. Bohlmann, C. Zdero, M. Grenz, Chem. Ber. 107, 3928 (1974)
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(2013). 6β-(2′-Methylbutyroyloxy)-10β-hydroxy-furanoeremophilane. In: Azimova, S.S., Saidkhodzhaev, A.I. (eds) Natural Compounds. Springer, New York, NY. https://doi.org/10.1007/978-1-4614-0539-9_1240
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