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Synthesis and characterization of Fe-containing biphasic calcium phosphate ceramics

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Abstract

Three biphasic calcium phosphate (BCP) ceramics with various Fe contents (e.g., 0.66, 1.32, and 1.98 at.%) were prepared using wet chemical synthesis. X-ray diffraction (XRD), Fourier transform infrared (FTIR) spectroscopy, differential thermal analysis (DTA), thermogravimetric analysis (TG), scanning electron microscopy (SEM), and energy dispersive X-ray (EDX) spectroscopy techniques were used to characterize the as-prepared BCPs. The DTA and TG results show that the as-prepared samples are thermally stable. The addition of Fe affects significantly the lattice parameters, unit cell volume, and morphology. The EDX data confirm the introduction of Fe.

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Authors and Affiliations

  1. Department of Physics, Faculty of Science, Firat University, 23119, Elazig, Turkey

    Omer Kaygili

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  1. Omer Kaygili
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Correspondence to Omer Kaygili.

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Kaygili, O. Synthesis and characterization of Fe-containing biphasic calcium phosphate ceramics. J Aust Ceram Soc 55, 381–385 (2019). https://doi.org/10.1007/s41779-018-0245-9

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  • DOI: https://doi.org/10.1007/s41779-018-0245-9

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