Abstract
Previous studies have shown that strain-controlled cyclic stability was maintained in bulk Cu samples with highly oriented nanoscale twins. In order to explore the underlying fatigue mechanism, transmission electron microscopy observations under two-beam diffraction condition were utilized to characterize the dislocation configurations in the twin/matrix layers of as-fatigued nanotwinned Cu. It was clarified that the threading dislocations with Burgers vector parallel to twin boundaries are mainly active during fatigue. A three-dimensional stereo projection was re-configured for demonstrating the special structure of dislocations in nanoscale twins.
中文摘要
块体择优取向纳米孪晶Cu在应变疲劳时保持循环稳定. 为了研究其本征疲劳机制, 本文利用透射电子显微镜在双束条件下 研究了纳米孪晶Cu疲劳后孪晶片层内位错形貌特征. 结果表明纳米孪晶Cu的疲劳变形多由受限于孪晶片层内部的滑移方向平行于孪晶界面、 滑移面倾斜于孪晶界面的单滑移贯穿位错主导. 通过三维投影模型重构了贯穿位错在纳米孪晶片层内的空间分布.
References
Lu L, Shen YF, Chen XH, et al. Ultrahigh strength and high electrical conductivity in copper. Science, 2004, 304: 422–426
Lu K, Lu L, Suresh S. Strengthening materials by engineering coherent internal boundaries at the nanoscale. Science, 2009, 324: 349–352
Lu L, You ZS, Lu K. Work hardening of polycrystalline Cu with nanoscale twins. Scripta Mater, 2012, 66: 837–842
You ZS, Lu L, Lu K. Tensile behavior of columnar grained Cu with preferentially oriented nanoscale twins. Acta Mater, 2011, 59: 6927–6937
Shute CJ, Myers BD, Xie S, et al. Microstructural stability during cyclic loading of multilayer copper/copper samples with nanoscale twinning. Scripta Mater, 2009, 60: 1073–1077
Shute CJ, Myers BD, Xie S, et al. Detwinning, damage and crack initiation during cyclic loading of Cu samples containing aligned nanotwins. Acta Mater, 2011, 59: 4569–4577
Yoo BG, Boles ST, Liu Y, et al. Quantitative damage and detwinning analysis of nanotwinned copper foil under cyclic loading. Acta Mater, 2014, 81: 184–193
Pan QS, Lu QH, Lu L. Fatigue behavior of columnar-grained Cu with preferentially oriented nanoscale twins. Acta Mater, 2013, 61: 1383–1393
Pan QS, Lu L. Strain-controlled cyclic stability and properties of Cu with highly oriented nanoscale twins. Acta Mater, 2014, 81: 248–257
Suresh S. Fatigue of Materials (2nd ed.). Cambridge: Cambridge University Press, 1998
Mughrabi H, Höppel HW. Cyclic deformation and fatigue properties of very fine-grained metals and alloys. Int J Fatigue, 2010, 32: 1413–1427
Agnew SR, Vinogradov AY, Hashimoto S, et al. Overview of fatigue performance of Cu processed by severe plastic deformation. J Electron Mater, 1999, 28: 1038–1044
Höppel HW, Brunnbauer M, Mughrabi H. Cyclic deformation behaviour of utrafine-grained size copper produced by equal channel angular pressing. In: Werkstoffwoche-Partnerschaft (ed.), Proceedings of Materials Week 2000. Frankfurt, 2000, 1–8
Mughrabi H, Wang R. Cyclic deformation of face-centred cubic polycrystals: a comparison with observations on single crystals. In: Hansen N, Horsewell A, Leffers T, Lilholt H (eds.). Proceedings of the Second Risø International Symposium on Metallurgy and Material Science. Denmark: Risø National Laboratory, 1981, 87–98
Polák J, Klesnil M. Cyclic stress-strain response and dislocation structures in polycrystalline copper. Mater Sci Eng, 1984, 63: 189–196
Pedersen OB, Rasmussen KV, Winter AT. The cyclic stress-strain curve of polycrystals. Acta Metall, 1982, 30: 57–62
Williams DB, Carter CB. Transmission Electron Microscopy: A Textbook for Materials Science (2nd ed.). New York: Springer Science/Business Media, 2009
Nix W. Mechanical properties of thin films. Metall Trans A, 1989, 20: 2217–2245
Misra A, Hirth JP, Hoagland RG. Length-scale-dependent deformation mechanisms in incoherent metallic multilayered composites. Acta Mater, 2005, 53: 4817–4824
Winter AT, Pedersen OR, Rasmussen KV. Dislocation microstructures in fatigued copper polycrystals. Acta Metall, 1981, 29: 735–748
Guo XL, Lu L, Li SX. Effects of twin size on the dislocation configuration during cyclic deformation of polycrystalline twin copper. Acta Metall Sin, 2005, 41: 23–27
Author information
Authors and Affiliations
Corresponding author
Additional information
Qingsong Pan received his PhD degree in materials physics and chemistry at the Institute of Metal Research, Chinese Academy of Sciences, in 2014, and joined Professor Lei Lu’s group as an assistant professor. His research focuses on the fati gue behavior of nanotwinned metals.
Lei Lu is a professor at Shenyang National Laboratory for Materials Science at the Institute of Metal Research, Chinese Academy of Sciences. She is the member of International Community of Nanostructured Materials. Her research is focused on the fundamental study of the synthesis, microstructure characteristic and mechanical properties of nanostructured metallic materials. She authored and co-authored more than 80 international journal publications (including Science, Nature, Acta Mater, etc.) with total citations exceeding 5500.
Rights and permissions
About this article
Cite this article
Pan, Q., Lu, L. Dislocation characterization in fatigued Cu with nanoscale twins. Sci. China Mater. 58, 915–920 (2015). https://doi.org/10.1007/s40843-015-0104-8
Received:
Accepted:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s40843-015-0104-8