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Nano-sphere silica sulfuric acid: novel and efficient catalyst in the one-pot multi-component synthesis

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Abstract

In this report, synthesis, characterization and application of nano-sphere silica sulfuric acid as a novel and heterogeneous catalyst for the synthesis of β-acetamido ketone derivatives at room temperature are described. The catalyst has been identified using various techniques (XRD, SEM, TEM, EDX, TGA, FT-IR), and results show that it has a spherical shape and its particle size is between 60 and 90 nm.

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Acknowledgments

The authors gratefully acknowledge partial support of this work by the Research Affairs Office of Bu-Ali Sina University and Center of Excellence in Development of Chemical Method (CEDCM), Hamedan, I.R. Iran.

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Authors and Affiliations

  1. Faculty of Chemistry, Bu-Ali Sina University, P.O. Box 6517838683, Hamedan, Iran

    Ardeshir Khazaei, Mohammad Ali Zolfigol, Mohammad Mokhlesi & Rahele Rostamian

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  1. Ardeshir Khazaei
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  2. Mohammad Ali Zolfigol
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  3. Mohammad Mokhlesi
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  4. Rahele Rostamian
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Correspondence to Mohammad Mokhlesi.

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Khazaei, A., Zolfigol, M.A., Mokhlesi, M. et al. Nano-sphere silica sulfuric acid: novel and efficient catalyst in the one-pot multi-component synthesis. J IRAN CHEM SOC 10, 1297–1301 (2013). https://doi.org/10.1007/s13738-013-0272-y

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