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Synthesis of gold nanoparticles using Euphorbia tirucalli latex and the microwave method

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Abstract

Uniformly sized and shaped gold nanoparticles (AuNP) were produced by microwave irradiation using Euphorbia tirucalli latex. The AuNPs were characterized by ultraviolet visible spectroscopy (UV–Vis), Fourier transform infrared spectroscopy (FTIR), dynamic light scattering, zeta potential, and transmission electron microscopy (TEM). UV–Vis analysis was employed to detect the characteristic surface plasmon resonance pattern of the AuNPs (550 nm). The carboxylic and polyphenolic groups were associated with the euphol-capped AuNP, which was confirmed using FTIR spectroscopy. The AuNPs studied here show a z-average diameter varying from 35 to 500 ± 0.8 nm. TEM reveals that the particles were spherical and polydispersed. The latex itself is very toxic and can be harmful during manipulation, thus highlighting a negative aspect in it use. However, we have demonstrated that the isolation procedure did not impair the reduction action of the dry latex powder. This study provides a robust solution for the synthesis of stable capped gold nanoparticles. Furthermore, the dried powdered E. tirucalli latex seems to be an attractive capping agent for nanoparticles in drug delivery.

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Acknowledgments

The authors thank the Brazilian National Council for Scientific and Technological Development (CNPq), the Brazilian Coordination for the Improvement of Higher Educational Personnel (CAPES), the Federal District Research Foundation (FAPDF), and the University of Brasilia Grant Commissions for the financial support. The authors also thank the LabMic/UFG for conducting the TEM analysis.

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Authors and Affiliations

  1. Laboratory of Photochemistry and Nanobiotechnology, University of Brasilia, Brasilia, 72220-240, Brazil

    Claure N. Lunardi, Mirella P. F. Barros, Marina L. Rodrigues & Anderson J. Gomes

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  1. Claure N. Lunardi
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  2. Mirella P. F. Barros
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Correspondence to Claure N. Lunardi.

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Lunardi, C.N., Barros, M.P.F., Rodrigues, M.L. et al. Synthesis of gold nanoparticles using Euphorbia tirucalli latex and the microwave method. Gold Bull 51, 131–137 (2018). https://doi.org/10.1007/s13404-018-0231-6

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