Skip to main content
Log in

Tensile and plane bending fatigue properties of pure iron and iron-phosphorus alloys at room temperature in the air

  • Published:
Transactions of the Indian Institute of Metals Aims and scope Submit manuscript

Abstract

In many low alloys as well as in plain carbon steels, segregation of trace element, especially phosphorus (P), sulfur (S), arsenic (As), etc. is really a great problem. Because, it induces brittleness in the steels and subsequently causes deterioration in mechanical properties. In this present work, commercial grade of pure iron with varying amount of phosphorus contents such as 0.001, 0.11 and 0.21 wt% were annealed at different temperatures and time periods to induce varying degrees of temper embrittlement. After annealing heat treatment, tensile and plane bending fatigue tests of these ferrous alloys were carried out at room temperature in the air. The tensile and fatigue fracture surfaces were observed under scanning electron microscope (SEM) to study various fracture features. It has been found that the addition of phosphorus in the pure iron increased the tensile strength, however, it decreased the ductility. The grain refining effects and increase in tensile strength due to additions of P were found to be very significant. However, with increase in annealing time at any temperature, the mechanical properties were found to deteriorate gradually and the fatigue fracture mode was also found to change from its transgranular cleavage type to intergranular type fracture.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. Naudin N, Frund J M and Pineau A, Intergranular fracture Stress and Phosphorus Grain Boundary Segregation of a Mn-Ni-Mo Steel, Scripta Materiala, 40 (1999) 1013.

    Article  CAS  Google Scholar 

  2. Yu J and Jr. Mchahon C J, Effect of Composition and Carbide Precipitation on Temper Embrittlement of 2.25Cr-1Mo Steel: Part 1. Effect of P and Sn. Met. Trans, 11A, (1980) 277.

    CAS  Google Scholar 

  3. Thomson R C and Miller M K, Carbide Precipitation in Martensite During the Early Stages of Tempering in Cr-and-Mo-Containing Low Alloy Steels, Acta Mater, 46(6) 2203.

  4. Islam M A, Novovic M, Bowen P and Knott J F, Effect of Phosphorus Segregation on Fracture Properties of 2.25Cr-1Mo Pressure Vessel Steel, Journal of Materials Engineering and Performance, ASM International, 12(3) (2003) 244.

    Article  CAS  Google Scholar 

  5. Islam M A, Knott J F and Bowen P, Kinetics of phosphorus segregation and its effect on low temperature fracture behavior in 2.25Cr-1Mo pressure vessel steel, Journal of Materials Science and Technology, UK, 21(1) (2005) 76.

    Article  CAS  Google Scholar 

  6. Islam M A, Bowen P and Knott J F, Intergranular Fracture on Fatigue Fracture Surface of 2.25Cr-1Mo Steel at Room Temperature in Air, Journal of Materials Engineering and Performance, ASM International, 14(1) (2005) 28.

    Article  CAS  Google Scholar 

  7. Islam M A and Tomota Y, Plane Bending Fatigue Behavior of Interstitial Free Steel at Room Temperature, International Journal of Materials Research (formerly Metallkunde, German), 97(11) (2006) 1559.

    CAS  Google Scholar 

  8. Islam M.A and Tomota Y, Fatigue Strength and Fracture Mechanisms of IF28 Steels, Journal of Advanced Materials Research (Switzerland), 15–17 (2007) 804.

    Article  Google Scholar 

  9. Islam M A and Tomota Y, Fatigue strength and fracture behavior of steels with and without interstitial carbon at room temperature in air, Published in the International Journal of Materials Research (formerly Metallkunde, German), 98(3) (2007) 209.

    CAS  Google Scholar 

  10. Islam M A and Tomota Y, Investigation of Effects of Phosphorus on the Fatigue Life of Carbon Steels, Proceedings of International Conference of SPPM2010, held in Dhaka on 24–26 February, No.E19, 2010

  11. Islam M A, Nemoto T and Tomota Y, In-situ measurement of Fatigue Crack During Plane Bending Fatigue Test Without any Additional Set-up, Proceedings of International Conference of SPPM2010, held in Dhaka on 24–26 February, No.E19, 2010.

  12. Zhenyu N L, Qiu Y, Xiu L X and Wang G, Solidification Structure of Low Carbon Steel Strips with Different Phosphorus Contents Produced by Strip Casting, Journal of Materials Science and Technology, 22(6) (2006) 755.

    Google Scholar 

  13. Furuya Y, Matsuoka S, Shimakura S, Hanamura T and Torizuka S, Effects of Carbon and Phosphorus Addition on the Fatigue Properties of Ultra fine-grained Steels, Scripta Materiala, 52(11) (2005) 1163.

    Article  CAS  Google Scholar 

  14. Basu P C, Shylamoni P and Roshan A D, Characterization of Steel Reinforcement for RC Structures: An Overview and Related Issues, The Indian Concrete Journal, (2004) 18.

  15. Manna M, Chakrabarti I and Bandyopadhyay N, Phosphorus Treatment of TMT Rebar Bundle to avoid Early Rusting: An Option for Single Step Process, Journal of Surface and Coatings Technology, 201(3–4) (2006) 1583.

    Article  CAS  Google Scholar 

  16. Gadadhar S and Balsubramanium R, Studies on Phosphoric Irons for Concrete Reinforcement Applications, International Symposium of Research Students ISRS) on Material Science and Engineering, Held in Chennai, India, (2004) 1.

  17. Panigrahi B K, Srikanth S and Sahoo G, Effect of Alloying Elements on Tensile Properties, Microstructure and Corrosion Resistance of Reinforcing Bar Steel, JMEPEG, ASM International, 18 (2009) 1102.

    CAS  Google Scholar 

  18. Shin K S and Tsao, Scripta Metall. 22 (1988) 585.

    Article  CAS  Google Scholar 

  19. Gouthama and Balasubramaniam R, Bull. Mat. Sci. 26 (2003) 483.

    Article  CAS  Google Scholar 

  20. Rangarajan V, Toncheff R and Franks L L, Met. Mat. Trans. A 29A (1998) 2707.

    Article  CAS  Google Scholar 

  21. Maier P, Faulkner R G, Spellward P and Cowan J R, Mat. Sci. Tech, 17 (2001) 1377.

    CAS  Google Scholar 

  22. Islam M A, Embrittlement in Cr-Mo Steel, Ph.D. Thesis, The University of Birmingham, England, 2001.

    Google Scholar 

  23. http://resources.alibaba.com/topic/800012723/Phosphorus_on_non_alloy_electrical_steel_of_the_organization.htm.

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to M. A. Islam.

Rights and permissions

Reprints and permissions

About this article

Cite this article

Islam, M.A., Sato, N. & Tomota, Y. Tensile and plane bending fatigue properties of pure iron and iron-phosphorus alloys at room temperature in the air. Trans Indian Inst Met 64, 315–320 (2011). https://doi.org/10.1007/s12666-011-0064-y

Download citation

  • Received:

  • Revised:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s12666-011-0064-y

Keywords

Navigation