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Research on water retention and microstructure characteristics of compacted GMZ bentonite under free swelling conditions

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Abstract

In this study, water retention tests under free swelling conditions were performed to investigate the water intake (or loss) behaviour of compacted GMZ bentonite. First, the water retention characteristics were investigated, and then the microscopic pore structure was observed by environmental scanning electron microscope (ESEM). The results indicate that GMZ bentonite has a strong swelling (or a limited shrinkage ability) due to water intake (loss). The suction behaviour of GMZ bentonite is similar to MX80 bentonite and FEBEX bentonite. We also find that the confinement conditions can affect the suction behaviour of the material, especially at high relative humidity (RH). Additionally, a mathematic model can fit the mass change data very well. Microscopic tests show that the granular sensation of GMZ bentonite is obvious for a sample at low RH. With the increase in RH, the surface of GMZ bentonite becomes more smooth. The differences in the porosities calculated by the macroscopic and microscopic tests can be attributed to image resolution. The inter-laminar pores and intra-aggregate pores cannot be observed by the ESEM method. In addition, ESEM observation can provide an intuitive basis for the further research of the seepage property of GMZ bentonite.

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References

  • Agus SS, Schanz T, Fredlund DG (2010) Measurements of suction versus water content for bentonite-sand mixtures. Can Geotech J 47:583–594

    Article  Google Scholar 

  • Alonso EE, Romero E, Hoffmann C, García-Escudero E (2005) Expansive bentonite–sand mixtures in cyclic controlled-suction drying and wetting. Eng Geol 81:213–226

    Article  Google Scholar 

  • Blunt MJ, Bijeljic B, Hu D, Gharbi O, Iglauer S, Mostaghimi P, Paluszny A, Pentland C (2013) Pore-scale imaging and modeling. Adv Water Resour 51:197–216

    Article  Google Scholar 

  • Camillis MD, Emidio GD, Bezuijen A, Verástegui-Flores RD (2016) Hydraulic conductivity and swelling ability of a polymer modified bentonite subjected to wet–dry cycles in seawater. Geotext Geomembr 44:739–747

    Article  Google Scholar 

  • Cariou S, Dormieux L, Skoczylas F (2013) An original constitutive law for Callovo-Oxfordian argillite, a two-scale double-porosity material. Appl Clay Sci 81:18–30

    Article  Google Scholar 

  • Chen L, Liu YM, Wang J, Cao SF, Xie JL, Ma LK, Zhao XG, Li YW, Liu J (2014) Investigation of the thermal-hydro-mechanical (THM) behavior of GMZ bentonite in the China-Mock-up test. Eng Geol 172:57–68

    Article  Google Scholar 

  • Chen YG, Zhu CM, Ye WM, Cui YJ, Wang Q (2015) Swelling pressure and hydraulic conductivity of compacted GMZ01 bentonite under salinization–desalinization cycle conditions. Appl Clay Sci 114:454–460

    Article  Google Scholar 

  • Crank J (1975) The mathematics of diffusion, 2nd ed. WSEAS TRANSACTIONS on SYSTEMS and CONTROL Ahmet Kuzu, Metin Gokasan, Seta Bogosyan ISSN: 1991-8763, Issue 8(3):625–626

  • Cui S-L, Zhang H-Y, Zhang M (2012) Swelling characteristics of compacted GMZ bentonite–sand mixtures as a buffer/backfill material in China. Eng Geol 141–142:65–73

    Article  Google Scholar 

  • Hoffmann C, Alonso EE, Romero E (2007) Hydro-mechanical behaviour of bentonite pellet mixtures. Phys Chem Earth A/B/C 32:832–849

    Article  Google Scholar 

  • Horseman ST, Harrington JF, Sellin P (1999) Gas migration in clay barriers. Eng Geol 54:139–149

    Article  Google Scholar 

  • Komine H (2004) Simplified evaluation for swelling characteristics of bentonites. Eng Geol 71:265–279

    Article  Google Scholar 

  • Komine H (2010) Predicting hydraulic conductivity of sand-bentonite mixture backfill before and after swelling deformation for underground disposal of radioactive wastes. Eng Geol 114:123–134

    Article  Google Scholar 

  • Komine H, Ogata N (1994) Experimental study on swelling characteristics of compacted bentonite. Can Geotech J 31:478–490

    Article  Google Scholar 

  • Komine H, Ogata N (1999) Experimental study on swelling characteristics of sand-bentonite mixture for nuclear waste disposal. Soils Foundations 39:83–97

    Article  Google Scholar 

  • Li X, Kang Y, Haghighi M (2018) Investigation of pore size distributions of coals with different structures by nuclear magnetic resonance (NMR) and mercury intrusion porosimetry (MIP). Measurement 116:122–128

    Article  Google Scholar 

  • Liu J (2011) Etude expérimentale de la perméabilité relative des matériaux cimentaires et simulation numérique du transfert d’eau dans le béton. PhD thesis, Ecole Centrale De Lille

  • Liu JF, Davy CA, Talandier J, Skoczylas F (2014a) Effect of gas pressure on the sealing efficiency of compacted bentonite–sand plugs. J Contam Hydrol 170:10–27

    Article  Google Scholar 

  • Liu JF, Skoczylas F, Liu J (2014b) Experimental research on water retention and gas permeability of compacted bentonite/sand mixtures. Soils Found 54:1027–1038

    Article  Google Scholar 

  • Liu JF, Skoczylas F, Talandier J (2015) Gas permeability of a compacted bentonite–sand mixture: coupled effects of water content, dry density, and confining pressure. Can Geotech J 52:1159–1167

    Article  Google Scholar 

  • Liu JF, Wu Y, Cai CZ, Ni HY, Cao XL, Pu H, Song SB, Pu SY, Skoczylas F (2018) Investigation into water retention and gas permeability of Opalinus clay. Environ Earth Sci 77:213

    Article  Google Scholar 

  • Lloret A, Villar MV (2007) Advances on the knowledge of the thermo-hydro-mechanical behaviour of heavily compacted “FEBEX” bentonite. Phys Chem Earth A/B/C 32:701–715

    Article  Google Scholar 

  • Marcial D, Delage P, Yu JC (2002) On the high stress compression of bentonites. Can Geotech J 39:812–820

    Article  Google Scholar 

  • Houben ME, Desbois G, Urai JL (2013) Pore morphology and distribution in the Shaly facies of Opalinus Clay (Mont Terri, Switzerland): insights from representative 2D BIB–SEM investigations on mm to nm scale. Appl Clay Sci 71:82–97

    Article  Google Scholar 

  • Mishra AK, Ohtsubo M, Li L, Higashi T (2011) Controlling factors of the swelling of various bentonites and their correlations with the hydraulic conductivity of soil-bentonite mixtures. Appl Clay Sci 52:78–84

    Article  Google Scholar 

  • Sheng DS, Fredlund DGFG, Gens AG (2008) A new modelling approach for unsaturated soils using independent stres. Can Geotech J 45:511–534

    Article  Google Scholar 

  • Shirazi SM (2010) The influence of temperature on swelling characteristics of compacted bentonite for waste disposal. Environmentasia 3:284–286

    Google Scholar 

  • Song Y, Davy CA, Troadec D, Blanchenet AM, Skoczylas F, Talandier J, Robinet JC (2015) Multi-scale pore structure of COx claystone: towards the prediction of fluid transport. Marine Pet Geol 65:63–82

    Article  Google Scholar 

  • Tada S, Watanabe K (2005) Dynamic determination of sorption isotherm of cement based materials. Cem Concr Res 35:2271–2277

    Article  Google Scholar 

  • Villar MV, Lloret A (2007) Dismantling of the first section of the FEBEX in situ test: THM laboratory tests on the bentonite blocks retrieved. Phys Chem Earth 32:716–729

    Article  Google Scholar 

  • Villar MV, Lloret A (2008) Influence of dry density and water content on the swelling of a compacted bentonite. Appl Clay Sci 39:38–49

    Article  Google Scholar 

  • Wang Q, Tang AM, Cui YJ, Delage P, Gatmiri B (2012) Experimental study on the swelling behaviour of bentonite/claystone mixture. Eng Geol 124:59–66

    Article  Google Scholar 

  • Wang Q, Cui YJ, Tang AM, Barnichon JD, Saba S, Ye WM (2013) Hydraulic conductivity and microstructure changes of compacted bentonite/sand mixture during hydration. Eng Geol 164:67–76

    Article  Google Scholar 

  • Ye WM, Wan M, Chen B, Chen YG, Cui YJ, Wang J (2013) Temperature effects on the swelling pressure and saturated hydraulic conductivity of the compacted GMZ01 bentonite. Environ Earth Sci 68:281–288

    Article  Google Scholar 

  • Ye WM, Borrell NC, Zhu JY, Chen B, Chen YG (2014a) Advances on the investigation of the hydraulic behavior of compacted GMZ bentonite. Eng Geol 169:41–49

    Article  Google Scholar 

  • Ye WM, Zheng ZJ, Chen B, Chen YG, Cui YJ, Wang J (2014b) Effects of pH and temperature on the swelling pressure and hydraulic conductivity of compacted GMZ01 bentonite. Appl Clay Sci 101:192–198

    Article  Google Scholar 

  • Yen JC, Chang FJ, Chang S (1995) A new criterion for automatic multilevel thresholding. IEEE Trans Image Process 4:370–378

    Article  Google Scholar 

Download references

Acknowledgements

The authors are grateful to the support of the Fundamental Research Funds for the Central Universities (China University of Mining and Technology) (2017QNA29).

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Correspondence to Jiang-Feng Liu or Yong-Gui Chen.

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Liu, JF., Ni, HY., Chen, YG. et al. Research on water retention and microstructure characteristics of compacted GMZ bentonite under free swelling conditions. Environ Earth Sci 77, 583 (2018). https://doi.org/10.1007/s12665-018-7760-4

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  • DOI: https://doi.org/10.1007/s12665-018-7760-4

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