Abstract
In this paper we synthesized nickel ferrite nanoparticles by using a chemical method. Synthesized nanoparticles were characterized by using X-ray diffraction, Fourier transform infrared spectroscopy, vibrating sample magnetometer, transmission electron microscopy, and energy-dispersive X-ray spectroscopy. Magnetic properties, size, purity, stoichiometry and morphology of the samples were determined. Some samples were calcined at different temperatures. We found that the size of nanoparticles increased with the increase in calcination temperature and the nanoparticles transformed from amorphous phase to crystalline phase. When the size of nanoparticles decreased to less than a critical size (10 nm) the nanomaterial underwent a transition from a ferromagnetic to a superparamagnetic.
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G Mandal and T Ganguly Indian J. Phys. 85 1229 (2011)
S Mitra et al. Indian J. Phys. 85 649 (2011)
S Karan, D Dutta Majumder and A Goswami Indian J. Phys. 86 667 (2012)
J Bhadra and D Sarkar Indian J. Phys. 84 693 (2010)
M R Vaezi, S K Shendy and T Ebadzadeh Indian J. Phys. 86 9 (2012)
S Sarmah and A Kumar Indian J. Phys. 85 713 (2011)
S Devi and M Srivastva Indian J. Phys. 84 1561 (2010)
S Tekerek, A Kudret and Ü Alver Indian J. Phys. 85 1469 (2011)
K Maaz et al. J. Magn. Magn. Mater. 321 1838 (2009)
D Sellmyer and R Skomski Advanced Magnetic Nanostructures (New York: Springer) Ch 7, p 183 (2006)
B D Cullity and C D Graham Introduction to Magnetic Materials (New Jersey: Wiley) 2nd ed, Ch 11, p 360 (2009)
P Mallick, C Rath, R Biswal and N C Mishra Indian J. Phys. 83 517 (2009)
I M L Billas, A Chatelain and W A de Heer Science 265 1682 (1994)
A Ceylanab et al. J. Magn. Magn. Mater. 320 857 (2008)
S Son et al. J. Appl. Phys. 91 7589 (2002)
B Martinez et al. Phys. Rev. Lett. 80 181 (1998)
R D K Misra et al. Mater. Sci. Eng. B 111 164 (2004)
H Nathani, S Gubbala and R D K Misra Mater. Sci. Eng. B 121 126 (2005)
J Jacob and M Abdul Khadar J. Appl. Phys. 107 114310 (2010)
S Maensiri et al. Scr. Mater. 56 797 (2007)
J A C de Paiva et al. J. Alloys Compd. 485 637 (2009)
Acknowledgments
The authors are grateful to the University of Sistan and Baluchestan (Iran) for financial support.
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Aliahmad, M., Noori, M. Synthesis and characterization of nickel ferrite nanoparticles by chemical method. Indian J Phys 87, 431–434 (2013). https://doi.org/10.1007/s12648-013-0246-z
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DOI: https://doi.org/10.1007/s12648-013-0246-z