Skip to main content
Log in

High-Strength AZ91 Alloy Fabricated by Rapidly Solidified Flaky Powder Metallurgy and Hot Extrusion

  • Published:
Metals and Materials International Aims and scope Submit manuscript

Abstract

A high-strength AZ91 alloy is produced via hot extrusion using flakes fabricated through the rapidly solidified flaky powder metallurgy. The AZ91 alloy flakes have an extremely fine dendritic structure without any second-phase particles owing to the fast cooling rate during solidification; these microstructural features considerably promote dynamic recrystallization and precipitation behaviors during extrusion process. As a result, the AZ91 alloy extruded using the flakes exhibits an almost fully recrystallized microstructure with a very small average grain size of 1.2 µm owing to an increase in the number of nucleation sites for recrystallization, and it shows a high microstructural homogeneity owing to the numerous Mg17Al12 precipitates uniformly distributed throughout the material. This extruded AZ91 alloy has a tensile yield strength of 345 MPa, ultimate tensile strength of 417 MPa, and total elongation of 5.6%. These superior tensile strengths are mainly attributed to the combined effects of precipitation hardening caused by abundant fine precipitates and grain boundary hardening caused by fine recrystallized grains.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6

Similar content being viewed by others

References

  1. T. Homma, N. Kunito, S. Kamado, Scr. Mater. 61, 644–647 (2009)

    Article  Google Scholar 

  2. W.W. Jian, G.M. Cheng, W.Z. Xu, H. Yuan, M.H. Tsai, Q.D. Wang, C.C. Koch, Y.T. Zhu, S.N. Mathaudhu, Mater. Res. Lett. 1, 61–66 (2013)

    Article  Google Scholar 

  3. Y. Kawamura, K. Hayashi, A. Inoue, T. Masumoto, Mater. Trans. 42, 1172–1176 (2001)

    Article  Google Scholar 

  4. E. Ayman, U. Junko, K. Katsuyoshi, Acta Mater. 59, 273–282 (2011)

    Article  Google Scholar 

  5. K.S. Govind, M.C. Nair, K. Mittal, R.K. Lal, C.S. Mahanti, Sivaramakrishnan. Mater. Sci. Eng. A 304–306, 520–523 (2001)

    Article  Google Scholar 

  6. M. Yamasaki, N. Hayashi, S. Izumi, Y. Kawamura, Corros. Sci. 49, 255–262 (2007)

    Article  Google Scholar 

  7. H. Okouchi, Y. Seki, T. Sekigawa, H. Hira, Y. Kawamura, Mater. Sci. Forum 638–642, 1476–1481 (2010)

    Article  Google Scholar 

  8. G. Garcés, G. Requena, D. Tolnai, P. Pérez, J. Medina, A. Stark, N. Schell, P. Adeva, Mater. Charact. 118, 514–518 (2016)

    Article  Google Scholar 

  9. T. Lee, M. Yamasaki, Y. Kawamura, Y. Lee, C.S. Lee, Mater. Lett. 234, 245–248 (2019)

    Article  Google Scholar 

  10. M.Ş. Turhal, T. Savaşkan, J. Mater. Sci. 38, 2639–2646 (2003)

    Article  Google Scholar 

  11. F.C. Campbell, Phase Diagrams: Understanding the Basics (ASM International, Materials Park, 2012)

    Google Scholar 

  12. J. Campbell, Castings, 2nd edn. (Butterworth-Heinemann, Oxford, 2003)

    Google Scholar 

  13. T.Z. Kattamis, J.C. Coughlin, M.C. Flemings, Trans. Met. Soc. AIME 239, 1504–1511 (1967)

    Google Scholar 

  14. M.C. Zhao, M. Liu, G. Song, A. Atrens, Corros. Sci. 50, 1939–1953 (2008)

    Article  Google Scholar 

  15. J.Y. Li, J.X. Xie, Adv. Mater. Res. 264–265, 66–71 (2011)

    Google Scholar 

  16. J. Cai, G.C. Ma, Z. Liu, H.F. Zhang, A.M. Wang, Z.Q. Hu, Mater. Sci. Eng. A 456, 364–367 (2007)

    Article  Google Scholar 

  17. C. Bettles, M. Barnett, Advances in Wrought Magnesium Alloys: Fundamentals of Processing, Properties and Applications, 1st edn. (Woodhead Publishing, Philadelphia, 2012)

    Book  Google Scholar 

  18. Y. Chen, Q. Wang, J. Peng, C. Zhai, W. Ding, J. Mater. Process. Technol. 182, 281–285 (2007)

    Article  Google Scholar 

  19. S.H. Kim, J.U. Lee, Y.J. Kim, B.G. Moon, B.S. You, H.S. Kim, S.H. Park, Mater. Sci. Eng. A 703, 1–8 (2017)

    Article  Google Scholar 

  20. S.H. Park, J.H. Bae, S.H. Kim, J. Yoon, B.S. You, Metall. Mater. Trans. A 46, 5482–5488 (2015)

    Article  Google Scholar 

  21. G.E. Dieter, Mechanical Metallurgy, SI Metrix edition (McGraw-Hill, London, 1988)

    Google Scholar 

  22. S.W. Bae, S.H. Kim, J.U. Lee, W.K. Jo, W.H. Hong, W. Kim, S.H. Park, J. Alloys Compd. 766, 748–758 (2018)

    Article  Google Scholar 

  23. H.Y. Wang, J. Rong, G.J. Liu, M. Zha, C. Wang, D. Luo, Q.C. Jiang, Mater. Sci. Eng. A 698, 249–255 (2017)

    Article  Google Scholar 

  24. S.H. Kim, J.U. Lee, Y.J. Kim, J.G. Jung, S.H. Park, J. Alloys Compd. 751, 1–11 (2018)

    Article  Google Scholar 

  25. B. Wang, F. Pan, X. Chen, W. Guo, J. Mao, Mater. Sci. Eng. A 656, 165–173 (2016)

    Article  Google Scholar 

  26. Z. Yu, C. Xu, J. Meng, X. Zhang, S. Kamado, Mater. Sci. Eng. A 713, 234–243 (2018)

    Article  Google Scholar 

  27. S.H. Kim, J.G. Jung, B.S. You, S.H. Park, J. Alloys Compd. 695, 344–350 (2017)

    Article  Google Scholar 

  28. J.U. Lee, S.H. Kim, Y.J. Kim, S.H. Park, Mater. Sci. Eng. A 714, 49–58 (2018)

    Article  Google Scholar 

  29. K. Máthis, J. Gubicza, N.H. Nam, J. Alloys Compd. 394, 194–199 (2005)

    Article  Google Scholar 

  30. M. Mabuchi, Y. Chino, H. Iwasaki, T. Aizawa, K. Higashi, Mater. Trans. 42, 1182–1189 (2001)

    Article  Google Scholar 

  31. S.H. Kim, B.S. You, S.H. Park, J. Alloys Compd. 690, 417–423 (2017)

    Article  Google Scholar 

  32. B. Chen, D.L. Lin, L. Jin, X.Q. Zeng, C. Lu, Mater. Sci. Eng. A 483–484, 113–116 (2008)

    Article  Google Scholar 

  33. S.I. Wright, M.M. Nowell, D.P. Field, Microsc. Microanal. 17, 316–329 (2011)

    Article  Google Scholar 

  34. J. Bohlen, P. Dobroň, J. Swiostek, D. Letzig, F. Chmelík, P. Lukáč, K.U. Kainer, Mater. Sci. Eng. A 462, 302–306 (2007)

    Article  Google Scholar 

  35. C.H. Cáceres, C.J. Davidson, J.R. Griffiths, C.L. Newton, Mater. Sci. Eng. A 325, 344–355 (2002)

    Article  Google Scholar 

Download references

Acknowledgements

This work was supported by the National Research Foundation of Korea (NRF) grants funded by the Korean government (MSIP, South Korea) (Nos. 2016R1C1B2012140 and 2018R1C1B6002068).

Author information

Authors and Affiliations

Authors

Corresponding authors

Correspondence to Michiaki Yamasaki or Sung Hyuk Park.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Lee, T., Yamasaki, M., Kawamura, Y. et al. High-Strength AZ91 Alloy Fabricated by Rapidly Solidified Flaky Powder Metallurgy and Hot Extrusion. Met. Mater. Int. 25, 372–380 (2019). https://doi.org/10.1007/s12540-018-0204-6

Download citation

  • Received:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s12540-018-0204-6

Keywords

Navigation