Skip to main content
Log in

Hydrogen response of palladium nanoparticles washed with different solvents

  • Published:
Bulletin of Materials Science Aims and scope Submit manuscript

Abstract

Hydrogen sensor response of palladium (Pd) nanoparticles changes when the nanoparticles are washed with different solvents prior to device formation. This study presents the effect of washing Pd nanoparticles with distilled water or ethanol on their hydrogen response. The change induced in the surface characteristics of the Pd nanoparticles after washing is analysed with the help of UV–Vis absorption spectroscopy and glancing angle X-ray diffraction (GAXRD) studies. The nature of strain in nanoparticles after washing is particularly analysed from GAXRD data to understand the hydrogen response mechanism. The performance of the nanoparticle-based devices in humid ambient was also studied and the results were correlated to the consequence of sample washing. A suitable sensing mechanism within the purview of Langmuir model is discussed to understand the role of washing of the palladium nanoparticle yield.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Figure 1
Figure 2
Figure 3
Figure 4
Figure 5
Figure 6

Similar content being viewed by others

References

  1. Cho T J, Pettibone J M, Gorham J M, Nguyen T M, MacCuspie R I, Gigault J et al 2015 Langmuir 31 7673

    Article  CAS  Google Scholar 

  2. Saha B, Evers T H and Prins M W J 2014 Anal. Chem. 86 8158

    Article  CAS  Google Scholar 

  3. Billing B K, Agnihotri P K and Singh N 2017 J. Mater. Chem. C 5 4226

    Article  Google Scholar 

  4. Adams S M, Campione S, Caldwell J D, Bezares F J, Culbertson J C, Capolino F et al 2012 Small 8 2239

    Article  CAS  Google Scholar 

  5. Orchard K L, Shaffer M S P and Williams C K 2012 Chem. Mater. 24 2443

    Article  CAS  Google Scholar 

  6. Kim D S, Park M S and Jang J H 2011 J. Nanosci. Nanotechnol. 11 7407

    Article  CAS  Google Scholar 

  7. Pooja, Barman P B and Hazra S K 2018 J. Cluster. Sci. 29 1209

  8. Gupta D, Dutta D, Kumar M, Barman P B, Sarkar C K, Basu S et al 2014 Sens. Actuators B 196 215

    Article  CAS  Google Scholar 

  9. Nehl C L, Liao H and Hafner J H 2006 Nano Lett. 6 683

    Article  CAS  Google Scholar 

  10. Tagliazucchi M, Blaber M G, Schatz G C, Weiss E A and Szleifer I 2012 ACS Nano. 6 8397

    Article  CAS  Google Scholar 

  11. Yang D, Chen Y, Peng H, Chen G and Lin Z 2018 Nanoscale 10 22750

    Article  CAS  Google Scholar 

  12. Budijono S J, Russ B, Saad W, Adamson D H and Prud’homme R K 2010 Colloids Surf. A 360 105

    Article  CAS  Google Scholar 

  13. Calabrese I, Merli M and Liveri M L T 2015 Spectrochim. Acta A 142 150

    Article  CAS  Google Scholar 

  14. Sung C S P, Pyun E and Sun H L 1986 Macromolecules 19 2922

    Article  CAS  Google Scholar 

  15. Griffiths P C, Hirst N, Paul A, King S M, Heenan R K and Farley R 2004 Langmuir 20 6904

    Article  CAS  Google Scholar 

  16. Strasser P, Koh S, Anniyev T, Greeley J, More K, Yu C F et al 2010 Nat. Chem. 2 454

    Article  CAS  Google Scholar 

  17. Gan L, Yu R, Luo J, Cheng Z and Zhu J 2012 J. Phys. Chem. Lett. 3 934

    Article  CAS  Google Scholar 

  18. Walia S, Gupta R, Rao K D M and Kulkarni G U 2016 ACS Appl. Mater. Interfaces 8 23419

    Article  CAS  Google Scholar 

  19. Gupta R, Sagade A A and Kulkarni G U 2012 Int. J. Hydrog. Energy 37 9443

    Article  CAS  Google Scholar 

  20. Hassan K and Chung G S 2017 Sens. Actuators B 239 824

    Article  CAS  Google Scholar 

  21. Teng J, Bates S, Engers D A, Leach K, Schields P and Yang Y 2010 J. Pharm. Sci. 99 3815

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to PARTHA BIR BARMAN.

Electronic supplementary material

Below is the link to the electronic supplementary material.

Supplementary material 1 (DOC 171 kb)

Rights and permissions

Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

BHARDWAJ, P., BARMAN, P.B. & HAZRA, S.K. Hydrogen response of palladium nanoparticles washed with different solvents. Bull Mater Sci 44, 45 (2021). https://doi.org/10.1007/s12034-020-02323-z

Download citation

  • Received:

  • Accepted:

  • Published:

  • DOI: https://doi.org/10.1007/s12034-020-02323-z

Keywords

Navigation